Tailoring of the properties of long glass fibre reinforced thermoplastics:
Saved in:
| Main Author: | |
|---|---|
| Format: | Thesis Book |
| Language: | English |
| Published: |
Kaiserslautern
Institut für Verbundwerkstoffe
c 2004
|
| Series: | IVW-Schriftenreihe
47 |
| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Physical Description: | XIII, 123 S. Ill., graph. Darst. |
| ISBN: | 3934930433 |
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Record in the Search Index
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| adam_text | TAILORING OF THE PROPERTIES OF LONG GLASS FIBRE REINFORCED
THERMOPLASTICS
VOM FACHBEREICH FUR MASCHINENBAU UND VERFAHRENSTECHNIK
DER TECHNISCHEN UNIVERSITAT KAISERSLAUTERN
ZUR VERLEIHUNG DES AKADEMISCHEN GRADES
DOKTOR-LNGENIEUR (DR.-LNG.)
GENEHMIGTE DISSERTATION
VON
DIPL.-LNG. JUHA HARTIKAINEN
AUS ESPOO, FINNLAND
TAG DER MUNDLICHEN PRUFUNG:
PRUFUNGSVORSITZENDER:
1. BERICHTERSTATTER:
2. BERICHTERSTATTER:
23. JULI 2004
PROF. DR.-LNG. D.-H. HELLMANN
PROF. DR.-LNG. K. FRIEDRICH
PROF. DR.-LNG. S. TOLL
D386
INDEX
INDEX
ACKNOWLEDGEMENTS
ABBREVIATIONS AND SYMBOLS VII
ABSTRACT X
KURZFASSUNG XII
1 INTRODUCTION TO THE TOPIC 1
2 DISCONTINUOUS LONG GLASS FIBRE REINFORCED THERMO-
PLASTICS (LFT): PROPERTIES AND THEIR MODIFICATION 5
2.1 MANUFACTURE AND PROPERTIES OF LFT COMPOSITES 5
2.1.1 LFT MANUFACTURING METHODS 5
2.1.2 PROPERTIES 7
2.2 COMPOSITE MATERIALS BASED ON THERMOPLASTIC STYRENIC RESINS 10
2.2.1 THERMOPLASTIC STYRENIC RESINS 10
2.2.2 COMPOSITES BASED ON THERMOPLASTIC STYRENIC RESINS 12
2.3 POLYPROPYLENE HYBRID COMPOSITES 14
2.3.1 POLYPROPYLENE 14
2.3.2 POLYPROPYLENE COMPOSITES 15
2.3.3 PARTICLE FILLED POLYPROPYLENE 16
2.3.4 THERMOPLASTIC HYBRID REINFORCEMENT SYSTEMS 18
2.4 WATER RESISTANCE OF LONG GLASS FIBRE REINFORCED POLYAMIDE COMPOSITES
20
2.4.1 POLYAMIDE AND ITS BLENDS 20
2.4.1.1 POLYAMIDE-PHENOLIC RESIN BLENDS 22
2.4.2 POLYAMIDE COMPOSITES 24
2.4.2.1 WATER IN POLYAMIDE COMPOSITES 25
3 AIMS OF THE WORK 27
INDEX
4 MATERIALS AND SAMPLE PREPARATION 31
4.1 MATERIAL SYSTEM A: THERMOPLASTIC STYRENIC COMPOSITES 31
4.1.1 MATERIALS 31
4.1.2 SAMPLE PREPARATION 31
4.2 MATERIAL SYSTEM B: POLYPROPYLENE HYBRID COMPOSITES 31
4.2.1 MATERIALS 31
4.2.2 SAMPLE PREPARATION 32
4.3 MATERIAL SYSTEM C: POLYAMIDE COMPOSITES 34
4.3.1 MATERIALS 34
4.3.2 SAMPLE PREPARATION 34
5 CHARACTERISATION METHODS 35
5.1 MECHANICAL TESTING 35
5.1.1 TENSILE STRENGTH TEST 35
5.1.2 CHARPY IMPACT TOUGHNESS TEST 35
5.1.3 DYNAMIC MECHANICAL THERMAL ANALYSIS 35
5.1.4 FRACTURE MECHANICAL TEST 36
5.2 MICROSCOPIC METHODS 36
5.2.1 OPTICAL MICROSCOPY 36
5.2.2 SCANNING ELECTRON MICROSCOPY 37
5.2.3 TRANSMISSION ELECTRON MICROSCOPY 37
5.3 DIFFERENTIAL SCANNING CALORIMETRY 37
5.4 FOURIER TRANSFORM INFRARED SPECTROSCOPY 37
5.5 OPTICAL IMAGE ANALYSIS 38
5.6 ACOUSTIC EMISSION ANALYSIS 39
5.7 DENSITY MEASUREMENTS 39
5.8 SOLUTION VISCOSITY ANALYSIS 40
INDEX
5.9 THEORETICAL CALCULATIONS 41
6 RESULTS AND DISCUSSION 43
6.1 SYSTEM A: LGF REINFORCED THERMOPLASTIC STYRENIC RESINS 43
6.1.1 IMPROVEMENT OF THE INTERFACIAL PROPERTIES IN LGF STYRENICS 43
6.1.2 DEVELOPMENT OF LGF CONCENTRATE FOR THERMOPLASTIC STYRENICS 49
6.1.3 CONCLUSIONS 54
6.2 SYSTEM B: LGF-PP/MINERAL FILLER HYBRID COMPOSITES 56
6.2.1 EFFECT OF FILLERS ON CRYSTALLINE MORPHOLOGY OF PP 56
6.2.2 EFFECT OF FILLERS ON FIBRE ORIENTATION AND LENGTH IN LGF-PP
COMPOSITES 58
6.2.2.1 FIBRE ORIENTATION 58
6.2.2.2 FIBRE LENGTH DISTRIBUTION 60
6.2.3 TENSILE PROPERTIES OF LGF-PP/FILLER HYBRID COMPOSITES 62
6.2.4 IMPACT ENERGY OF LGF-PP/FILLER HYBRID COMPOSITES 64
6.2.5 FRACTURE TOUGHNESS OF PP-LGF/FILLER HYBRID COMPOSITES 66
6.2.6 CONCLUSIONS 75
6.3 SYSTEM C: IMPROVED WATER RESISTANCE OF LGF REINFORCED POLYAMIDE
COMPOSITES 77
6.3.1 CHEMICAL STRUCTURE AND MORPHOLOGY OF POLYAMIDE-PHENOLIC
RESIN BLENDS 77
6.3.1.1 CALCULATIONS 77
6.3.1.2 FOURIER TRANSFORM INFRARED SPECTROSCOPY OF PA66-PFR
BLENDS 81
6.3.1.3 DIFFERENTIAL SCANNING CALORIMETRY OF PA66-PFR BLENDS 85
6.3.1.4 MICROSCOPY STUDIES OF PA66-PFR BLENDS 90
6.3.2 PROPERTIES OF LGF REINFORCED POLYAMIDE-PHENOLIC RESIN BLENDS 92
JY INDEX
6.3.2.1 WATER ABSORPTION OF LGF REINFORCED PA66-PFR BLENDS 92
6.3.2.2 TENSILE PROPERTIES OF LGF REINFORCED PA66-PFR BLENDS 93
6.3.2.3 IMPACT ENERGY OF LGF REINFORCED PA66-PFR BLENDS 95
6.3.2.4 THERMAL BEHAVIOUR OF LGF REINFORCED PA66-PFR BLENDS ... 97
6.3.2.5 ELECTRON MICROSCOPY STUDIES OF LGF REINFORCED
PA66-PFR BLENDS 99
6.3.3 CONCLUSIONS 101
7 CONCLUDING REMARKS 103
8 REFERENCES 109
LIST OF PUBLICATIONS
LIST OF STUDENT WORKS
CURRICULUM VITAE
|
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| discipline | Maschinenbau / Maschinenwesen Werkstoffwissenschaften / Fertigungstechnik |
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| spelling | Hartikainen, Juha Verfasser aut Tailoring of the properties of long glass fibre reinforced thermoplastics Juha Hartikainen Kaiserslautern Institut für Verbundwerkstoffe c 2004 XIII, 123 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier IVW-Schriftenreihe 47 Zugl.: Kaiserslautern, Techn. Univ., Diss., 2004 Glasfaserverstärkter Thermoplast (DE-588)4157432-1 gnd rswk-swf Faserverstärkter Thermoplast (DE-588)4626537-5 gnd rswk-swf Glasfaser (DE-588)4021153-8 gnd rswk-swf (DE-588)4113937-9 Hochschulschrift gnd-content Glasfaserverstärkter Thermoplast (DE-588)4157432-1 s DE-604 Glasfaser (DE-588)4021153-8 s 1\p DE-604 Faserverstärkter Thermoplast (DE-588)4626537-5 s 2\p DE-604 IVW-Schriftenreihe 47 (DE-604)BV013248875 47 DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=012908435&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis 1\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk 2\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk |
| spellingShingle | Hartikainen, Juha Tailoring of the properties of long glass fibre reinforced thermoplastics IVW-Schriftenreihe Glasfaserverstärkter Thermoplast (DE-588)4157432-1 gnd Faserverstärkter Thermoplast (DE-588)4626537-5 gnd Glasfaser (DE-588)4021153-8 gnd |
| subject_GND | (DE-588)4157432-1 (DE-588)4626537-5 (DE-588)4021153-8 (DE-588)4113937-9 |
| title | Tailoring of the properties of long glass fibre reinforced thermoplastics |
| title_auth | Tailoring of the properties of long glass fibre reinforced thermoplastics |
| title_exact_search | Tailoring of the properties of long glass fibre reinforced thermoplastics |
| title_full | Tailoring of the properties of long glass fibre reinforced thermoplastics Juha Hartikainen |
| title_fullStr | Tailoring of the properties of long glass fibre reinforced thermoplastics Juha Hartikainen |
| title_full_unstemmed | Tailoring of the properties of long glass fibre reinforced thermoplastics Juha Hartikainen |
| title_short | Tailoring of the properties of long glass fibre reinforced thermoplastics |
| title_sort | tailoring of the properties of long glass fibre reinforced thermoplastics |
| topic | Glasfaserverstärkter Thermoplast (DE-588)4157432-1 gnd Faserverstärkter Thermoplast (DE-588)4626537-5 gnd Glasfaser (DE-588)4021153-8 gnd |
| topic_facet | Glasfaserverstärkter Thermoplast Faserverstärkter Thermoplast Glasfaser Hochschulschrift |
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