200 and more NMR experiments: a practical course
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| Previous Title: | Braun, Siegmar 100 and more basic NMR experiments |
|---|---|
| Main Authors: | , |
| Format: | Book |
| Language: | English |
| Published: |
Weinheim
Wiley-VCH
2004
|
| Edition: | [3. ed., rev. and expanded] |
| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Item Description: | Hier auch später erschienene, unveränderte Nachdrucke |
| Physical Description: | XV, 838 S. Ill., graph. Darst. |
| ISBN: | 3527310673 |
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| 084 | |a CHE 244f |2 stub | ||
| 100 | 1 | |a Berger, Stefan |d 1946-2023 |e Verfasser |0 (DE-588)124698107 |4 aut | |
| 245 | 1 | 0 | |a 200 and more NMR experiments |b a practical course |c Stefan Berger ; Siegmar Braun |
| 246 | 1 | 3 | |a Two hundred and more NMR experiments |
| 250 | |a [3. ed., rev. and expanded] | ||
| 264 | 1 | |a Weinheim |b Wiley-VCH |c 2004 | |
| 300 | |a XV, 838 S. |b Ill., graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 500 | |a Hier auch später erschienene, unveränderte Nachdrucke | ||
| 650 | 4 | |a Spectroscopie de la résonance magnétique nucléaire | |
| 650 | 4 | |a Nuclear magnetic resonance spectroscopy | |
| 650 | 0 | 7 | |a Experiment |0 (DE-588)4015999-1 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a NMR-Spektroskopie |0 (DE-588)4075421-2 |2 gnd |9 rswk-swf |
| 689 | 0 | 0 | |a NMR-Spektroskopie |0 (DE-588)4075421-2 |D s |
| 689 | 0 | 1 | |a Experiment |0 (DE-588)4015999-1 |D s |
| 689 | 0 | |5 DE-604 | |
| 700 | 1 | |a Braun, Siegmar |e Verfasser |4 aut | |
| 780 | 0 | 0 | |i Frühere Ausg. u.d.T. |a Braun, Siegmar |t 100 and more basic NMR experiments |
| 856 | 4 | 2 | |m Digitalisierung UB Augsburg |q application/pdf |u http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=012780351&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |3 Inhaltsverzeichnis |
| 999 | |a oai:aleph.bib-bvb.de:BVB01-012780351 | ||
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| _version_ | 1804132726361554944 |
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| adam_text | Contents
Preface
v
Chapter
1
The
NM R
Spectrometer
1
1.
1 Components of an
NM R
Spectrometer
1
1.1.1
The Magnet
1
1.1.2
The Spectrometer Cabinet
2
1.1.3
The Computer
3
1.1.4
Maintenance
3
1.2
Tuning a Probe-Head
3
1.3
The Lock Channel
4
1.4
The Art of Shimming
6
1.4.1
The Shim Gradients
6
1.4.2
The.Shimming Procedure
8
1.4.3
Gradient Shimming
11
Chapter
2
Determination of Pulse-Duration
14
Exp.
2.1:
Determination of the
90°
Ή
Transmitter Pulse-Duration
15
Exp.
2.2:
Determination of the
90°
bC Transmitter Pulse-Duration
18
Exp.
2.3:
Determination of the
90°
Ή
Decoupler Pulse-Duration
21
Exp.
2.4: .
The
90°
Ή
Pulse with Inverse Spectrometer Configuration
24
Exp.
2.5:
The
90°
L C Decoupler Pulse with Inverse Configuration
27
Exp.
2.6:
Composite Pulses
30
Exp.
2.7:
Radiation Damping
33
Exp.
2.8:
Pulse and Receiver Phases
36
Exp.
2.9:
Determination of Radiofrequency Power
39
Chapter
3
Routine NMR Spectroscopy and Standard Tests
43
Exp.
3.1 :
The Standard
H NMR
Experiment
44
Exp.
3.2:
The Standard 13C NMR Experiment
49
Exp.
3.3:
The Application of Window Functions
54
Exp.
3.4:
Computer-Aided Spectral Analysis
58
Exp.
3.5:
Line Shape Test for
Ή
NMR Spectroscopy
61
Exp.
3.6:
Resolution Test for
Ή
NMR Spectroscopy
64
Exp.
3.7:
Sensitivity Test for
H NMR
Spectroscopy
67
Exp.
3.8:
Line Shape Test for I3C NMR Spectroscopy
70
Exp.
3.9:
ASTM
Sensitivity Test for
C NMR Spectroscopy
73
Exp.
3.10:
Sensitivity Test for T NMR Spectroscopy
76
Exp.
3.11:
Quadrature Image Test
79
Exp.
3.12:
Dynamic Range Test for Signal Amplitudes
82
Exp.
3.13: 13°
Phase Stability Test
85
Exp.
3.14:
Radiofrequency Field Homogeneity
88
Chapter
4
Decoupling Techniques
91
Exp.
4.1 :
Decoupler Calibration for Homonuclear Decoupling
92
Exp.
4.2:
Decoupler Calibration for Heteronuclear Decoupling
95
Exp.
4.3:
Low-Power Calibration for Heteronuclear Decoupling
98
Exp.
4.4:
Homonuclear Decoupling
101
Exp.
4.5:
Homonuclear Decoupling at Two Frequencies
104
Exp.
4.6:
The Homonuclear SPT Experiment
107
Exp.
4.7:
The Heteronuclear SPT Experiment
110
Exp.
4.8:
The Basic Homonuclear
NOE
Difference Experiment
113
Exp.
4.9: 1
D
Nuclear Overhauser Difference Spectroscopy
116
Exp.
4.10:
ID
NOE
Spectroscopy with Multiple Selective Irradiation
1
1
9
Exp.
4.11 :
Ή
Off-Resonance Decoupled I3C NMR Spectra
122
Exp.
4.12:
The Gated H-Decoupling Technique
125
Exp.
4.13:
The Inverse Gated H-Decoupling Technique
128
Exp.
4.14:
Ή
Single-Frequency Decoupling of I3C NMR Spectra
131
Exp.
4.15:
Ή
Low-Power Decoupling of I3C NMR Spectra
134
Exp.
4.16:
Measurement of the Heteronuclear Overhauser Effect
137
Chapter
5
Dynamic NMR Spectroscopy
140
Exp.
5.1:
Low-Temperature Calibration Using
Methanol 141
Exp.
5.2:
High-Temperature Calibration Using 1,2-Ethanediol
145
Exp.
5.3:
Dynamic
Ή
NMR Spectroscopy on Dimethylformamide
149
Exp.
5.4:
The Saturation Transfer Experiment
152
Exp.
5.5:
Measurement of the Rotating-Frame Relaxation Time T p
155
Chapter
6
ID
M
ultipulse Sequences
159
Exp.
6.
1
:
Measurement of the Spin-Lattice Relaxation Time T
160
Exp.
6.2:
Measurement of the Spin-Spin Relaxation Time T2
164
Exp.
6.3:
С
NMR Spectra with SEFT
167
Exp.
6.4:
- С
NMR Spectra with APT
170
Exp.
6.5:
The Basic INEPT Technique
173
Exp.
6.6:
1NEPT+
176
Exp.
6.7:
Refocused INEPT
179
Exp.
6.8:
Reverse INEPT
182
Exp.
6.9:
DEPT-
135 185
Exp.
6.10:
Editing I3C NMR Spectra Using
DEPT
188
Exp.
6.11:
DEPTQ
191
Exp.
6.12:
Multiplicity Determination Using PENDANT
194
Exp.
6.13:
ID-INADEQUATE
197
Exp.
6.14:
The BIRD Filter
201
Exp.
6.15:
TANGO
204
Exp.
6.16:
The Heteronuclear Double-Quantum Filter
207
Exp.
6.17:
Purging with a Spin-Lock Pulse
210
Exp.
6.18:
Water Suppression by Presaturation
213
Exp.
6.19:
Water Suppression by the Jump-and-Return Method
216
Chapter
7
NMR Spectroscopy with Selective Pulses
219
Exp.
7.1:
Determination of a Shaped
90°
Ή
Transmitter Pulse
220
Exp.
7.2:
Determination of a Shaped
90°
Ή
Decoupler Pulse
223
Exp.
7.3:
Determination of a Shaped
90°
13C Decoupler Pulse
226
Exp.
7.4:
Selective Excitation Using DANTE
229
Exp.
7.5:
SELCOSY
232
Exp.
7.6:
SELINCOR: Selective Inverse H,C Correlation via ./(CH)
235
Exp.
7.7:
SELINQUATE
238
Exp.
7.8:
Selective TOCSY
242
Exp.
7.9:
INAPT
246
Exp.
7.10:
Determination of Long-Range C,H Coupling Constants
249
Exp.
7.11:
SELRESOLV
252
Exp.
7.12:
SERF
255
Chapter
8
Auxiliary Reagents, Quantitative Determinations,
258
and Reaction Mechanisms
Exp.
8.1: ■
Signal Separation Using
a
Lanthanide
Shift Reagent
259
Exp.
8.2:
Signal Separation of Enantiomers Using a Chiral Shift Reagent
262
Exp.
8.3:
Signal Separation of Enantiomers Using a Chiral Solvating Agent
265
Exp.
8.4:
Determination of Enantiomeric Purity with Pirkle s Reagent
268
Exp.
8.5:
Determination of Enantiomeric Purity by P NMR
271
Exp.
8.6:
Determination of Absolute Configuration by the Advanced
Mosher Method
274
Exp.
8.7:
Aromatic Solvent-Induced Shift
(ASIS)
277
Exp.
8.8:
NMR Spectroscopy of OH Protons and H/D Exchange
280
Exp.
8.9:
Water Suppression Using an Exchange Reagent
283
Exp.
8.10:
Isotope Effects on Chemical Shielding
286
Exp.
8.11 :
pKa Determination by I3C NMR
290
Exp.
8.12:
Determination of Association Constants Ka
293
Exp.
8.13:
Saturation Transfer Difference NMR
298
Exp.
8.14:
The Relaxation Reagent
Crtacac).,
302
Exp.
8.15:
Determination of Paramagnetic Susceptibility by NMR
305
Exp.
8.16:
Ή
and 13C NMR of Paramagnetic Compounds
308
Exp.
8.17:
The CIDNP Effect
312
Exp.
8.18:
Quantitative
Ή
NMR Spectroscopy: Determination of the
Alcohol Content of Polish Vodka
315
Exp.
8.19:
Quantitative nC NMR Spectroscopy with Inverse Gated
H-Decoupling
318
Exp.
8.20:
NMR Using Liquid-Crystal Solvents
321
Chapter
9
Heteronuclear NMR Spectroscopy
324
Exp.
9.1:
H-Decoupled^N NMR Spectra Using
DEPT
330
Exp.
9.2:
H-Coupled
5N NMR Spectra Using
DEPT
333
Exp.
9.3:
|C)F NMR Spectroscopy
336
Exp.
9.4:
: Si NMR Spectroscopy Using
DEPT
339
Exp.
9.5:
29Si NMR Spectroscopy
Using Spin-Lock Polarization
342
Exp.
9.6:
9Sn NMR Spectroscopy
346
Exp.
9.7:
2H NMR Spectroscopy
349
Exp.
9.8:
В
NMR Spectroscopy
352
Exp.
9.9:
17O NMR Spectroscopy
Using
RIDE
355
Exp.
9.10:
47 49Ti NMR Spectroscopy
Using
ARING 358
Chapter
10
The Second Dimension
362
Exp.
10.1:
2D
J-Resolved
Ή
NMR Spectroscopy
367
Exp.
10.2:
2D/-Resolved UC NMR Spectroscopy
370
Exp.
10.3:
The Basic
Η,Η
-COSY
Experiment
373
Exp.
10.4:
Long-Range
COSY
377
Exp.
10.5:
Phase-Sensitive COSY
380
Exp.
10.6:
Phase-Sensitive COSY-45
383
Exp.
10.7:
E.COSY
386
Exp.
10.8:
Double-Quantum-Filtered COSY with Presaturation
389
Exp.
10.9:
Fully Coupled C,H Correlation (FUCOUP)
393
Exp.
10.10:
CH-Correlation by Polarization Transfer (HETCOR)
396
Exp.
10.11:
Long-Range CH-Correlation by Polarization Transfer
399
Exp.
10.12:
C,H Correlation via Long-Range Couplings (COLOC)
402
Exp.
10.13:
The Basic HMQC Experiment
405
Exp.
10.14:
Phase-Sensitive HMQC with BIRD Filter and GARP Decoupling
409
Exp.
10.15:
Poor Man s Gradient HMQC
412
Exp.
10.16:
Phase-Sensitive HMBC with BIRD Filter
415
Exp.
10.17:
The Basic HSQC Experiment
418
Exp.
10.18:
The HOHAHA or TOCSY Experiment
422
Exp.
10.19:
HETLOC
426
Exp.
10.20:
The NOESY Experiment
430
Exp.
10.21:
The CAMELSPIN or
ROES Y
Experiment
434
Exp.
10.22:
The HOESY Experiment
438
Exp.
10.23:
2D-IN ADEQUATE
441
Exp.
10.24:
The EXSY Experiment
445
Exp.
10.25:
Χ,Υ
-Correlation
448
Chapter
11
ID NMR Spectroscopy with Pulsed Field Gradients
453
Exp.
Exp.
E p.
Exp.
Exp.
Exp.
Exp.
Exp.
Exp.
Exp.
Exp.
1.1:
Calibration of Pulsed Field Gradients
455
1.2:
Gradient Pre-emphasis
458
1.3:
Gradient Amplifier Test
461
1
.4:
Determination of Pulsed Field Gradient Ring-Down Delays
464
1.5:
The Pulsed Field Gradient Spin-Echo Experiment
467
1.6:
Excitation Pattern of Selective Pulses
470
1.7:
The Gradient Heteronuclear Double-Quantum Filter
474
1.8:
The Gradient zz-Filter
477
1.9:
The Gradient-Selected Dual Step Low-Pass Filter
480
1.10:
gs-SELCOSY
484
1.11:
gs-SELTOCSY
488
Exp.
11.12:
DPFGSE-NOE
492
Exp.
11.13:
gs-SELINCOR
496
Exp.
11.14:
a/ß-SELINCOR-TOCSY
499
Exp.
11.15:
GRECCO
503
Exp.
11.16:
WATERGATE
506
Exp.
11.17:
Water Suppression by Excitation Sculpting
509
Exp.
11.18:
Solvent Suppression Using WET
512
Exp.
11.19:
DOSY
515
Exp.
11.20:
INEPT-DOSY
518
Exp.
11.21:
DOSY-HMQC
521
Chapter
1
2
2D NMR Spectroscopy With Field Gradients
525
Exp.
12.1:
gs-COSY
526
Exp.
12.2:
Constant-Time COSY
530
Exp.
12.3:
Phase-Sensitive gs-DQF-COSY
534
Exp.
12.4:
gs-HMQC
538
Exp.
12.5:
gs-HMBC
542
Exp.
12.6:
ACCORD-HMBC
546
Exp.
12.7: ·
HMSC
550
Exp.
12.8:
Phase-Sensititive gs-HSQC with Sensitivity Enhancement
554
Exp.
12.9:
Edited HSQC with Sensitivity Enhancement
558
Exp.
12.10:
HSQC with Adiabatic Pulses for High-Field instruments
563
Exp.
12.11:
gs-TOCSY
567
Exp.
12.12:
gs-HMQC-TOCSY
571
Exp.
12.13:
gs-HETLOC
575
Exp.
12.14:
gs-J-Resolved
H MBC
581
Exp. 12.15í
2Q-HMBC
585
Exp.
12.16:
H-Detected 2D
INEPT-INADEQUATE
589
Exp.
12.17:
1,1
-ADEQUATE
593
Exp.
12.18:
Ι,η
-ADEQUATE
597
Exp.
12.19:
gs-NOESY
601
Exp.
12.20:
gs-HSQC-NOESY
604
Exp.
12.21:
gs-HOESY
608
Exp.
12.22:
H,15N
Correlation with gs-HMQC
612
Chapter
13
The Third Dimension
616
Exp.
13.1:
3D
HMQC-COSY
618
Exp.
13.2:
SDgs-HSQC-TOCSY
622
Exp.
13.3:
3DH,C,P-Correlation
626
Exp.
13.4:
3DHMBC
630
Chapter
14
Solid-State NMR Spectroscopy
634
Exp.
14.1:
Shimming Solid-State Probe-Heads
635
Exp.
14.2:
Adjusting the Magic Angle
639
Exp.
14.3:
Hartmann-Hahn Matching
642
Exp.
14.4:
The Basic
CP/MAS
Experiment
645
Нхр.
14.5:
TOSS
649
Exp.
14.6:
SELTICS
653
Пхр.
14.7:
Connectivity Determination in the Solid State
656
Exp.
14.8:
REDOR
659
Exp.
14.9:
High-Resolution Magic-Angle Spinning
663
Chapter
15
Protein NMR
666
Exp.
15.1 :
Pulse Determination for Protein NMR
670
Exp.
15.2:
HN-HSQC
673
Exp.
15.3:
HC-HSQC
678
Exp.
15.4:
MUSIC
682
Exp.
15.5:
HN-Correlation using TROSY
688
Exp.
15.6:
HN-TOCSY-HSQC
692
Exp.
15.7:
HNCA
698
Exp.
15.8:
HN(CO)CA
705
Exp.
15.9:
HNCO
711
Exp.
15.10:
HN(CA)CO
718
Exp.
15.11:
HCACO
725
Exp.
15.12:
HCCH-TOCSY
732
Exp.
15.13:
CBCANH
739
Нхр.
15.14:
CBCA(CO)NH
746
Exp.
15.15:
HBHA(CBCACO)NH
753
Exp.
15.16:
HN(CA)NNH
760
Exp.
15.17:
HN-NOESY-HSQC
766
Exp.
15.18:
HC-NOESY-HSQC
773
Exp.
15.19: 3D
HCN-NOESY
779
Exp.
15.20:
HNCA-J
785
Appendix
1 791
Pulse Programs
Appendix
2 794
Instrument Dialects
Appendix
3 797
Classification of Experiments
Appendix
4 . 799
Elementary Product Operator Fonnalism Rules
Appendix
5 802
Chemical Shift and Spin-Coupling Data for Ethyl Crotonate and Strychnine
Glossary and Index
804
|
| any_adam_object | 1 |
| author | Berger, Stefan 1946-2023 Braun, Siegmar |
| author_GND | (DE-588)124698107 |
| author_facet | Berger, Stefan 1946-2023 Braun, Siegmar |
| author_role | aut aut |
| author_sort | Berger, Stefan 1946-2023 |
| author_variant | s b sb s b sb |
| building | Verbundindex |
| bvnumber | BV019312623 |
| callnumber-first | Q - Science |
| callnumber-label | QD96 |
| callnumber-raw | QD96.N8 |
| callnumber-search | QD96.N8 |
| callnumber-sort | QD 296 N8 |
| callnumber-subject | QD - Chemistry |
| classification_rvk | VG 9500 VG 9501 |
| classification_tum | CHE 244f |
| ctrlnum | (OCoLC)55685718 (DE-599)BVBBV019312623 |
| dewey-full | 543/.66 |
| dewey-hundreds | 500 - Natural sciences and mathematics |
| dewey-ones | 543 - Analytical chemistry |
| dewey-raw | 543/.66 |
| dewey-search | 543/.66 |
| dewey-sort | 3543 266 |
| dewey-tens | 540 - Chemistry and allied sciences |
| discipline | Chemie / Pharmazie Chemie |
| edition | [3. ed., rev. and expanded] |
| format | Book |
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| id | DE-604.BV019312623 |
| illustrated | Illustrated |
| indexdate | 2024-07-09T19:57:24Z |
| institution | BVB |
| isbn | 3527310673 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-012780351 |
| oclc_num | 55685718 |
| open_access_boolean | |
| owner | DE-20 DE-91G DE-BY-TUM DE-703 DE-M49 DE-BY-TUM DE-355 DE-BY-UBR DE-19 DE-BY-UBM DE-29T DE-384 DE-634 DE-83 DE-91S DE-BY-TUM DE-11 DE-188 DE-Er8 |
| owner_facet | DE-20 DE-91G DE-BY-TUM DE-703 DE-M49 DE-BY-TUM DE-355 DE-BY-UBR DE-19 DE-BY-UBM DE-29T DE-384 DE-634 DE-83 DE-91S DE-BY-TUM DE-11 DE-188 DE-Er8 |
| physical | XV, 838 S. Ill., graph. Darst. |
| publishDate | 2004 |
| publishDateSearch | 2004 |
| publishDateSort | 2004 |
| publisher | Wiley-VCH |
| record_format | marc |
| spelling | Berger, Stefan 1946-2023 Verfasser (DE-588)124698107 aut 200 and more NMR experiments a practical course Stefan Berger ; Siegmar Braun Two hundred and more NMR experiments [3. ed., rev. and expanded] Weinheim Wiley-VCH 2004 XV, 838 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Hier auch später erschienene, unveränderte Nachdrucke Spectroscopie de la résonance magnétique nucléaire Nuclear magnetic resonance spectroscopy Experiment (DE-588)4015999-1 gnd rswk-swf NMR-Spektroskopie (DE-588)4075421-2 gnd rswk-swf NMR-Spektroskopie (DE-588)4075421-2 s Experiment (DE-588)4015999-1 s DE-604 Braun, Siegmar Verfasser aut Frühere Ausg. u.d.T. Braun, Siegmar 100 and more basic NMR experiments Digitalisierung UB Augsburg application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=012780351&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Berger, Stefan 1946-2023 Braun, Siegmar 200 and more NMR experiments a practical course Spectroscopie de la résonance magnétique nucléaire Nuclear magnetic resonance spectroscopy Experiment (DE-588)4015999-1 gnd NMR-Spektroskopie (DE-588)4075421-2 gnd |
| subject_GND | (DE-588)4015999-1 (DE-588)4075421-2 |
| title | 200 and more NMR experiments a practical course |
| title_alt | Two hundred and more NMR experiments |
| title_auth | 200 and more NMR experiments a practical course |
| title_exact_search | 200 and more NMR experiments a practical course |
| title_full | 200 and more NMR experiments a practical course Stefan Berger ; Siegmar Braun |
| title_fullStr | 200 and more NMR experiments a practical course Stefan Berger ; Siegmar Braun |
| title_full_unstemmed | 200 and more NMR experiments a practical course Stefan Berger ; Siegmar Braun |
| title_old | Braun, Siegmar 100 and more basic NMR experiments |
| title_short | 200 and more NMR experiments |
| title_sort | 200 and more nmr experiments a practical course |
| title_sub | a practical course |
| topic | Spectroscopie de la résonance magnétique nucléaire Nuclear magnetic resonance spectroscopy Experiment (DE-588)4015999-1 gnd NMR-Spektroskopie (DE-588)4075421-2 gnd |
| topic_facet | Spectroscopie de la résonance magnétique nucléaire Nuclear magnetic resonance spectroscopy Experiment NMR-Spektroskopie |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=012780351&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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