Spectral-isotopic method for the determination of hydrogen in metals:
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| Main Authors: | , , |
|---|---|
| Format: | Book |
| Language: | English |
| Published: |
London
Butterworth
1961
|
| Online Access: | Inhaltsverzeichnis |
| Item Description: | Aus dem Russ. übers. |
| Physical Description: | XIX, 100 S. Ill., graph. Darst. |
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| 100 | 1 | |a Zajdelʹ, Aleksandr N. |e Verfasser |4 aut | |
| 240 | 1 | 0 | |a Spektralʹno-izotopnyj metod opredelenija vodoroda v metallach |
| 245 | 1 | 0 | |a Spectral-isotopic method for the determination of hydrogen in metals |c A. N. Zaidel' ; A. A. Petrov ; G. V. Veinberg. Transl. by A. Behr. Ed. by G. E. Cardam. Publ. in association with Department of Scientific and Industrial Research |
| 264 | 1 | |a London |b Butterworth |c 1961 | |
| 300 | |a XIX, 100 S. |b Ill., graph. Darst. | ||
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| 500 | |a Aus dem Russ. übers. | ||
| 700 | 1 | |a Petrov, Arkadij A. |e Verfasser |4 aut | |
| 700 | 1 | |a Vejnberg, Galina V. |e Verfasser |4 aut | |
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| adam_text | Spectral-Isotopic Method
for the Determination of
Hydrogen in Metals
A N ZAIDEL
A A PETROV
G V VEINBERG
Translated, by
A BEHR
EDITEDBY
GE GARDAM
Published, in association with
DEPARTMENTOFSCIENTIFICANDINDUSTRIALRESEARCH
LONDON
BUTTERWORTHS
CONTENTS
Page
PREFACE v i i
INTRODUCTION i x
1 Effect of hydrogen on properties of metals ix
2 Interaction of hydrogen with metals x
3 Physico-chemical methods of determining hydrogen
inmetalsxiv
4 Spectral determination of hydrogen in metals xvi
1 METHOD OF ISOTOPIC BALANCING 1
1 Isotopic dilution 1
2 Determination of hydrogen in metals by means of
isotopic balancing 3
2 ISOTOPIC ANALYSIS OF HYDROGEN 10
1 Methods of isotopic analysis of hydrogen 10
2 Spectral-isotopic analysis of hydrogen 11
3 Causes of the deviation of the intensity ratio of
the lines of the isotopes from the concentration
ratio16
4 Examination of the conditions for isotopic analysis 20
t
3 DESCRIPTION OF APPARATUS 31
1 Vacuum apparatus 31
2 Apparatus for producing the deuterium 36
3 Resistance furnaces and temperature measurement 37
4 The high frequency generator 38
5 The spectroscopic apparatus 39
6 The photoelectric recording unit 45
4 PREPARATION AND CARRYING OUT OF ANALYSES 51
1 Production of deuterium 51
2 Isotopic analysis 53
3 Isotopic balancing 57
Preparatory operations 59
CONTENTS
Page
5 USE OF THE METHOD OF ISOTOPIC BALANCING FOR THE
ANALYSIS OF SOME METALS 69
1 Analysis of zinc, cadmium, aluminium and alloy
Kh20N80 69
2 Analysis of iron and steels 73
3 Analysis of titanium 76
4 Analysis of zirconium, tantalum, niobium and
uranium80
CONCLUSION85
APPENDICES89
I Separation of isotopes in the capillaries of the flow
system89
II Preparation of the standard samples 90
III Method of taking into account the systematic error
in the preparation of standard samples resulting
from the incorrect determination of the concen
tration of hydrogen in the deuterium being used 93
IV Example of the calculation of the hydrogen con
tentofmetal94
BIBLIOGRAPHY and REFERENCES 96
I
|
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| indexdate | 2024-07-09T19:19:37Z |
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| spelling | Zajdelʹ, Aleksandr N. Verfasser aut Spektralʹno-izotopnyj metod opredelenija vodoroda v metallach Spectral-isotopic method for the determination of hydrogen in metals A. N. Zaidel' ; A. A. Petrov ; G. V. Veinberg. Transl. by A. Behr. Ed. by G. E. Cardam. Publ. in association with Department of Scientific and Industrial Research London Butterworth 1961 XIX, 100 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Aus dem Russ. übers. Petrov, Arkadij A. Verfasser aut Vejnberg, Galina V. Verfasser aut HEBIS Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=010581847&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Zajdelʹ, Aleksandr N. Petrov, Arkadij A. Vejnberg, Galina V. Spectral-isotopic method for the determination of hydrogen in metals |
| title | Spectral-isotopic method for the determination of hydrogen in metals |
| title_alt | Spektralʹno-izotopnyj metod opredelenija vodoroda v metallach |
| title_auth | Spectral-isotopic method for the determination of hydrogen in metals |
| title_exact_search | Spectral-isotopic method for the determination of hydrogen in metals |
| title_full | Spectral-isotopic method for the determination of hydrogen in metals A. N. Zaidel' ; A. A. Petrov ; G. V. Veinberg. Transl. by A. Behr. Ed. by G. E. Cardam. Publ. in association with Department of Scientific and Industrial Research |
| title_fullStr | Spectral-isotopic method for the determination of hydrogen in metals A. N. Zaidel' ; A. A. Petrov ; G. V. Veinberg. Transl. by A. Behr. Ed. by G. E. Cardam. Publ. in association with Department of Scientific and Industrial Research |
| title_full_unstemmed | Spectral-isotopic method for the determination of hydrogen in metals A. N. Zaidel' ; A. A. Petrov ; G. V. Veinberg. Transl. by A. Behr. Ed. by G. E. Cardam. Publ. in association with Department of Scientific and Industrial Research |
| title_short | Spectral-isotopic method for the determination of hydrogen in metals |
| title_sort | spectral isotopic method for the determination of hydrogen in metals |
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