Thermodynamic properties of complex fluid mixtures: research report
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| Language: | English |
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Weinheim
Wiley-VCH
2004
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| Online Access: | Inhaltsverzeichnis |
| Physical Description: | XXI, 652 S. graph. Darst. |
| ISBN: | 3527277706 |
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| 245 | 1 | 0 | |a Thermodynamic properties of complex fluid mixtures |b research report |c Deutsche Forschungsgemeinschaft. Ed. by Gerd Maurer |
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| 650 | 4 | |a Thermodynamics | |
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| adam_text | DEUTSCHE FORSCHUNGSGEMEINSCHAFT THERMODYNAMIC PROPERTIES OF COMPLEX
FLUID MIXTURES EDITED BY GERD MAURER RESEARCH REPORT WILEY- ^ ^ ^ _ DFG
WILEY-VCH VERLAG GMBH & CO. KGAA CONTENTS I CHEMICAL REACTIVE SYSTEMS 1
EXPERIMENTAL AND THEORETICAL INVESTIGATIONS AT THE SYSTEM CH 3 OH + H 2
S0 4 + H 2 0 3 MATTHIAS BEHMANN, SAE-HOON KIM, HANS-JUERGEN KOSS, AND
KLAUS LUCAS 1.1 ABSTRACT 3 1.2 INTRODUCTION 3 1.3 EXPERIMENTAL METHODS 4
1.3.1 APPARATUS 4 1.3.2 MATERIALS 5 1.3.3 CALIBRATION AND ANALYSIS OF
RAMAN SIGNALS 5 1.4 THEORY 9 1.5 RESULTS AND DISCUSSION 12 1.5.1 THE
SYSTEM CH 3 OH + H 2 0 13 1.5.2 THE SYSTEM H 2 S0 4 + H 2 0 13 1.5.3 THE
SYSTEM CH 3 OH -F H 2 S0 4 + H 2 0 17 1.5.4 THE SYSTEM CH3SO4H + CH 3 OH
18 1.5.5 THE SYSTEM CH 3 OH + H 2 S0 4 + H 2 0 WITH CH 3 S0 4 H 18 1.5.6
THE SYSTEM CH 3 OH + H 2 S0 4 + H 2 0 WITH CH 3 S0 4 H AND (CH 3 ) 2 0
21 1.6 CONCLUSION 22 REFERENCES 23 NOMENCLATURE 24 2 MEASUREMENT OF
BINARY PHASE EQUILIBRIA OF ESTERIFICATION SYSTEMS .... 26 MARKO
TISCHMEYER AND WOLFGANG ARLT 2.1 ABSTRACT 26 2.2 INTRODUCTION 26 2.3
FUNDAMENTALS 27 2.3.1 CALCULATION OF LIQUID AND VAPOR PHASE FUGACITIES
27 2.3.2 REACTION SPACE AND COORDINATES TRANSFORMATION 28 2.3.3 STANDARD
STATE IN VLE CALCULATION WITH CHEMICAL EQUILIBRIUM 31 2.3.4 KINETIC
MODELLING 32 2.4 EXPERIMENTAL 34 V CONTENTS 2.4.1 CHEMICALS 34 2.4.2
EQUIPMENT AND EXPERIMENTAL PROCEDURE 35 2.5 RESULTS 39 2.6 CONCLUSION 45
REFERENCES 45 NOMENCLATURE 46 3 SOLUBILITY OF CARBON DIOXIDE IN AQUEOUS
ALKANOLAMINE SOLUTIONS IN THE TEMPERATURE RANGE 313 TO 353 K AND
PRESSURES UP TO 2.7 MPA 4 8 DIRK SILKENBAEUMER, BERND RUMPF, AND RUEDIGER
N. LICHTENTHALER 3.1 ABSTRACT 48 3.2 INTRODUCTION 48 3.3 EXPERIMENTAL 49
3.3.1 APPARATUS 49 3.3.2 PROCEDURE 50 3.3.3 MATERIALS 51 3.4 RESULTS 51
3.4.1 TEST OF PROCEDURE: RESULTS FOR THE SYSTEM C0 2 + H 2 0 51 3.4.2
RESULTS FOR THE SYSTEM C0 2 + MDEA + H 2 0 52 3.4.3 RESULTS FOR THE
SYSTEM C0 2 + AMP + H 2 0 54 3.4.4 RESULTS FOR THE SYSTEM C0 2 + MDEA +
AMP + H 2 0 57 3.5 MODELING 58 3.6 COMPARISON WITH LITERATURE DATA 64
3.7 CONCLUSIONS 66 REFERENCES 66 NOMENCLATURE 67 4 THE INFLUENCE OF N0 2
ON COMPLEX PHASE AND REACTION EQUILIBRIA IN WET FLUE GAS CLEANING
PROCESSES 69 MOHAMMAD A. SIDDIQI, JENS PETERSEN, AND KLAUS LUCAS 4.1
ABSTRACT 69 4.2 INTRODUCTION , 69 4.3 EXPERIMENTAL 71 4.3.1 APPARATUS 71
4.3.2 MATERIALS 72 4.4 EXPERIMENTAL RESULTS 73 4.4.1 STUDIES AT 298.65 K
73 4.4.2 STUDIES AT 318.45 K AND 333.35 K 77 4.5 MODEL CALCULATIONS 78
4.6 RESULTS AND DISCUSSION 85 REFERENCES 88 NOMENCLATURE 90 VI CONTENTS
5 AN INFRARED SPECTROSCOPIC INVESTIGATION OF THE SPECIES DISTRIBUTION IN
THE SYSTEM NH 3 + C0 2 + H 2 0 92 UTE LICHTFERS AND BERND RUMPF 5.1
ABSTRACT 92 5.2 INTRODUCTION 92 5.3 PHASE EQUILIBRIA AND QUANTITATIVE
INFRARED SPECTROSCOPY IN THE SYSTEM NH 3 + C0 2 + H 2 0 93 5.4
EXPERIMENTAL 98 5.4.1 APPARATUS 98 5.4.2 MATERIALS 99 5.4.3 RESULTS 99
5.4.4 CALIBRATION MEASUREMENTS 101 5.4.5 EVALUATION OF SPECTRA 102
5.4.5.1 SPECTRA TAKEN IN CALIBRATION MEASUREMENTS 102 5.4.5.2 SPECTRA IN
THE SYSTEM NH 3 + C0 2 + H 2 0 103 5.5 RESULTS 106 5.6 MODELING 107 5.7
PREDICTION OF CALORIC EFFECTS 112 5.8 CONCLUSION 114 ACKNOWLEDGEMENTS
115 REFERENCES 115 NOMENCLATURE 117 II ASSOCIATING MIXTURES 121 6 VLLE
FOR MIXTURES OF WATER AND ALCOHOLS: MEASUREMENTS AND CORRELATIONS 123
FRANK GREMER, GERHARD HERRES, AND DIETER GORENFLO 6.1 ABSTRACT 123 6.2
INTRODUCTION 123 6.3 EXPERIMENTAL 124 6.4 EXPERIMENTAL RESULTS 127 6.5
CONCLUSIONS 132 REFERENCES 133 NOMENCLATURE 134 7 PHASE EQUILIBRIA IN
TERNARY SYSTEMS CONTAINING PHENOLS, HYDROCARBONS, AND WATER 135 JUERGEN
SCHMELZER, KLAUS TAUBERT, ANTJE MARTIN, RENE MEINHARDT, AND JOCHEN KEMPE
7.1 ABSTRACT 135 7.2 INTRODUCTION 135 7.3 EXPERIMENTAL 136 7.3.1
LIQUID-LIQUID EQUILIBRIUM 136 7.3.2 VAPOR-LIQUID EQUILIBRIUM 137 VII
CONTENTS 7.3.3 INFRARED SPECTROSCOPIC INVESTIGATIONS 139 7.3.4 MATERIALS
139 7.4 THEORY 139 7.4.1 UNIFAC GROUP-CONTRIBUTION METHOD 139 7.4.2 NRTL
AND UNIQUAC GIBBS EXCESS ENERGY MODELS 140 7.4.3 ESD EQUATION OF STATE
(ESD-EOS) 140 7.5 RESULTS AND DISCUSSIONS 142 7.5.1 PREDICTION USING
UNIFAC 142 7.5.2 CORRELATION OF BINARY DATA WITH NRTL, UNIQUAC, AND
ESD-EOS 143 7.5.3 PREDICTION FOR TERNARY SYSTEMS WITH NRTL, UNIQUAC, AND
ESD-EOS ... 143 7.6 CONCLUSIONS 146 ACKNOWLEDGEMENTS 147 REFERENCES 147
NOMENCLATURE 148 8 INFLUENCE OF ADDITIVES ON HYDROPHOBIE ASSOCIATION IN
POLYNARY AQUEOEUS MIXTURES. AN NMR RELAXATION AND SELF-DIFFUSION STUDY
150 MANFRED HOLZ AND MANGHAIKO MAYELE 8.1 ABSTRACT 150 8.2 INTRODUCTION
150 8.3 METHODS AND EXPERIMENTAL 152 8.3.1 THEORETICAL BACKGROUND OF THE
^-PARAMETER PROCEDURE 153 8.3.2 EXPERIMENTAL DETERMINATION OF THE
^-PARAMETER 154 8.3.2.1 MEASUREMENT OF THE INTERMOLECULAR RELAXATION
RATE 154 8.3.2.2 PFG NMR FOR THE DETERMINATION OF SELF-DIFFUSION
COEFFICIENTS 155 8.3.2.3 MEASUREMENT OF THE SPIN DENSITY 155 8.3.3
EXPERIMENTAL 156 8.3.3.1 APPARATUS 156 8.3.3.2 SAMPLE PREPARATION 156
8.3.4 MATERIALS 157 8.4 RESULTS AND DISCUSSION 157 8.4.1 THE BINARY
SYSTEM: WATER + TERT-BUTANOL 157 8.4.2 THE TERNARY SYSTEM: WATER +
TERT-BUTANOL + UREA 159 8.4.2.1 UREA EFFECT ON THE TRANSLATIONAL
DYNAMICS OF TERT-BUTANOL AND WATER 160 8.4.2.2 INFLUENCE OF UREA ON
TERT-BUTANOL SELF-ASSOCIATION 166 8.4.3 WATER + ETHYLENE GLYCOL SYSTEMS
169 8.4.3.1 THE BINARY SYSTEM: WATER + ETHYLENE GLYCOL 170 8.4.3.2
TERNARY SYSTEMS: WATER + ETHYLENE GLYCOL + ADDITIVE 172 THE ADDITIVE
DIOXANE 172 THE ADDITIVE N-BUTANOL 174 SALTS AS ADDITIVES 175 8.5
CONCLUSIONS 177 REFERENCES 178 NOMENCLATURE 181 VIII CONTENTS III
AQUEOUS SOLUTIONS OF STRONG ELECTROLYTES 185 9 PHASE EQUILIBRIA OF
AQUEOUS SOLUTIONS CONTAINING VOLATILE ELECTROLYTES . 187 JUERGEN
ZIPPRIAN, NILS ELM, AND KARLHEINZ SCHABER 9.1 ABSTRACT 187 9.2
INTRODUCTION 187 9.3 EXPERIMENTAL 188 9.3.1 APPARATUS 188 9.3.2
IR-SPECTRA AND CALIBRATION CURVES 190 9.4 RESULTS AND DISCUSSION 192
9.4.1 SYSTEM NH 3 + H 2 0 192 9.4.2 SYSTEM HCL + H 2 0 195 9.4.3 SYSTEM
HBR + H 2 0 197 9.4.4 SYSTEM HCL + CACL 2 + H 2 0 198 9.4.5 SYSTEM HCL +
HBR + H 2 0 200 9.5 THEORY 202 9.6 RESULTS AND DISCUSSION 203 9.6.1
PARTIAL PRESSURE OF HCL 203 9.6.2 PARTIAL PRESSURE OF H 2 0 204 9.7
CONCLUSIONS 204 REFERENCES 205 NOMENCLATURE 206 10 EXPERIMENTAL
DETERMINATION AND PREDICTION OF PHASE EQUILIBRIA IN SYSTEMS CONTAINING
STRONG ELECTROLYTES 208 MAGNUS TOPPHOFF, CHRISTIAN ROSE, JOERN KIEPE, AND
JUERGEN GMEHLING 10.1 ABSTRACT 208 10.2 INTRODUCTION 209 10.3 GROUP
CONTRIBUTION MODEL FOR THE PREDICTION OF ACTIVITY COEFFICIENTS IN
SYSTEMS CONTAINING STRONG ELECTROLYTES 210 10.3.1 THERMODYNAMIC
FRAMEWORK 210 10.3.1.1 ESTIMATION OF PARAMETERS 213 10.3.2 RESULTS AND
DISCUSSION FOR VLE DATA 214 10.3.3 PREDICTION OF SOLID-LIQUID EQUILIBRIA
217 10.3.3.1 THEORY 218 10.3.3.2 RESULTS AND DISCUSSION 218 10.3.4
PREDICTION OF GAS SOLUBILITIES 221 10.3.4.1 MODIFIED PSRK GROUP
CONTRIBUTION METHOD 222 10.3.4.2 RESULTS AND DISCUSSION 224 10.4
DETERMINATION OF VAPOR-LIQUID EQUILIBRIA FOR SYSTEMS CONTAINING STRONG
ELECTROLYTES 225 10.4.1 MATERIALS 226 10.4.2 HEADSPACE GAS
CHROMATOGRAPHY 226 10.4.3 EBULLIOMETRY 226 10.4.3.1 EXPERIMENTAL RESULTS
227 IX CONTENTS 10.4.4 MEASUREMENT OF ACTIVITY COEFFICIENTS AT INFINITE
DILUTION IN ELECTROLYTE SYSTEMS USING THE DILUTOR TECHNIQUE 228 10.4.4.1
EXPERIMENTAL AND MEASUREMENT PROCEDURE 228 10.4.4.2 PRINCIPLE OF THE
APPLIED METHOD 230 10.4.4.3 EXPERIMENTAL RESULTS 231 10.4.5 MEASUREMENT
OF THE MEAN ACTIVITY COEFFICIENTS OF IONS BY DETERMINATION OF THE
ELECTROMOTIVE FORCE 233 10.5 CONCLUSION 235 REFERENCES 236 NOMENCLATURE
238 11 ION COORDINATION AND THERMODYNAMIC MODELING OF MOLTEN SALT
HYDRATE MIXTURES 241 WOLFGANG VOIGT, KAY HETTRICH, AND DEWEN ZENG 11.1
ABSTRACT 241 11.2 INTRODUCTION 241 11.3 EXPERIMENTAL 243 11.3.1
SOLID-LIQUID EQUILIBRIA 243 11.3.2 UV-VIS SPECTROSCOPY 243 11.3.3 RAMAN
SPECTROSCOPY 243 11.3.4 CHEMICALS 244 11.4 RESULTS AND DISCUSSION 244
11.4.1 SYSTEM MGCL 2 + CUCL 2 + H 2 0 244 11.4.1.1 SOLID-LIQUID
EQUILIBRIA 244 11.4.1.2 UV-VIS SPECTROSCOPY 247 11.4.1.3 RAMAN SPECTRA
250 11.4.2 MGCL 2 + CSCL + H Z O 251 11.5 THERMODYNAMIC MODELING 253
11.5.1 MODELING STRATEGY 253 11.5.2 COMPUTATIONAL PROBLEMS OF PARAMETER
ESTIMATION 254 11.5.3 MODEL DEVELOPMENT FOR THE SYSTEMS MGCL 2 + KCL + H
2 0 AND MGCL 2 + CUCL 2 + H 2 0 255 11.5.3.1 BINARY SYSTEMS 255 MGCL 2 +
KCL 255 KCL + H 2 0 257 MGCL 2 + H 2 0 258 11.5.3.2 TERNARY SYSTEMS 260
MGCL 2 + KCL + H 2 0 260 MGCL 2 + CUCL 2 + H 2 0 261 11.6 CONCLUSIONS
263 ACKNOWLEDGEMENTS 263 REFERENCES 263 NOMENCLATURE 266 X CONTENTS 12
EFFECTS OF SALTS ON EXCESS ENTHALPIES OF BINARY LIQUID MIXTURES 268
PETER ULBIG, THORSTEN FRIESE, AND KATRIN WAGNER 12.1 ABSTRACT 268 12.2
INTRODUCTION 268 12.3 EXPERIMENTAL/METHODS 269 12.3.1 APPARATUS 269
12.3.1.1 CALORIMETRIC MEASUREMENTS 269 12.3.1.2 SOLUBILITY MEASUREMENTS
271 12.3.1.3 CONDUCTIVITY MEASUREMENTS 272 12.3.1.4 MEASUREMENT OF THE
EXCESS VOLUME 273 12.3.2 MATERIALS 273 12.3.3 ANALYSIS 273 12.4 RESULTS
AND DISCUSSION 275 12.4.1 EXCESS ENTHALPY 275 12.4.1.1 EFFECT OF THE
SALT CONCENTRATION 275 12.4.1.2 EFFECT OF TEMPERATURE 275 12.4.1.3
EFFECT OF DIFFERENT ALCOHOLS 275 12.4.1.4 EFFECT OF DIFFERENT SALTS 278
12.4.2 SOLUBILITY 279 12.4.3 CONDUCTIVITY 279 12.4.4 EXCESS VOLUME 280
12.5 THEORY 280 12.5.1 THE HEACE MODEL 280 12.5.2 CONDUCTIVITY THEORY
282 12.6 RESULTS AND DISCUSSION 283 12.7 CONCLUSION 286 ACKNOWLEDGEMENTS
287 REFERENCES 287 NOMENCLATURE 288 13 HYDRATE EQUILIBRIA IN AQUEOUS
SOLUTIONS CONTAINING INHIBITORS 290 ARMIN M. ROCK AND LOTHAR R. OELLRICH
13.1 ABSTRACT 290 13.2 INTRODUCTION 290 13.3 FUNDAMENTAL HYDRATE
STRUCTURAL AND PHASE BEHAVIOR 292 13.4 EXPERIMENTAL 296 13.4.1 APPARATUS
296 13.4.2 PROCEDURE 298 13.5 THEORY 300 13.5.1 THERMODYNAMIC FRAMEWORK
300 SOLID HYDRATE PHASE 301 FLUID PHASES 304 13.5.2 ESTIMATION OF
HYDRATE CAVITY INTERACTION PARAMETERS 306 13.6 RESULTS AND DISCUSSION
308 13.7 CONCLUSIONS 315 ACKNOWLEDGEMENT 316 XI CONTENTS REFERENCES 316
NOMENCLATURE 319 IV PHASE EQUILIBRIUM OF AQUEOUS TWO-PHASE SYSTEMS 321
14 EXPERIMENTAL AND THEORETICAL INVESTIGATIONS ON THE PRECIPITATION OF
POLYELECTROLYTES FROM AQUEOUS SOLUTIONS BY NEUTRAL POLYMERS 323 THOMAS
GRUENFELDER AND GERD MAURER 14.1 ABSTRACT 323 14.2 INTRODUCTION 323 14.3
EXPERIMENTAL/METHODS 325 14.3.1 MATERIALS 325 14.3.2 EXPERIMENTAL
PROCEDURES 326 14.3.2.1 TURBIDITY MEASUREMENTS 326 14.3.2.2 COMPOSITIONS
OF COEXISTING PHASES 328 FREEZE DRYING 328 ATOMIC ABSORPTION
SPECTROSCOPY 329 POLYMER CONCENTRATIONS 329 14.4 RESULTS AND DISCUSSION
329 14.4.1 OVERVIEW 329 14.4.2 CLOUD POINTS 330 14.4.3 COMPOSITION OF
COEXISTING PHASES 331 14.4.4 INFLUENCE OF MOLECULAR WEIGHT ON THE PHASE
BEHAVIOR 332 14.4.5 INFLUENCE OF TEMPERATURE ON THE PHASE BEHAVIOR 332
14.5 MODELING 334 14.5.1 INTRODUCTION TO VERS-PE 334 14.5.2
DETERMINATION OF PARAMETERS OF THE VERS-PE MODEL 338 14.5.3 RESULTS OF
CORRELATIONS/PREDICTIONS WITH THE VERS-PE MODEL 340 14.6 CONCLUSIONS 341
ACKNOWLEDGEMENTS 341 REFERENCES 342 NOMENCLATURE 342 15 EXPERIMENTAL AND
THEORETICAL STUDIES ON PARTITIONING OF NATIVE AND UNFOLDED ENZYMES IN
AQUEOUS TWO-PHASE SYSTEMS 345 MARIA-REGINA KULA AND CHRISTIAN RAMSCH
15.1 ABSTRACT 345 15.2 INTRODUCTION 345 15.3 MATERIAL AND METHODS 346
15.3.1 CHEMICALS AND LYSOZYME MUTANTS 346 15.3.2 DETERMINATION OF PHASE
DIAGRAMS 347 15.3.3 PROTEIN CONFORMATION 347 15.3.4 PARTITION
COEFFICIENTS 348 15.4 RESULTS AND DISCUSSION 348 15.4.1 PHASE DIAGRAMS
OF QUATERNARY SYSTEMS 348 XII CONTENTS 15.4.2 STABILITY OF T 4-LYSOZYME
VARIANTS 350 15.4.3 PARTITION OF T 4-LYSOZYME VARIANTS 352 15.4.4 T
4-LYSOZYME UNFOLDING AND REFOLDING IN PEG + NA 2 S0 4 SYSTEMS 354 15.5
CONCLUSION 356 ACKNOWLEDGEMENTS 356 REFERENCES 356 NOMENCLATURE 357 16
EXPERIMENTAL AND THEORETICAL INVESTIGATIONS ON THE PARTITIONING OF
PROTEINS IN AQUEOUS TWO-PHASE SYSTEMS 359 JOCHEN BRENNEISEN AND GERD
MAURER 16.1 ABSTRACT 359 16.2 INTRODUCTION 359 16.3 THEORY 360 16.3.1
MODEL 360 16.3.2 GIBBS ENERGY OF THE AQUEOUS SOLUTIONS 363 16.3.3
CHEMICAL REACTIONS 363 16.4 EXPERIMENTAL/METHODS 364 16.4.1
LIQUID-LIQUID EQUILIBRIUM MEASUREMENTS 364 16.4.2 EXPERIMENTS ON
SUBSYSTEMS 365 16.4.2.1 ISOPIESTIC MEASUREMENTS 365 16.4.2.2 MEASUREMENT
OF PH 365 16.4.2.3 DETERMINATION OF THE PROTEIN NET-CHARGE 366 16.4.3
MATERIALS 366 16.5 EXPERIMENTAL RESULTS/MODELLING 367 16.5.1 PARAMETERS
FOR THE GIBBS EXCESS ENERGY MODEL 367 16.5.2 PROTEIN NET CHARGE 371
16.5.3 PROTEIN PARTITIONING 371 16.6 CONCLUSIONS 374 ACKNOWLEDGEMENTS
375 REFERENCES 375 NOMENCLATURE 376 V PHASE EQUILIBRIUM OF POLYMER
SYSTEMS 379 17 PHASE BEHAVIOR OF QUATERNARY POLYMER SOLUTIONS 381
CLAUDIA BARTH-WIEDMANN, MATTHIAS WUENSCH, AND BERNHARD ANTON WOLF 17.1
ABSTRACT 381 17.2 INTRODUCTION 381 17.3 EXPERIMENTAL PART 382 17.3.1
APPARATUS AND PROCEDURES 382 17.3.1.1 STATIC LIGHT SCATTERING 382
17.3.1.2 HEADSPACE-GASCHROMATOGRAPHY 382 17.3.1.3 DETERMINATION OF PHASE
DIAGRAMS 384 17.3.2 MATERIALS 384 XIII CONTENTS IIA THEORETICAL
BACKGROUND 385 17.4.1 FLORY-HUGGINS INTERACTION PARAMETERS 385 17.4.2
CALCULATION OF PHASE DIAGRAMS 387 17.4.3 CALCULATION OF VAPOR PRESSURES
389 17.5 RESULTS AND DISCUSSION 390 17.5.1 BINARY SYSTEMS 390 17.5.1.1
MIXED SOLVENTS 390 17.5.1.2 POLYMER SOLUTIONS 391 17.5.2 TERNARY SYSTEMS
393 17.5.2.1 PHASE DIAGRAMS 393 17.5.2.2 VAPOR PRESSURES 395 17.5.3
QUATERNARY SYSTEMS 398 17.6 CONCLUSIONS 399 ACKNOWLEDGEMENT 399
REFERENCES 400 NOMENCLATURE 401 ABBREVIATIONS 402 18 CALCULATION OF THE
HIGH PRESSURE PHASE EQUILIBRIUM OF MIXTURES OF ETHYLENE,
POLY(ETHYLENE-CO-VINYLACETATE) COPOLYMERS AND VINYL ACETATE WITH A CUBIC
EQUATION OF STATE 403 C. BROWARZIK, D. BROWARZIK, AND H. KEHLEN 18.1
ABSTRACT 403 18.2 INTRODUCTION 403 18.3 THEORY 405 18.3.1 SEGMENT-MOLAR
QUANTITIES AND POLYDISPERSITY 405 18.3.2 CALCULATION OF THE CLOUD-POINT
CURVES 407 18.3.3 CALCULATION OF THE COEXISTENCE CURVES 409 18.3.4
SAKO-WU-PRAUSNITZ EQUATION OF STATE (SWP-EOS) 411 18.3.5 FIT OF
PURE-COMPONENT PARAMETERS 412 18.4 RESULTS AND DISCUSSION 414 18.4.1 THE
BINARY SYSTEM ETHYLENE (A) + EVA (B) 414 18.4.2 THE BINARY SYSTEM
ETHYLENE (A) + VA (C) 421 18.4.3 THE BINARY SYSTEM EVA (B) + VA (C) 422
18.4.4 THE TERNARY SYSTEM 423 18.5 CONCLUSIONS 425 REFERENCES 426
NOMENCLATURE 428 19 MODELING OF COPOLYMER PHASE EQUILIBRIA USING THE
PERTURBED-CHAIN SAFT EQUATION OF STATE 430 FEELLY TUMAKAKA AND GABRIELE
SADOWSKI 19.1 ABSTRACT 430 19.2 INTRODUCTION 430 19.3 THEORY 431 19.3.1
COPOLYMER CONCEPT 431 XIV CONTENTS 19.3.2 PERTURBED-CHAIN SAFT AND ITS
EXTENSION TO COPOLYMER SYSTEMS 432 19.4 PURE-COMPONENT POLYMER
PARAMETERS 434 19.5 RESULTS FOR COPOLYMER SYSTEMS 437 19.5.1
POLY(ETHYLENE-CO-PROPYLENE) (PEP) SYSTEMS 437 19.5.2
POLY(ETHYLENE-CO-L-BUTENE) (EB) SYSTEMS 439 19.5.3
POLY(ETHYLENE-CO-VINYL ACETATE) (EVA) SYSTEMS 441 19.5.4
POLY(ETHYLENE-CO-METHYL ACRYLATE) (EMA) SYSTEMS 443 19.6 CONCLUSIONS 446
ACKNOWLEDGEMENTS 447 REFERENCES 447 NOMENCLATURE 449 20 CLOUD POINT
PRESSURES OF ETHENE + ACRYLATE + POLY(ETHENE-CO-ACRYLATE) SYSTEMS 451
MICHAEL BUBACK AND MARKUS BUSCH 20.1 ABSTRACT 451 20.2 INTRODUCTION 452
20.3 EXPERIMENTAL METHODS 455 20.4 RESULTS AND DISCUSSION 458 20.5
CONCLUSIONS 468 REFERENCES 468 NOMENCLATURE 470 21 GAS EXPANDED POLYMER
SOLUTIONS 472 BERND BUNGERT AND WOLFGANG ARLT 21.1 ABSTRACT 472 21.2
INTRODUCTION 472 21.3 FUNDAMENTALS 474 21.3.1 SEPARATION PROCESSES 474
21.3.1.1 ANTISOLVENT CRYSTALLIZATION 474 21.3.1.2 LIQUID-LIQUID-PHASE
SEPARATION OF POLYMER SOLUTIONS 475 21.3.1.3 LIQUID-LIQUID-VAPOR TO
VITRIFIED LIQUID-VAPOR EQUILIBRIUM 475 21.3.1.4 CHANGE OF PROPERTIES BY
THE DISSOLUTION OF COMPRESSED GASES 477 21.3.2 THERMODYNAMIC MODELING OF
PHASE EQUILIBRIUM 477 21.4 EXPERIMENTAL 478 21.4.1 APPARATUS AND
CHEMICALS 478 21.5 RESULTS 479 21.6 CONCLUSION 484 ACKNOWLEDGEMENT 484
REFERENCES 484 NOMENCLATURE 486 XV CONTENTS 22 CALCULATION OF THE
STABILITY AND OF THE PHASE EQUILIBRIUM ON THE SYSTEM METHYLCYCLOHEXANE +
POLYSTYRENE BASED ON AN EQUATION OF STATE 488 DIETER BROWARZIK AND MARIO
KOWALEWSKI 22.1 ABSTRACT 488 22.2 INTRODUCTION 488 22.3 THEORY 490
22.3.1 CALCULATION OF THE CLOUD-POINT AND THE SHADOW CURVES 490 22.3.2
CALCULATION OF THE SPINODAL CURVE 492 22.3.3 CALCULATION OF CRITICAL
POINTS 494 22.3.4 SAKO-WU-PRAUSNITZ EQUATION OF STATE (SWP-EOS) 495 22.4
RESULTS 497 22.4.1 PARAMETER FIT 497 22.4.2 FORMATION OF THE HOUR-GLASS
CURVES IN THE POLYDISPERSE CASE 498 22.4.3 APPLICATION OF THE EOS TO A
REAL POLYDISPERSE SYSTEM MCH + PS 504 22.5 CONCLUSIONS 506 REFERENCES
506 NOMENCLATURE 507 VI HIGH-PRESSURE PHASE EQUILIBRIA 509 23 PHASE
EQUILIBRIUM (SOLID-LIQUID-GAS) IN BINARY SYSTEMS OF POLYETHYLENE
GLYCOLS), POLYETHYLENE GLYCOL) DIMETHYL ETHER WITH CARBON DIOXIDE,
PROPANE, AND NITROGEN 511 ECKHARD WEIDNER AND VERONIKA WIESMET 23.1
ABSTRACT 511 23.2 INTRODUCTION 512 23.3 EXPERIMENTAL EQUIPMENT, METHODS,
AND SUBSTANCES 512 23.3.1 POLYMERS 512 23.3.2 DETERMINATION OF MELTING
POINT 512 23.3.3 DETERMINATION OF SOLUBILITY 513 23.3.4 CORRELATION OF
THE EXPERIMENTAL RESULTS WITH SAFT 514 23.4 RESULTS AND DISCUSSION 514
23.4.1 PEG + CARBON DIOXIDE 515 23.4.1.1 LIQUID + GAS SYSTEMS 515
23.4.1.2 SOLID-LIQUID TRANSITION 517 23.4.2 PEG + NITROGEN 519 23.4.2.1
LIQUID + GAS SYSTEMS 519 23.4.2.2 SOLID-LIQUID TRANSITION 520 23.4.3 PEG
+ PROPANE 520 23.4.3.1 LIQUID + GAS SYSTEMS 520 23.4.3.2 SOLID-LIQUID
TRANSITION 523 23.4.4 COMPARISON OF THE PHASE BEHAVIOR OF LIQUID AND
SOLID PEGS WITH DIFFERENT GASES 524 23.4.5 INFLUENCE OF FUNCTIONAL
GROUPS 525 23.4.5.1 SHORT POLYMER CHAMS 526 XVI CONTENTS 23.4.5.2 LONGER
POLYMER CHAINS 528 23.4.6 CLASSIFICATION OF PHASE BEHAVIOR FOR (SOLID
AND LIQUID) PEGS AND PRESSURIZED GASES 529 23.5 APPLICATION 530 23.5.1
POWDER GENERATION FROM POLYETHYLENE GLYCOLS) 531 23.5.2 POLYGLYCOLS AS
LUBRICANTS IN CLIMATISATION SYSTEMS 531 23.6 CONCLUSION 532
ACKNOWLEDGEMENTS 533 REFERENCES 533 NOMENCLATURE 534 24 MEASUREMENTS AND
MODELING OF HIGH-PRESSURE FLUID PHASE EQUILIBRIUM OF SYSTEMS CONTAINING
BENZENE DERIVATIVES AND C0 2 535 GERD BRUNNER, OLIVER PFOHL, AND
STANIMIR PETKOV 24.1 ABSTRACT 535 24.2 INTRODUCTION 536 24.3
EXPERIMENTAL/ METHODS 536 24.3.1 APPARATUS 536 24.3.2 PROCEDURE 537
24.3.3 ANALYSIS 538 24.3.4 MATERIALS 539 24.4 RESULTS AND DISCUSSION 539
24.4.1 BINARY SYSTEMS: BENZENE DERIVATIVE + CARBON DIOXIDE 539 24.4.2
TERNARY SYSTEMS 543 24.4.3 DISCUSSION OF EXPERIMENTAL RESULTS 550
24.4.3.1 BINARY SYSTEMS BENZENE DERIVATIVE + CARBON DIOXIDE 550 24.4.3.2
TERNARY SYSTEM O-CRESOL +/?-CRESOL + CARBON DIOXIDE 550 24.4.3.3 TERNARY
SYSTEMS BENZENE DERIVATIVE + WATER + CARBON DIOXIDE 551 24.4.3.4 TERNARY
SYSTEMS CRESOL ISOMER + ETHANOL + CARBON DIOXIDE 552 24.5 THEORY/METHODS
552 24.5.1 EQUATIONS OF STATE 552 24.5.1.1 CUBIC EOS 552 24.5.1.2
ASSOCIATION EOS 554 24.5.1.3 MIXING RULES 555 24.5.2 PARAMETER
ESTIMATION 556 24.5.2.1 PURE COMPONENT PARAMETERS 556 24.5.2.2 BINARY
SYSTEMS: DETERMINING BINARY INTERACTION PARAMETERS 559 24.5.2.3 TERNARY
SYSTEMS 559 24.6 RESULTS AND DISCUSSION 563 24.7 CONCLUSION 565
REFERENCES 566 NOMENCLATURE 567 XVII CONTENTS VII PHASE EQUILIBRIUM IN
MICROEMULSION SYSTEMS 569 25 THE POTENTIAL OF SURFACTANTS MODIFIED
SUPERCRITICAL FLUIDS FOR DISSOLVING DIFFERENT CLASSES OF SUBSTANCES 571
UTA LEWIN-KRETZSCHMAR AND PETER HARTING 25.1 ABSTRACT 571 25.2
INTRODUCTION 571 25.3 EXPERIMENTAL/METHODS 573 25.3.1 EQUIPMENT 573
25.3.2 PROCEDURE 573 25.3.3 ANALYSIS 575 25.3.4 DYEING EXPERIMENTS 575
25.3.5 MATERIALS 576 25.3.6 STATISTICAL METHODS 578 25.4 CORRELATION AND
PREDICTION OF THE SOLUBILITY OF DYES IN SUPERCRITICAL FLUIDS . 578
25.4.1 METHOD OF MITRA/WILSON 579 25.4.2 METHOD OF DEL VALLE/AGUILERA
579 25.4.3 GROUP CONTRIBUTION EQUATION OF STATE 580 25.5 RESULTS AND
DISCUSSION 580 25.5.1 SOLUBILITY OF NITROAROMATICS IN PURE AND
SURFACTANT-MODIFIED SCC0 2 580 25.5.2 SOLUBILITY OF ADAMANTANE IN PURE
AND SURFACTANT-MODIFIED SUPERCRITICAL FLUIDS 584 25.5.3 SOLUBILITY OF
POLAR DYES IN PURE AND SURFACTANT-MODIFIED SCC0 2 AND SCC 2 H 6 585
25.5.4 DYEING TESTS 592 25.6 CONCLUSION 593 ACKNOWLEDGEMENT 594
REFERENCES 594 NOMENCLATURE 596 26 LIQUID-LIQUID PHASE EQUILIBRIA IN
MICROEMULSION FORMING SYSTEMS BASED ON CARBOHYDRATE SURFACTANTS 598
SABINE ENDERS, DIRK HAENTZSCHEL, HEIKE KAHL, AND KONRAD QUITZSCH 26.1
ABSTRACT 598 26.2 INTRODUCTION 598 26.3 EXPERIMENTAL 601 26.3.1
APPARATUS 601 26.3.1.1 PHASE EQUILIBRIUM 601 26.3.1.2 SURFACE TENSION
602 26.3.1.3 INTERFACIAL TENSION 603 26.3.1.4 DYNAMIC LIGHT SCATTERING
603 26.3.2 MATERIALS 603 26.4 THEORY 604 26.4.1 MICELLE FORMATION MODEL
604 26.4.2 G E -MODEL 609 26.4.3 LANDAU-THEORY 611 XVIII CONTENTS 26.5
RESULTS AND DISCUSSION 613 26.5.1 STRATEGY AND CONCEPTS OF THE
INVESTIGATIONS 613 26.5.2 BINARY SUBSYSTEMS 614 26.5.3 TERNARY
SUBSYSTEMS 615 26.5.4 QUATERNARY SYSTEMS 619 26.6 CONCLUSION 625
ACKNOWLEDGEMENT 626 REFERENCES 626 NOMENCLATURE 629 27 INTERACTIONS OF
POLYELECTROLYTES AND ZWITTERIONIC SURFACTANTS IN AQUEOUS SOLUTION 632
HEINZ HOFFMANN, HOLGER LAUER, AND KLAUS REDLICH 21A ABSTRACT 632 27.2
INTRODUCTION 633 27.3 EXPERIMENTAL/METHODS 633 27.4 RESULTS AND
DISCUSSION 634 27.4.1 AQUEOUS SOLUTIONS OF POLYACRYLIC ACIDS 634 27.4.2
AQUEOUS SOLUTIONS OF C 14 DMAO 636 27.4.3 INTERACTIONS BETWEEN PAA AND C
14 DMAO IN AQUEOUS SOLUTION 638 27.4.4 MODIFIED PAAS IN AQUEOUS SOLUTION
642 27.4.5 INTERACTIONS BETWEEN MODIFIED PAAS AND C, 4 DMAO IN AQUEOUS
SOLUTION . 646 27.5 CONCLUSION 650 ACKNOWLEDGEMENT 651 REFERENCES 651
NOMENCLATURE 651
|
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| illustrated | Illustrated |
| indexdate | 2024-07-09T19:19:28Z |
| institution | BVB |
| institution_GND | (DE-588)2007744-0 |
| isbn | 3527277706 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-010574662 |
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| physical | XXI, 652 S. graph. Darst. |
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| spelling | Thermodynamic properties of complex fluid mixtures research report Deutsche Forschungsgemeinschaft. Ed. by Gerd Maurer Weinheim Wiley-VCH 2004 XXI, 652 S. graph. Darst. txt rdacontent n rdamedia nc rdacarrier Complex fluids Thermodynamics Thermodynamische Eigenschaft (DE-588)4126056-9 gnd rswk-swf Mehrstoffsystem (DE-588)4132152-2 gnd rswk-swf Komplexe Flüssigkeit (DE-588)4311495-7 gnd rswk-swf Flüssig-Flüssig-System (DE-588)4154706-8 gnd rswk-swf (DE-588)4143413-4 Aufsatzsammlung gnd-content Flüssig-Flüssig-System (DE-588)4154706-8 s Komplexe Flüssigkeit (DE-588)4311495-7 s Thermodynamische Eigenschaft (DE-588)4126056-9 s DE-604 Mehrstoffsystem (DE-588)4132152-2 s b DE-604 Maurer, Gerd Sonstige oth Deutsche Forschungsgemeinschaft Sonstige (DE-588)2007744-0 oth GBV Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=010574662&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Thermodynamic properties of complex fluid mixtures research report Complex fluids Thermodynamics Thermodynamische Eigenschaft (DE-588)4126056-9 gnd Mehrstoffsystem (DE-588)4132152-2 gnd Komplexe Flüssigkeit (DE-588)4311495-7 gnd Flüssig-Flüssig-System (DE-588)4154706-8 gnd |
| subject_GND | (DE-588)4126056-9 (DE-588)4132152-2 (DE-588)4311495-7 (DE-588)4154706-8 (DE-588)4143413-4 |
| title | Thermodynamic properties of complex fluid mixtures research report |
| title_auth | Thermodynamic properties of complex fluid mixtures research report |
| title_exact_search | Thermodynamic properties of complex fluid mixtures research report |
| title_full | Thermodynamic properties of complex fluid mixtures research report Deutsche Forschungsgemeinschaft. Ed. by Gerd Maurer |
| title_fullStr | Thermodynamic properties of complex fluid mixtures research report Deutsche Forschungsgemeinschaft. Ed. by Gerd Maurer |
| title_full_unstemmed | Thermodynamic properties of complex fluid mixtures research report Deutsche Forschungsgemeinschaft. Ed. by Gerd Maurer |
| title_short | Thermodynamic properties of complex fluid mixtures |
| title_sort | thermodynamic properties of complex fluid mixtures research report |
| title_sub | research report |
| topic | Complex fluids Thermodynamics Thermodynamische Eigenschaft (DE-588)4126056-9 gnd Mehrstoffsystem (DE-588)4132152-2 gnd Komplexe Flüssigkeit (DE-588)4311495-7 gnd Flüssig-Flüssig-System (DE-588)4154706-8 gnd |
| topic_facet | Complex fluids Thermodynamics Thermodynamische Eigenschaft Mehrstoffsystem Komplexe Flüssigkeit Flüssig-Flüssig-System Aufsatzsammlung |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=010574662&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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