In vivo EPR (ESR): theory and application
Saved in:
| Format: | Book |
|---|---|
| Language: | English |
| Published: |
New York [u.a.]
Kluwer Academic / Plenum Publ.
2003
|
| Series: | Biological magnetic resonance
18 |
| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Physical Description: | XXVII, 656 S. Ill., graph. Darst. |
| ISBN: | 0306477904 |
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MARC
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| 245 | 1 | 0 | |a In vivo EPR (ESR) |b theory and application |c ed. by Lawrence J. Berliner |
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Record in the Search Index
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| adam_text | Contents
Chapter 1
Introduction to in Vivo EPR
Harold M. Swartz and Lawrence J. Berliner
1. Aim and Scope of the Book 1
2. Rationale for in Vivo EPR 2
3. Challenges of in Vivo EPR 3
4. Types of Paramagnetic Species Observable with in Vivo EPR 6
5. Types of Instrumental Approaches Used for in Vivo EPR 8
6. Experiments with Animals 12
7. Conclusions and a Look to the Future 16
8. The Nomenclature of Biomedical EPR—Reducing the
Confusion 19
9. References 20
Section I. Theory and Instrumentation
Chapter 2
Principles of in Vivo EPR
Sankaran Subramanian, James B. Mitchell, andMurali C. Krishna
1. Introduction 23
2. Time Domain EPR 27
3. CW versus Time Domain EPR 34
4. Summary and Conclusions 38
5. References 39
x* CONTENTS
Chapter 3
Frequency and Power Considerations for in Vivo EPR and Related
Techniques
James M. S. Hutchison
1. Introduction 41
2. RF Absorption in Ideal Sample Shapes 43
3. Resonators and RF Absorption 47
4. Bi and Power 50
5. Localised EPR and Surface Coils 52
6. Summary and Conclusions 57
7. References 58
Chapter 4
CW EPR Signal Detection Bridges
Janusz Koscielniak
1. Introduction 61
2. Principles of CW Mode Signal DetectionI I I !!I ! I 62
3. Bridge Devices 64
4. Detectors 66
5. Automatic Frequency Control Circuits ... 68
6. The Complete CW EPR System ZZZZZZ Z Z . 70
7. Conclusions jq
8. Acknowledgments 72
9. References 72
Chapter 5
Resonators for Low Field in Vivo EPR
Kenneth A. Rubinson
1. Origin of Radiofrequency Resonance 73
2. Transmission Lines 7o
3. Matching Impedances . . . . . .. 83
4. Resonant Structures Used in Vivo 87
5. References ^
CONTENTS xxi
Chapter 6
Principles of Imaging
Periannan Kuppusamy, Michael Chzhan, and Jay L. Zweier
1. Introduction 99
2. Fundamentals of Imaging 100
3. Definition of Projection 110
4. Field Gradient Techniques 112
5. Projection Data Acquisition 114
6. Data Processing and Image Reconstruction 118
7. Software 130
8. Instrumentation 131
9. Magnet and Gradient Coil Design 132
10. Special Imaging Techniques/Applications 140
11. Scope and Limitations 147
12. Acknowledgments 148
13. References 148
Chapter 7
Time Domain Radio Frequency EPR Imaging
Sankaran Subramanian, James B. Mitchell, andMurali C. Krishna
1. Introduction 153
2. Challenges in Time Domain EPR Spectroscopy and Imaging at
RF 155
3. Instrumentation 162
4. Data Collection and Image Reconstruction 175
5. Spin Probes 187
6. Examples of Time Domain Imaging Experiments at 300 MHz.... 187
7. Conclusion and Future Directions 195
8. Acknowledgements 195
9. References 196
Section II. Biochemical Applications: Biochemistry and Biophysics
Chapter 8
Stable Soluble Paramagnetic Compounds
Howard J. Halpern
1. Introduction 201
xxti CONTENTS
2. What s in a Spectrum? 202
3. Nitroxyls 212
4. Trityls 222
5. Overview of Application of Infusible Paramagnetic
Compounds 226
6. Conclusions 229
7. Acknowledgments 229
8. References 229
Chapter 9
Stable Participate Paramagnetic Materials as Oxygen Sensors in EPR
Oximetry: Coals, Lithium Phthalocyanine, and Carbon Chars
R. B. Clarkson, Paul Ceroke, Shong Wan Norby, and
B. M. Odintsov
1. Introduction 234
2. Oxygen and EPR Line Width 237
3. Carbon Char Synthesis 239
4. Sensor Morphology 241
5. Chars as Oxygen Sensors 244
6. Dynamic Nuclear Polarization 248
7. DNP Imaging and Oximetry 253
8. Conclusions 255
9. Acknowledgments 255
10. References 256
Chapter 10
Packaging of Paramagnetic Materials in Oximetry and Other
Applications
Bernard Gallez
1. Introduction 260
2. Applications 267
3. Conclusions and Perspectives 281
4. Acknowledgments 281
5. References 281
CONTENTS „„,
Chapter 11
Spin Trapping in Vivo: Facts and Artifacts
Graham S. Timmins and Ke Man Liu
1. Introduction 285
2. Classes of Spin Traps 286
3. Considerations for in Vivo Spin Trapping Experiments 290
4. Potential Problems, Artifacts and General Recommendations
for in Vivo Spin Trapping 298
5. Future Prospects for in Vivo Spin Trapping 306
6. Acknowledgments 306
7. References 306
Chapter 12
Ex Vivo Detection of Free Radical Metabolites of Toxic Chemicals and
Drugs by Spin Trapping
Ronald P. Mason and Maria B. Kadiiska
1. Introduction 309
2. Spin Traps 309
3. Sensitivity Advance 310
4. Applications of Spin Trapping 310
5. Complete Table of All Free Radical Metabolites Detected by ex
VivoESR 314
6. References 319
Chapter 13
Chemistry and Biology of Nitric Oxide
Andrei M. Komarov
1. Introduction 325
2. Nitric Oxide Molecule: Redox Forms of NO 327
3. NO as an EPR Probe for Metalloproteins 331
4. Discovery of Endothelium Derived Relaxation Factor (EDRF)
and EPR Studies of EDRF 336
5. Biosynthesis of Nitric Oxide: Three Isoforms of Nitric Oxide
Synthase 340
6. Biological Functions and Molecular Targets of Nitric Oxide 346
7. Nitric Oxide in Disease 358
8. Global Importance of Nitric Oxide 363
xxiv CONTENTS
9. Acknowledgments 365
10. References 365
Chapter 14
In Vivo and in Vitro Detection of NO by EPR
Hirotada Fujii and Lawrence J. Berliner
1. Introduction 381
2. Physico Chemical Methods of Detecting NO 382
3. Detection of NO by EPR 382
4. Detection and Quantitation of NO in Biological Specimens 384
5. In Vivo Detection of NO Generated in Biological Systems 388
6. Visualization of NO Generation in Biological Systems 395
7. Conclusions and Perspectives 400
8. Acknowledgments 400
9. References 400
Chapter 15
The Measurement of Oxygen in Vivo Using EPR Techniques
Harold M. Swartz
1. Introduction 404
2. Methods and Materials Available for EPR Oximetry 408
3. Interactions and Use of Oxygen Sensitive Paramagnetic
Materials in Biological Systems 412
4. Physical Basis for EPR Oximetry 419
5. Overview of Results of EPR Oximetry 422
6. Summary and Conclusions 431
7. Acknowledgments 432
8. References 432
Chapter 16
Cardiac Applications of in Vivo EPR Spectroscopy and Imaging
JayL. Zweier, Alexandre Samouilov, andPeriannan Kuppusamy
1. Introduction 442
2. Why Image Free Radicals in the Heart? ZZI . 443
3. Instrumentation for EPR Spectroscopy and Imaging of the
Heart 444
CONTENTS xxv
4. Measurement of Nitroxide Radicals in the Normally Perftised
and Ischemic Heart 447
5. EPR Oximetry in the Perfused Heart 453
6. Three Dimensional Spectral Spatial EPR Imaging of the Heart... 455
7. Four Dimensional Spectral Spatial EPR Imaging of the Heart 457
8. Three Dimensional Spatial Imaging of the Heart 459
9. Gated EPR Imaging of the Beating Heart 461
10. Imaging of Nitric Oxide in the Heart 464
11. Conclusions 466
12. References 466
Chapter 17
Applications of in Vivo EPR Spectroscopy and Imaging in Cancer
Research
Howard J. Halpern
1. Problems in Cancer Research 469
2. Conclusions 480
3. Acknowledgments 480
4. References 480
Chapter 18
Applications of in Vivo EPR Spectroscopy and Imaging to Skin
Jiirgen Fuchs, Norbert Groth, and Thomas Herrling
1. Introduction 483
2. Skin Morphology and Practical Implications for EPR Studies 484
3. Diseases of the Skin and Cutaneous Manifestations of Systemic
Diseases 493
4. Instrumental Aspects of Human Skin in Vivo EPR 496
5. Conclusions 505
6. References 505
Chapter 19
Pharmaceutical Applications of in Vivo EPR
Karsten Mdder and Bernard Gallez
1. Pharmaceutical Technology and Drug Delivery Systems 516
2. Metabolism of Xenobiotics and Drugs 525
3. Pharmacokinetics of Paramagnetic Compounds 527
xxvi CONTENTS
4. Pharmacodynamics Characterisation of Drugs 530
5. Conclusions and Perspectives 539
6. References 539
Chapter 20
Proton Electron Double Resonance Imaging (PEDRI)
David J. Lurie
1. Introduction 547
2. PEDRI Techniques and Pulse Sequences 555
3. Hardware for PEDRI and Related Techniques 561
4. Sensitivity Considerations 570
5. Biological Applications of PEDRI, FC PEDRI, and FC DNP 574
6. Conclusions 575
7. Acknowledgments .. 576
8. References 577
Chapter 21
Combining NMR and EPR/ESR for in Vivo Experiments
JeffF. Dunn and Harold M. Swartz
1. Introduction 579
2. Illustrative Combined Uses of NMR and EPR 584
3. Conclusions 594
4. Acknowledgments 595
5. References 595
Chapter 22
Potential Medical (Clinical) Applications of EPR: Overview and
Perspectives
Harold M. Swartz
1. Rationale for Development of Clinical Applications of in Vivo
EPR 600
2. Current Status of Clinical Uses of in Vivo EPR 601
3. Challenges and Feasible Solutions for the Implementation of in
Vivo EPR in the Clinical Setting 611
4. Suggested Strategy for the Initial Clinical Applications of in
Vivo EPR 618
5. Summary and Conclusions 619
CONTENTS xxvii
6. Acknowledgments 620
7. References 620
Glossary 623
Contents of Previous Volumes 627
Index 649
i
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| spelling | In vivo EPR (ESR) theory and application ed. by Lawrence J. Berliner New York [u.a.] Kluwer Academic / Plenum Publ. 2003 XXVII, 656 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Biological magnetic resonance 18 Electron Spin Resonance Spectroscopy Electron paramagnetic resonance spectroscopy Elektronenspinresonanz (DE-588)4132116-9 gnd rswk-swf Elektronenspinresonanz (DE-588)4132116-9 s DE-604 Berliner, Lawrence J. Sonstige oth Biological magnetic resonance 18 (DE-604)BV017940024 18 HBZ Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=010467230&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | In vivo EPR (ESR) theory and application Biological magnetic resonance Electron Spin Resonance Spectroscopy Electron paramagnetic resonance spectroscopy Elektronenspinresonanz (DE-588)4132116-9 gnd |
| subject_GND | (DE-588)4132116-9 |
| title | In vivo EPR (ESR) theory and application |
| title_auth | In vivo EPR (ESR) theory and application |
| title_exact_search | In vivo EPR (ESR) theory and application |
| title_full | In vivo EPR (ESR) theory and application ed. by Lawrence J. Berliner |
| title_fullStr | In vivo EPR (ESR) theory and application ed. by Lawrence J. Berliner |
| title_full_unstemmed | In vivo EPR (ESR) theory and application ed. by Lawrence J. Berliner |
| title_short | In vivo EPR (ESR) |
| title_sort | in vivo epr esr theory and application |
| title_sub | theory and application |
| topic | Electron Spin Resonance Spectroscopy Electron paramagnetic resonance spectroscopy Elektronenspinresonanz (DE-588)4132116-9 gnd |
| topic_facet | Electron Spin Resonance Spectroscopy Electron paramagnetic resonance spectroscopy Elektronenspinresonanz |
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