Synthesis, functionalization and surface treatment of nanoparticles:
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| Format: | Book |
|---|---|
| Language: | English |
| Published: |
Stevenson Ranch, Calif.
American Scientific Publ.
2003
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| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Physical Description: | XVII, 302 S. Ill., graph. Darst. |
| ISBN: | 1588830098 |
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| 245 | 1 | 0 | |a Synthesis, functionalization and surface treatment of nanoparticles |c ed. by Marie-Isabelle Baraton |
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| adam_text | Titel: Synthesis, functionalization and surface treatment of nanoparticles
Autor: Baraton, Marie-Isabelle
Jahr: 2003
Contents
List of Contributors......................................................................................xv
About the Editor..........................................................................................xix
Chapter 1. NANOPARTICLES FROM
MECHANICAL ATTRITION
Claudio L. De Castro, Brian S. Mitchell
1. Introduction............................................................................................1
2. Historical Perspective................................................................................2
3. Principles of Milling ................................................................................2
4. Attrition Devices ....................................................................................4
4.1. SPEX Shaker Mills..........................................................................4
4.2. Planetary Ball Mills........................................................................5
4.3. Attritor Mills .........................................................................5
4.4. Comparison of Mills........................................................................6
5. Milled Materials......................................................................................6
5.1. Solid-State Amorphization................................................................7
5.2. Metals, Alloys, and Intermetallics......................................................7
5.3. Ceramics......................................................................................9
5.4. Composites....................................................................................10
5.5. Polymers......................................................................................11
6. Contamination........................................................................................13
7. Characterization of Nanoparticles................................................................13
8. Summary and Conclusions........................................................................14
References ............................................................................................14
Chapter 2. ELECTROCHEMICAL SYNTHESIS OF
METALLIC NANOPOWDERS
Jean-Luc Delplancke
1. Introduction............................................................................................17
2. Electrocrystallization................................................................................18
3. Powder Electrodeposition..........................................................................19
3.1. Copper Powder Production ..............................................................19
3.2. Copper Alloy Powder Production ......................................................20
3.3. Silver and Silver Alloy Powder Production............................................20
3.4. Lead and Lead Alloy Powder Production............................................20
3.5. Nickel and Nickel Alloy Powder Production..........................................21
3.6. Cobalt Powder Production................................................................21
3.7. Iron and Iron Alloy Powder Production..............................................21
3.8. Other Powder Productions................................................................22
3.9. Conclusion..........................................................22
4. The Electropulse Technique....................................................................22
4.1. Introduction..................................................................................22
4.2. The Electropulse Technique ..........................................................23
4.3. Metallic Nanopowders ....................................................................24
4.4. Metal Alloy Nanopowders................................................................25
4.5. Semiconductor Nanopowders............................................................25
4.6. Oxide and Polymer Nanopowders......................................................25
4.7. Other Research Groups....................................................................26
5. Conclusion ............................................................................................26
Acknowledgments....................................................................................26
References ............................................................................................26
ix
X
CONTENTS
Chapter 3. SOL-GEL-DERIVED OXIDE AND SULFIDE
NANOPARTICLES
S. Shukla, S. Seal
1. Introduction..........................................
2. Semiconductor Quantum Dots.................• o u •........
2.1. Properties, Industrial Applications, and Problems in Synthesis.........
3. Nanocrystalline Ceramics.....................................
3.1. Industrial Applications..................................
3.2. Problems in the Synthesis of Nanocrystalline Oxide Powder..........
4. Sol-Gel Synthesis of Oxide Nanoparticles...........................
4.1. The Sol-Gel Process....................................
4.2. Growth Mechanism and the Particle Shape.....................
4.3. Colloidal Stability of Oxide Nanoparticle Sol....................
5. Selection of a Polymer as a Surfactant.............................
6. Adsorption Characteristics of the HPC Polymer and Their Effects...........
7. Microemulsion Technology....................................
8. Synthesis of Sulfide Nanoparticles with Sol-Gel and Gas Diffusion Techniques . . .
9. General Comments.........................................
Acknowledgments..........................................
References ..............................................
Chapter 4. TEMPLATING NANOSTRUCTURE
THROUGH THE SELF-ASSEMBLY OF
SURFACTANTS
Blake Simmons, Limin Liu, Vijay John, Chad Taylor,
Daniel Schwartz, Gary McPherson, Arijit Bose, Vivek Agarwal
1. Introduction..............................................
2. Synthesis of Cadmium Sulfide Nanoparticles.........................
3. Self-Assembled Organogels....................................
4. Synthesis of Organogel/Nanoparticle Composites......................
5. Conclusions..............................................
Acknowledgments..........................................
References ..............................................
Chapter 5. SYNTHESIS AND ASSEMBLY OF
FUNCTIONALIZED GOLD NANOPARTICLES
Marvin G. Warner, James E. Hutchison
1. Introduction..............................................
1.1. Fundamental Studies and Technological Applications of
Functionalized Metal Nanoparticles .........................
1.2. Challenges Faced in Functionalized Nanoparticle Synthesis...........
2. Synthesis of Functionalized Gold Nanoparticles.......................
2.1. Overview of Synthetic Approaches to Functionalized Nanoparticles.....
2.2. Direct Synthesis of Functionalized, Ligand-Stabilized Gold
Nanoparticles.................................
2.3. Ligand Exchange Methods for Synthesis of Functionalized,
Ligand-Stabilized Gold Nanoparticles.......................
2.4. Postsynthetic Modification of the Exterior of a Ligand Shell
Possessing an w-Functionality .............................
3. Chemical Approaches to Extended Nanoparticle Structures:
Functional Group-Directed Organization...............
3.1. Nanoparticle-to-Nanoparticle Binding.................... . .
3.2. Nanoparticle-to-Surface Binding................
3.3. Nanoparticle-to-Template Binding...............
4. Conclusions and Future Directions..............
Acknowledgments...................
References ....................................
31
33
33
34
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36
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40
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60
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87
87
CONTENTS xi
Chapter 6. ORGANIC FUNCTIONALIZATION OF
METAL OXIDE NANOPARTICLES
Guido Kickelbick, Ulrich Schubert
1. Introduction.............................................. 91
2. Modification of Metal Oxide Clusters and Particles
by Functional Organic Ligands................................. 92
2.1. Postsynthesis Modification................................ 92
2.2. Functionalization of Clusters and Particles
during Their Synthesis { In situ Functionalization )............... 94
3. Inorganic-Organic Nanocomposites .............................. 98
3.1. Grafting To Approach................................. 98
3.2. Grafting From Approach............................... 98
Acknowledgments..........................................101
References ..............................................101
Chapter 7. POLYMER METAL
NANOCLUSTER COMPOSITES
Horacio Rotstein, Rina Tannenbaum
1. Introduction..............................................103
2. Mechanism and Kinetics of Metal Cluster Formation...................107
2.1. Formation of Zero-Valent Cobalt Clusters......................108
2.2. Formation of Metal Oxide Clusters..........................110
3. Control of Particle Size Via Polymer Adsorption......................112
3.1. Effect of the Viscous Medium on Aggregation Mechanism...........112
3.2. Particle Size Distribution in a Polymer Containing Nanocomposite......115
4. Modeling of Cluster-Polymer Nanocomposite Formation.................117
4.1. Description of the Models................................117
4.2. Description of the Coefficients of Coagulation and Fragmentation......118
4.3. The Coagulation Process with Metal Cluster-Polymer Interactions......119
4.4. Solutions of the Coagulation-Fragmentation Equations.............120
5. Experimental Procedure......................................122
5.1. Preparation of Polystyrene Solutions.........................122
5.2. Decomposition of Cobalt Carbonyl Solutions....................122
5.3. Infrared Spectroscopic Measurements ........................123
5.4. Transmission Electron Microscopy...........................123
6. Summary................................................123
Acknowledgments..........................................123
References ..............................................124
Chapter 8. FUNCTIONALIZED Ti02
NANOPARTICLES FOR PIGMENTS,
PHOTOELECTROCHEMISTRY, AND
SOLID STATE CHEMICAL SENSORS
P. Knauth, R. Bouchet, O. Schaf, A. Weibel, G. Auer
1. Introduction..............................................127
2. Production and Characterization of Ti02 Powders.....................129
2.1. Industrial Process......................................129
2.2. Synthesis Process for Nanocrystalline Particles...................130
2.3. Characterization of Ti02 Nanoparticles .......................131
2.4. Surface Segregation in Si- and Al-Doped Ti02...................131
3. Preparation and Application of Nanocrystalline Ti02 Films...............133
3.1. Photoelectrochemical Cells ...............................133
3.2. Thin- and Thick-Film Gas Sensors...........................133
4. Ionic Conductor Composites with Nanocrystalline Ti02 .................134
4.1. Models............................................134
4.2. Polymer Composites....................................136
4.3. Ceramic Composites....................................137
xii
CONTENTS
...............138
5. Nanocrystalline Ti02 Ceramics ....................
5.1. Fabrication by Hot-Pressing...............................14l
5.2. Theoretical Analysis of Impedance Spectra.....................
6. Conclusion ............................................................................145
Acknowledgments..........................................................................^
References .........................................
Chapter 9. SURFACE MODIFICATION OF Ti02:
A ROUTE FOR EFFICIENT
SEMICONDUCTOR ASSISTED
PHOTOCATALYSIS
Tijana Rajh, Olga V Makarova, Marion C. Thurnauer, Donald Cropek
147
1. Introduction..............................................
2. Colloidal Semiconductors.....................................
2.1. Optical Properties of Semiconductors.........................148
2.2. Quantization Effect .................................... 4^
2.3. Space Charge Layer and Band Bending.......................150
2.4. Energy Band Structure of Ti02............................. 50
3. Basic Mechanisms of Semiconductor-Assisted Photocatalysis ..............151
3.1. Photogeneration of Charge Pairs and Intrinsic Properties of
Semiconductors...................................... 151
3.2. Charge Pair Separation and Charge Carrier Trapping ..............152
3.3. Charge Carrier Recombination and Interfacial Electron Transfer.......153
3.4. Nature of Trapping Sites.................................154
3.5. Adsorption..........................................156
4. Surface Modification: Route for Efficient Photodegradation...............156
4.1. Surface Modification for Selective Removal of Organic Pollutants......157
4.2. Surface Modification for Removal of Heavy Metals................162
4.3. Surface Modification for Nanolithographic Applications.............167
4.4. Surface Modification for Improved Optical Properties..............168
Acknowledgments..........................................170
References ..............................................170
Chapter 10. SILICON NANOPARTICLES: NEXT
GENERATION OF ULTRASENSITIVE
FLUORESCENT MARKERS
Munir H. Nayfeh, Elena V Rogozhina, Lubos Mitas
1. Introduction..............................................174
2. Synthesis of Silicon Nanoparticles................................175
2.1. Synthesis Techniques ...................................176
2.2. Synthesis of Uniform Ultrasmall Ultrabright
Silicon Nanoparticles...................................179
2.3. Magic Discrete Sizes....................................181
2.4. Delivery of Particles/Deposition ............................183
3. Functionalization of Hydrogenated Silicon Surfaces....................185
3.1. Hydrogenated and Halogenated Silicon .......................186
3.2. Si-Si Bond Cleavage on Hydrogenated Silicon Surfaces.............186
3.3. Replacement of Hydrogen in Si-H Bonds......................188
3.4. Modified Si Surfaces Containing Functional Groups...............195
3.5. Conclusion.........................
4. Functionalization of Silicon Nanoparticles........................................19g
4.1. Modification of H-Terminated Particles.................... 198
4.2. Direct Synthesis/Functionalization........................ 206
4.3. Conclusion.......................................................208
5. Optical Properties of Nanoparticles...................!!!!!!......208
5.1. Luminescence Models................................................209
5.2. Stimulated Emission and Gain..........................................211
5.3. Emission, Excitation, and Time Dynamics Measurements............212
5.4. Brightness/Detection of Single Particles/Photostability . 213
CONTENTS
xiii
5.5. Assays and Sensor Films/Nonlinear Response ...................214
5.6. Effect of Functionalization on the Optical Properties...............216
6. Nanosystems: New Challenge for Theory
and Computational Methods..................................219
6.1. Density Functional Approaches for the Electronic
and Atomic Structures..................................220
6.2. Quantum Monte Carlo..................................221
6.3. Computer Time: Scaling with Particle Size .....................222
6.4. Applications to Si Clusters................................222
6.5. Structure of Si-Si Bonds.................................227
Acknowledgments..........................................228
References ..............................................228
Chapter 11. SURFACE-ENGINEERED NANOPARTICLES
AS DRUG CARRIERS
Ruxandra Gref
1. Introduction..............................................234
2. Factors Influencing the Fate of Intravenously Administered Particles.........234
3. The Role of MPS in Removing Injected Particles......................235
4. Impairing the Phagocytic Capacity of MPS..........................235
5. Nanoparticle Interaction with Blood..............................235
5.1. Opsonins...........................................235
5.2. Dysopsonins.........................................236
6. Modeling the Interaction between Proteins and PEG-Grafted Surfaces........236
6.1. PEG: An Outstanding Polymer.............................236
6.2. Protein-Rejecting Abilities of PEG Brushes ...................237
6.3. The Role of Polymer Flexibility.............................237
6.4. Single-Chain Mean-Field Theory............................238
6.5. PEG Interaction with Proteins.............................238
7. Approaches to the Design of Long-Circulating Carriers with PEG Coatings .... 239
7.1. Coatings Obtained by Polymer Adsorption .....................239
7.2. PEG Grafting on the Particles Surface........................239
8. Detection and Study of PEG Coating on Nanoparticles..................240
8.1. Direct Techniques....................................240
8.2. Reduction of Protein Adsorption............................241
8.3. Interaction with Complement..............................241
8.4. Competitive Interaction with Plasma Proteins: 2D-PAGE............242
8.5. Interaction with Phagocytic Cells............................244
9. Biodistribution............................................244
10. Encapsulation ............................................245
10.1. Encapsulation of Lipophilic Drugs..........................245
10.2. Encapsulation of Macromolecules in Stealth
Nanoparticles: A Challenge..............................249
11. PEG Block Copolymers: Various Applications........................250
12. Other Polymers for the Steric Protection of Nanoparticles................251
13. Targeting................................................252
14. Conclusions and Perspectives...................................253
References ..............................................253
Chapter 12. CHARACTERIZATION OF SURFACE
STRUCTURE AND INTERACTION BETWEEN
PARTICLES
Hidehiro Kamiya, Makio Naito
1. Introduction..............................................258
2. Characterization for Molecular Level and Nanometer Scaled Microstructure
at the Solid/Liquid Interface and Surface Interaction between Particles.......258
2.1. Characterization of Surface Molecular Structure on Fine and
Nanosized Particles....................................258
xiv
CONTENTS
2.2. Interaction between Solid Surfaces in Liquid Phase................258
2.3. Characterization of Surface Interaction
between Particulate Solid Surfaces..........................261
2.4. Characterization of Aggregation and Dispersion Behavior
of Fine Powder in Aqueous Suspension.......................262
3. Surface Molecular and Nanosized Structure and Surface Interaction
of Silica—Influence of Particle Diameter on Surface Hydroxyl Group
and Hydration Force of Alkoxide-Derived Silica Particle................ 262
3.1. Aggregation and Dispersion Behavior of Alkoxide-Derived Silica.......262
3.2. Measurement of Surface Interaction and Molecular Structure
of Silica Particles with Different Diameters.....................264
3.3. Analysis of the Effect of Diameter on Surface Structure and Interaction . . 265
4. Surface Interaction and Dense Alumina Suspension Behavior Controlled
by the Adsorption of Polymer Dispersant on Powder Surface ............. 266
4.1. Effect of Molecular Structure of Polymer Dispersant on Surface
Interaction and Dense Alumina Suspension Behavior..............266
4.2. Effect of pH on Suspension Behavior with Anionic Polymer Dispersant. . . 269
4.3. Effect of Additive Polymer Dispersant Content on Alumina
Suspension Behavior and Surface Interaction...................270
4.4. Effect of Counterion Density and Solid Fraction
on Alumina Suspension Behavior...........................272
5. Surface Interaction and Suspension Behavior of Silicon Nitride
and Carbide Controlled by the Addition of Polymer Dispersant............ 275
5.1. Silicon Carbide Suspension Behavior and Analysis................276
5.2. Silicon Nitride Suspension Behavior and Analysis.................277
Acknowledgments..........................................278
References ..............................................278
Chapter 13. DIELECTRIC PROPERTIES OF
NANOPARTICLES
S. Berger
1. Introduction................................................................................279
2. Linear Dielectrics..............................................................................280
2.1. Homogeneous Materials............................................................280
2.2. Heterogeneous Materials............................................................281
3. Nonlinear Dielectrics....................................................284
3.1. Homogeneous Materials................................................284
3.2. Heterogeneous Materials............................................289
References .......................................~nc
Index
299
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| id | DE-604.BV017195697 |
| illustrated | Illustrated |
| indexdate | 2024-07-09T19:14:51Z |
| institution | BVB |
| isbn | 1588830098 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-010362877 |
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| owner_facet | DE-355 DE-BY-UBR DE-91 DE-BY-TUM DE-11 |
| physical | XVII, 302 S. Ill., graph. Darst. |
| publishDate | 2003 |
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| publishDateSort | 2003 |
| publisher | American Scientific Publ. |
| record_format | marc |
| spelling | Synthesis, functionalization and surface treatment of nanoparticles ed. by Marie-Isabelle Baraton Stevenson Ranch, Calif. American Scientific Publ. 2003 XVII, 302 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Oberflächenbehandlung (DE-588)4042908-8 gnd rswk-swf Synthese (DE-588)4418958-8 gnd rswk-swf Anwendung (DE-588)4196864-5 gnd rswk-swf Nanopartikel (DE-588)4333369-2 gnd rswk-swf Nanopartikel (DE-588)4333369-2 s Synthese (DE-588)4418958-8 s Oberflächenbehandlung (DE-588)4042908-8 s Anwendung (DE-588)4196864-5 s DE-604 Baraton, Marie-Isabelle Sonstige oth HBZ Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=010362877&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Synthesis, functionalization and surface treatment of nanoparticles Oberflächenbehandlung (DE-588)4042908-8 gnd Synthese (DE-588)4418958-8 gnd Anwendung (DE-588)4196864-5 gnd Nanopartikel (DE-588)4333369-2 gnd |
| subject_GND | (DE-588)4042908-8 (DE-588)4418958-8 (DE-588)4196864-5 (DE-588)4333369-2 |
| title | Synthesis, functionalization and surface treatment of nanoparticles |
| title_auth | Synthesis, functionalization and surface treatment of nanoparticles |
| title_exact_search | Synthesis, functionalization and surface treatment of nanoparticles |
| title_full | Synthesis, functionalization and surface treatment of nanoparticles ed. by Marie-Isabelle Baraton |
| title_fullStr | Synthesis, functionalization and surface treatment of nanoparticles ed. by Marie-Isabelle Baraton |
| title_full_unstemmed | Synthesis, functionalization and surface treatment of nanoparticles ed. by Marie-Isabelle Baraton |
| title_short | Synthesis, functionalization and surface treatment of nanoparticles |
| title_sort | synthesis functionalization and surface treatment of nanoparticles |
| topic | Oberflächenbehandlung (DE-588)4042908-8 gnd Synthese (DE-588)4418958-8 gnd Anwendung (DE-588)4196864-5 gnd Nanopartikel (DE-588)4333369-2 gnd |
| topic_facet | Oberflächenbehandlung Synthese Anwendung Nanopartikel |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=010362877&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT baratonmarieisabelle synthesisfunctionalizationandsurfacetreatmentofnanoparticles |