Differential scanning calorimetry:
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| Main Authors: | , , |
|---|---|
| Format: | Book |
| Language: | English |
| Published: |
Berlin [u.a.]
Springer
2003
|
| Edition: | 2., rev. and enl. ed. |
| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Physical Description: | XII, 298 S. graph. Darst. |
| ISBN: | 354000467X 9783540004677 |
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MARC
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| 245 | 1 | 0 | |a Differential scanning calorimetry |c G. W. H. Höhne ; W. Hemminger ; H.-J. Flammersheim |
| 250 | |a 2., rev. and enl. ed. | ||
| 264 | 1 | |a Berlin [u.a.] |b Springer |c 2003 | |
| 300 | |a XII, 298 S. |b graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 650 | 4 | |a Differential scanning calorimetry | |
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| 700 | 1 | |a Hemminger, Wolfgang |d 1941- |e Verfasser |0 (DE-588)123656249 |4 aut | |
| 700 | 1 | |a Flammersheim, Hans-Jürgen |e Verfasser |4 aut | |
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Record in the Search Index
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|---|---|
| adam_text |
G.W.H. HOHNE * W.E HEMMINGER H.-J. FLAMMERSHEIM DIFFERENTIAL SCANNING
CALORIMETRY 2ND REVISED AND ENLARGED EDITION WITH 130 FIGURES AND 19
TABLES SPRINGER CONTENTS 1 INTRODUCTION 1 2 TYPES OF DIFFERENTIAL
SCANNING CALORIMETERS AND MODES OF OPERATION 9 2.1 HEAT FLUX DSC ,10
2.1.1 HEAT FLUX DSC WITH DISK-TYPE MEASURING SYSTEM 10 2.1.2 HEAT FLUX
DSC WITH TURRET-TYPE MEASURING SYSTEM 13 2.1.3 HEAT FLUX DSC WITH
CYLINDER-TYPE MEASURING SYSTEM 14 2.2 POWER COMPENSATION DSC 17 2.2.1
FUNCTION PRINCIPLE 17 2.2.2 SPECIAL POWER COMPENSATING DSC 22 2.3 DSC
WITH COMBINED HEAT FLUX AND POWER COMPENSATION MEASURING SYSTEM 25 2.4
MODES OF OPERATION 25 2.4.1 CONSTANT HEATING RATE 26 2.4.2 VARIABLE
HEATING RATE (MODULATED TEMPERATURE) 27 3 THEORETICAL FUNDAMENTALS OF
DIFFERENTIAL SCANNING CALORIMETERS . . 31 3.1 HEAT FLUX DSC 31 3.2 POWER
COMPENSATION DSC 48 3.3 TEMPERATURE-MODULATED DSC (TMDSC) 50 3.3.1 THE
TEMPERATURE-MODULATED METHOD 51 3.3.2 INFLUENCES OF THE SAMPLE 52 3.3.3
INFLUENCES OF HEAT TRANSPORT 57 3.3.4 CONCLUSIONS 63 4 CALIBRATION OF
DIFFERENTIAL SCANNING CALORIMETERS 65 4.1 ASPECTS OF QUALITY ASSURANCE '
66 4.2 BASIC ASPECTS OF CALIBRATION 66 4.3 TEMPERATURE CALIBRATION 69
4.3.1 TEMPERATURE CALIBRATION ON HEATING 69 4.3.2 TEMPERATURE
CALIBRATION ON COOLING 84 4.4 CALORIC CALIBRATION 86 4.4.1 HEAT FLOW
RATE CALIBRATION 87 4.4.2 HEAT (PEAK AREA) CALIBRATION 90 4.4.3 EXAMPLES
OF CALORIC CALIBRATION 92 4.4.4 CALORIC CALIBRATION IN COOLING MODE 97
VIII CONTENTS 4.5 CONCLUSIONS REGARDING THE CALIBRATION OF DSCS 97 4.6
REFERENCE MATERIALS FOR DSC CALIBRATION 98 4.6.1 REFERENCE MATERIALS FOR
TEMPERATURE CALIBRATION 99 4.6.2 REFERENCE MATERIALS FOR HEAT FLOW RATE
CALIBRATION 101 4.6.3 REFERENCE MATERIALS FOR HEAT (PEAK AREA)
CALIBRATION 107 4.7 ADDITIONAL CALIBRATION IN TEMPERATURE-MODULATED MODE
OF OPERATION 107 4.7.1 CALIBRATION OF MAGNITUDE 113 4.7.2 CALIBRATION OF
PHASE 113 5 DSC CURVES AND FURTHER EVALUATION 115 5.1 CHARACTERISTIC
TERMS OF DSC CURVES 116 5.2 PARAMETERS INFLUENCING THE DSC CURVE 118 5.3
FURTHER EVALUATION OF DSC CURVES 119 5.3.1 DETERMINATION OF THE REAL
SAMPLE HEAT FLOW RATE 119 5.3.2 THE BASELINE AND THE DETERMINATION OF
PEAK AREAS (ENTHALPY DIFFERENCES) 121 5.4 DESMEARING OF THE DSC CURVE
126 5.4.1 CORRECTION OF THE TEMPERATURE AND HEAT FLOW RATE INDICATED
. 128 5.4.2 SUBTRACTION OF THE ZEROLINE 129 5.4.3 CALCULATION OF THE
TRUE HEAT FLOW RATE INTO THE SAMPLE 129 5.4.4 ADVANCED DESMEARING 133
5.4.5 FURTHER CALCULATIONS 140 5.5 TMDSC CURVES 140 5.5.1 REVERSING AND
NON-REVERSING HEAT CAPACITY 141 5.5.2 COMPLEX HEAT CAPACITY 143 5.5.3
CURVES FROM STEP-SCAN EVALUATION 145 5.6 INTERPRETATION AND PRESENTATION
OF RESULTS 145 6 APPLICATIONS OF DIFFERENTIAL SCANNING CALORIMETRY 147
6.1 MEASUREMENT OF THE HEAT CAPACITY 147 6.1.1 "CLASSICAL" THREE-STEP
PROCEDURE 148 6.1.2 THE "ABSOLUTE" DUAL STEP METHOD 153 6.1.3 GENERAL
PRECAUTIONS FOR THE MINIMIZATION OF ERRORS AND THEIR ESTIMATION 154
6.1.4 PROCEDURE OF SMALL TEMPERATURE STEPS 155 6.1.5 THE
TEMPERATURE-MODULATED METHOD 159 6.1.6 TYPICAL APPLICATIONS OF HEAT
CAPACITY MEASUREMENTS 160 6.2 DETERMINATION OF HEATS OF REACTION 162 6.3
KINETIC INVESTIGATIONS 168 6.3.1 INTRODUCTION AND DEFINITIONS 168 6.3.2
EXPERIMENTAL PREREQUISITES FOR A RELIABLE KINETIC ANALYSIS 173 6.3.3
SELECTION OF THE MEASURING CONDITIONS - ISOTHERMAL OR NON-ISOTHERMAL
REACTION MODE 175 6.3.4 ACTIVATION OF THE SAMPLE BY UV IRRADIATION 180
6.3.5 DIFFERENT STRATEGIES OF KINETIC EVALUATION 183 6.3.6 SELECTED
EXAMPLES AND POSSIBLE PREDICTIONS 189 CONTENTS IX 6.4 THE GLASS
TRANSITION PROCESS 200 6.4.1 THE PHENOMENOLOGY OF THE GLASS TRANSITION
200 6.4.2 THE NATURE OF THE GLASS TRANSITION AND CONSEQUENCES FOR DSC
MEASUREMENTS 201 6.4.3 DEFINITION AND DETERMINATION OF THE GLASS
TRANSITION TEMPERATURE T G 203 6.4.4 APPLICATIONS OF GLASS TRANSITION
MEASUREMENTS 212 6.4.5 THE DYNAMIC GLASS PROCESS, AN EXAMPLE 217 6.5
CHARACTERIZATION OF SUBSTANCES, THE PHASE BEHAVIOR 219 6.5.1
APPLICATIONS IN BIOLOGY AND FOOD SCIENCE 219 6.5.2 APPLICATIONS IN
PHARMACY 221 6.5.3 OTHER APPLICATIONS 224 6.5.4 POROSITY MEASUREMENTS
228 6.6 DETERMINATION OF PHASE DIAGRAMS 230 6.7 SAFETY ASPECTS AND
CHARACTERIZATION OF HIGH-ENERGETIC MATERIALS . . 232 6.8
CHARACTERIZATION OF POLYMERS 233 6.8.1 EFFECTS OF ORIGIN AND THERMAL
HISTORY 234 6.8.2 DETERMINATION OF THE DEGREE OF CRYSTALLINITY 236 6.8.3
ADVANCED CHARACTERIZATION WITH THE TMDSC METHOD 238 6.9 PURITY
DETERMINATION OF CHEMICALS 241 7 EVALUATION OF THE PERFORMANCE OF A
DIFFERENTIAL SCANNING CALORIMETER 245 7.1 CHARACTERIZATION OF THE
COMPLETE INSTRUMENT 245 7.2 CHARACTERIZATION OF THE MEASURING SYSTEM 245
7.3 CHARACTERIZATION OF THE RESULTS OF A MEASUREMENT: UNCERTAINTY
DETERMINATION 251 7.3.1 BLACK BOX METHOD 253 7.3.2 GUM METHOD 253 7.4
CHECK LIST FOR DSCS 257 APPENDIX 1 259 APPENDIX 2 263 REFERENCES 281
SUBJECT INDEX 291 |
| any_adam_object | 1 |
| author | Höhne, Günther 1937- Hemminger, Wolfgang 1941- Flammersheim, Hans-Jürgen |
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| dewey-full | 536.6 |
| dewey-hundreds | 500 - Natural sciences and mathematics |
| dewey-ones | 536 - Heat |
| dewey-raw | 536.6 |
| dewey-search | 536.6 |
| dewey-sort | 3536.6 |
| dewey-tens | 530 - Physics |
| discipline | Chemie / Pharmazie Physik Chemie |
| edition | 2., rev. and enl. ed. |
| format | Book |
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| id | DE-604.BV017109909 |
| illustrated | Illustrated |
| indexdate | 2024-07-20T08:36:11Z |
| institution | BVB |
| isbn | 354000467X 9783540004677 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-010317164 |
| oclc_num | 249262951 |
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| physical | XII, 298 S. graph. Darst. |
| publishDate | 2003 |
| publishDateSearch | 2003 |
| publishDateSort | 2003 |
| publisher | Springer |
| record_format | marc |
| spelling | Höhne, Günther 1937- Verfasser (DE-588)118000330 aut Differential scanning calorimetry G. W. H. Höhne ; W. Hemminger ; H.-J. Flammersheim 2., rev. and enl. ed. Berlin [u.a.] Springer 2003 XII, 298 S. graph. Darst. txt rdacontent n rdamedia nc rdacarrier Differential scanning calorimetry Differential scanning calorimetry (DE-588)4320176-3 gnd rswk-swf Differential scanning calorimetry (DE-588)4320176-3 s DE-604 Hemminger, Wolfgang 1941- Verfasser (DE-588)123656249 aut Flammersheim, Hans-Jürgen Verfasser aut HEBIS Datenaustausch Darmstadt application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=010317164&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Höhne, Günther 1937- Hemminger, Wolfgang 1941- Flammersheim, Hans-Jürgen Differential scanning calorimetry Differential scanning calorimetry Differential scanning calorimetry (DE-588)4320176-3 gnd |
| subject_GND | (DE-588)4320176-3 |
| title | Differential scanning calorimetry |
| title_auth | Differential scanning calorimetry |
| title_exact_search | Differential scanning calorimetry |
| title_full | Differential scanning calorimetry G. W. H. Höhne ; W. Hemminger ; H.-J. Flammersheim |
| title_fullStr | Differential scanning calorimetry G. W. H. Höhne ; W. Hemminger ; H.-J. Flammersheim |
| title_full_unstemmed | Differential scanning calorimetry G. W. H. Höhne ; W. Hemminger ; H.-J. Flammersheim |
| title_short | Differential scanning calorimetry |
| title_sort | differential scanning calorimetry |
| topic | Differential scanning calorimetry Differential scanning calorimetry (DE-588)4320176-3 gnd |
| topic_facet | Differential scanning calorimetry |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=010317164&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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