Reactive distillation: status and future directions
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| Format: | Book |
|---|---|
| Language: | English |
| Published: |
Weinheim
Wiley-VCH
2003
|
| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Item Description: | Literaturangaben |
| Physical Description: | XX, 287 S. Ill., graph. Darst. : 25 cm |
| ISBN: | 3527305793 |
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MARC
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| 245 | 1 | 0 | |a Reactive distillation |b status and future directions |c Kai Sundmacher ... (eds.) |
| 264 | 1 | |a Weinheim |b Wiley-VCH |c 2003 | |
| 300 | |a XX, 287 S. |b Ill., graph. Darst. : 25 cm | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 500 | |a Literaturangaben | ||
| 650 | 7 | |a Destilação (congressos) |2 larpcal | |
| 650 | 4 | |a Distillation - Appareils et matériel - Conception et construction | |
| 650 | 4 | |a Distillation - Congrès | |
| 650 | 4 | |a Réactivité (Chimie) - Applications industrielles - Congrès | |
| 650 | 4 | |a Distillation apparatus |x Design and construction |v Congresses | |
| 650 | 4 | |a Distillation |v Congresses | |
| 650 | 4 | |a Reactivity (Chemistry) |x Industrial applications |v Congresses | |
| 650 | 0 | 7 | |a Reaktivdestillation |0 (DE-588)4491776-4 |2 gnd |9 rswk-swf |
| 655 | 7 | |0 (DE-588)1071861417 |a Konferenzschrift |2 gnd-content | |
| 689 | 0 | 0 | |a Reaktivdestillation |0 (DE-588)4491776-4 |D s |
| 689 | 0 | |5 DE-604 | |
| 700 | 1 | |a Sundmacher, Kai |d 1965- |e Sonstige |0 (DE-588)115051252 |4 oth | |
| 856 | 4 | 2 | |m DNB Datenaustausch |q application/pdf |u http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=010211803&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |3 Inhaltsverzeichnis |
| 943 | 1 | |a oai:aleph.bib-bvb.de:BVB01-010211803 | |
Record in the Search Index
| _version_ | 1808226150354255872 |
|---|---|
| adam_text |
CONTENTS
PREFACE
XI
LIST
OF
CONTRIBUTORS
XIX
PART
I
INDUSTRIAL
APPLICATIONS
1
INDUSTRIAL
APPLICATIONS
OF
REACTIVE
DISTILLATION
3
1.1
INTRODUCTION
3
1.2
ETHERIFICATION:
MTBE,
ETBE,
AND
TAME
14
1.3
DIMERIZATION,
OLIGOMERIZATION,
AND
CONDENSATION
15
1.4
ESTERIFICATION:
METHYL
ACETATE
AND
OTHER
ESTERS
16
1.5
HYDROLYSIS
OF
ESTERS
18
1.6
HYDRATION
20
1.7
HYDROGENATION/HYDRODESULFURIZATION/HYDROCRACKING
20
1.7.1
BENZENE
TO
CYCLOHEXANE
21
1.7.2
SELECTIVE
HYDROGENATION
OF
C
4
STREAM
21
1.7.3
HYDROGENATION
OF
PENTADIENE
21
1.7.4
C
4
ACETYLENE
CONVERSION
22
1.7.5
HYDRODESULFURIZATION,
HYDRODENITROGENATION,
AND
HYDROCRACKING
22
1.7.6
MISCELLANEOUS
HYDROGENATIONS
22
1.8
CHLORINATION
23
1.9
ACETALIZATION/KETALIZATION
23
1.10
RECOVERY
AND
PURIFICATION
OF
CHEMICALS
24
1.11
DIFFICULT
SEPARATIONS
25
1.12
CHEMICAL
HEAT
PUMPS
26
1.13
RD
WITH
SUPERCRITICAL
FLUIDS
26
1.14
CONCLUSIONS
26
2
REACTIVE
DISTILLATION
PROCESS
DEVELOPMENT
IN
THE
CHEMICAL
PROCESS
INDUSTRIES
30
2.1
INTRODUCTION
30
2.2
PROCESS
SYNTHESIS
32
2.3
PROCESS
DESIGN
AND
OPTIMIZATION
35
VI
CONTENTS
2.4
LIMITATIONS
OF
THE
METHODS
FOR
SYNTHESIS
AND
DESIGN:
THE
SCALE-UP
PROBLEM
37
2.5
2.6
2.7
2.8
2.9
CHOICE
OF
EQUIPMENT
38
SOME
REMARKS
ON
THE
ROLE
OF
CATALYSIS
46
CONCLUSIONS
46
ACKNOWLEDGMENTS
47
NOTATION
47
3
3.1
3.2
3.2.1
3.2.2
3.2.3
3.3
3.3.1
3.3.2
3.3.2.1
3.3.2.2
3.3.2.3
3.3.3
3.3.4
3.4
APPLICATION
OF
REACTIVE
DISTILLATION
AND
STRATEGIES
IN
PROCESS
DESIGN
49
INTRODUCTION
49
CHALLENGES
IN
PROCESS
DESIGN
FOR
REACTIVE
DISTILLATION
51
FEASIBILITY
ANALYSIS
51
CATALYST
AND
HARDWARE
SELECTION
51
COLUMN
SCALE-UP
51
MTBE
DECOMPOSITION
VIA
REACTIVE
DISTILLATION
52
CONCEPTUAL
DESIGN
52
MODEL
DEVELOPMENT
54
CATALYST
SELECTION
AND
REACTION
KINETICS
55
PHASE
EQUILIBRIUM
MODEL
55
STEADY-STATE
SIMULATION
56
LAB-SCALE
EXPERIMENTS
57
PILOT-PLANT
EXPERIMENTS
58
CONCLUSIONS
61
PART
II
4
4.1
4.2
4.2.1
4.2.2
4.3
4.4
4.4.1
4.4.2
4.4.2.1
4.4.2.2
4.4.2.3
4.4.2.4
4.4.2.5
PHYSICOCHEMICAL
FUNDAMENTALS
THERMODYNAMICS
OF
REACTIVE
SEPARATIONS
65
INTRODUCTION
65
PROCESS
MODELS
FOR
REACTIVE
DISTILLATION
66
OUTLINE
66
CASE
STUDY:
METHYL
ACETATE
66
EQUILIBRIUM
THERMODYNAMICS
OF
REACTING
MULTIPHASE
MIXTURES
70
FLUID
PROPERTY
MODELS
FOR
REACTIVE
DISTILLATION
74
OUTLINE
74
EXAMPLES
75
HEXYL
ACETATE:
SENSITIVITY
ANALYSIS
75
METHYL
ACETATE:
PREDICTION
OF
POLYNARY
VAPOR-LIQUID
EQUILIBRIA
77
BUTYL
ACETATE:
THERMODYNAMIC
CONSISTENCY
81
ETHYL
ACETATE:
CONSEQUENCES
OF
INCONSISTENCY
82
FORMALDEHYDE
+
WATER
+
METHANOL:
INTRINSICALLY
REACTIVE
COMPLEX
MIXTURE
83
4.5
4.5.1
4.5.2
4.5.2.1
4.5.2.2
EXPERIMENTAL
STUDIES
OF
PHASE
EQUILIBRIA
IN
REACTING
SYSTEMS
88
OUTLINE
88
REACTIVE
VAPOR-LIQUID
EQUILIBRIA
90
BATCH
EXPERIMENTS
90
FLOW
EXPERIMENTS
91
CONTENTS
I
VII
4.5.23
RECIRCULATION
EXPERIMENTS
92
4.6
CONCLUSIONS
92
4.7
ACKNOWLEDGMENTS
93
4.8
NOTATION
93
5
IMPORTANCE
OF
REACTION
KINETICS
FOR
CATALYTIC
DISTILLATION
PROCESSES
97
5.1
INTRODUCTION
97
5.2
REACTIVE
IDEAL
BINARY
MIXTURES
98
5.2.1
REACTION-DISTILLATION
PROCESS
WITH
EXTERNAL
RECYCLING
100
5.2.1.1
(O,O)-ANALYSIS
101
5.2.1.2
(OO,
N
MLN
)-ANALYSIS
102
5.2.2
DISTILLATION
COLUMN
WITH
REACTIVE
REBOILER
103
5.2.3
FULLY
REACTIVE
DISTILLATION
COLUMN
106
5.3
KINETIC
EFFECTS
ON
ATTAINABLE
PRODUCTS
109
5.3.1
SINGULAR
POINT
ANALYSIS
110
5.3.2
IDEAL
TERNARY
MIXTURES
112
5.3.2.1
CASE
A:
A
AC
=
0.2,
A
BC
=
3.0
112
53.2.2
CASE
B:
A
AC
=
5.0,
A
BC
=
3.0
112
5.3.3
NON-IDEAL
MIXTURES
115
5.33.1
SYNTHESIS
OF
MTBE
115
5.33.2
SYNTHESIS
OF
TAME
117
5.3.4
SYSTEMS
WITH
LIQUID-PHASE
SPLITTING
121
5.3.5
SYSTEMS
WITH
INTERFACIAL
MASS-TRANSFER
RESISTANCES
126
5.4
DETERMINATION
AND
ANALYSIS
OF
REACTION
KINETICS
129
5.4.1
PHYSICOCHEMICAL
TRANSPORT
PHENOMENA
129
5.4.2
PROCESS
EVALUATION
BY
DIMENSIONLESS
NUMBERS
131
5.4.3
FORMULATION
OF
REACTION
RATE
EXPRESSIONS
133
5.4.4
IMPORTANCE
OF
TRANSPORT
RESISTANCES
FOR
COLUMN
OPERATION
135
5.5
CONCLUSIONS
138
5.6
ACKNOWLEDGMENTS
139
5.7
NOTATION
140
PART
III
PROCESS
DESIGN
6
FEASIBILITY
AND
PROCESS
ALTERNATIVES
FOR
REACTIVE
DISTILLATION
145
6.1
INTRODUCTION
145
6.2
MOTIVATION
147
6.3
FLASH
CASCADE
MODEL
153
6.4
FEASIBILITY
HYPOTHESIS
156
6.5
BIFURCATION
ANALYSIS
OF
THE
FLASH
CASCADE
MODEL
160
6.6
CONCLUSIONS
165
6.7
NOTATION
165
VIII
I
CONTENTS
7
HARDWARE
SELECTION
AND
DESIGN
ASPECTS
FOR
REACTIVE
DISTILLATION
COLUMNS
169
7.1
7.2
7.2.1
7.3
7.3.1
7.3.2
7.4
7.5
7.6
INTRODUCTION
169
HARDWARE
FOR
HOMOGENEOUS
REACTIVE
DISTILLATION
169
CASE
STUDY
FOR
METHYL
ACETATE
PRODUCTION
173
HARDWARE
FOR
HETEROGENEOUS
REACTIVE
DISTILLATION
177
DIFFERENT
HARDWARE
CONFIGURATIONS
177
HARDWARE
SELECTION
ASPECTS
183
THE
SIDE-REACTOR
CONCEPT
185
CONCLUSIONS
187
ACKNOWLEDGMENTS
188
8
DEVELOPMENT
OF
UNSTRUCTURED
CATALYTIC
PACKING
FOR
REACTIVE
DISTILLATION
PROCESSES
190
8.1
8.2
8.3
8.3.1
8.3.2
8.3.2.1
8.3.2.2
8.4
8.4.1
8.4.2
8.5
8.6
8.6.1
8.6.2
8.6.3
8.6.4
8.6.5
8.7
INTRODUCTION
190
REQUIREMENTS
FOR
RD
CATALYTIC
PACKING
190
STATE
OF
THE
ART:
CATALYTIC
PACKING
FOR
RD
PROCESSES
191
COMMERCIAL
PACKING
191
ALTERNATIVE
CONCEPTS
193
CATALYSTS
MADE
OF
PURE
CATALYTIC
MATERIAL
193
CATALYSTS
SUPPORTED
ON
CARRIER
MATERIALS
194
NEW
CATALYST
CONCEPT:
POROUS
POLYMER/CARRIER
COMPOSITE
195
REQUIREMENTS
FOR
THE
CARRIER
MATERIALS
198
REQUIREMENTS
FOR
THE
POLYMERIZATION
PROCESS
199
PREPARATION
OF
SULFONATED
ION-EXCHANGE
POLYMER/CARRIER
CATALYSTS
200
PERFORMANCE
OF
POLYMER/CARRIER
CATALYSTS
203
INFLUENCE
OF
POLYMER
CONTENT
AND
REACTANT
CONCENTRATION
204
INFLUENCE
OF
REACTION
TEMPERATURE
205
INFLUENCE
OF
CROSS-LINKING
207
INFLUENCE
OF
CROSS-LINKING
AT
LOW
POLYMER
CONTENT
207
INFLUENCE
OF
CROSS-LINKING
AT
HIGH
POLYMER
CONTENT
209
OUTLOOK:
EXTENSION
TO
OTHER
SYNTHETIC
PROCESSES
WITH
INTEGRATED
SEPARATION
210
8.7.1
8.7.2
8.7.3
8.8
REACTIVE
STRIPPING
210
REACTIVE
CHROMATOGRAPHY
211
POLYMER-ASSISTED
SOLUTION-PHASE
ORGANIC
SYNTHESIS
212
CONCLUSIONS
212
PART
IV
9
MODELING
AND
PROCESS
CONTROL
MODELING
OF
HOMOGENEOUS
AND
HETEROGENEOUS
REACTIVE
DISTILLATION
PROCESSES
217
9.1
9.2
9.3
9.3.1
INTRODUCTION
217
EQUILIBRIUM
STAGE
MODELS
217
NON-EQUILIBRIUM
STAGE
MODELING
220
THE
CONVENTIONAL
NEQ
MODEL
220
CONTENTS
IX
9.3.2
NEQ
MODELING
OF
REACTIVE
DISTILLATION
223
9.3.3
HOMOGENEOUS
SYSTEMS
223
9.3.4
HETEROGENEOUS
SYSTEMS
225
9.3.5
NEQ
CELL
MODEL
227
9.3.6
PROPERTIES,
HYDRODYNAMICS,
AND
MASS
TRANSFER
232
9.4
COMPARISON
OF
EQ
AND
NEQ
MODELS
232
9.5
A
VIEW
OF
REACTIVE
DISTILLATION
PROCESS
DESIGN
237
9.6
NOTATION
238
10
NONLINEAR
DYNAMICS
AND
CONTROL
OF
REACTIVE
DISTILLATION
PROCESSES
241
10.1
INTRODUCTION
241
10.2
MULTIPLICITY
AND
OSCILLATIONS
IN
CHEMICAL
PROCESS
SYSTEMS
242
10.3
METHYL
FORMATE
SYNTHESIS
245
10.3.1
SINGULARITY
ANALYSIS
OF
A
ONE-STAGE
COLUMN
246
10.3.2
OO/OO-ANALYSIS
OF
LAB-SCALE
COLUMN
247
10.3.3
CONTINUATION
ANALYSIS
OF
LAB-SCALE
COLUMN
248
10.4
ETHYLENE
GLYCOL
SYNTHESIS
249
10.4.1
SINGULARITY
ANALYSIS
OF
A
ONE-STAGE
COLUMN
250
10.4.2
CONTINUATION
ANALYSIS
OF
INDUSTRIAL
SIZE
DISTILLATION
COLUMN
251
10.5
MTBE
AND
TAME
SYNTHESIS
257
10.5.1
MTBE
SYNTHESIS
257
10.5.2
TAME
SYNTHESIS
258
10.5.3
KINETIC
INSTABILITIES
FOR
FINITE
TRANSPORT
INSIDE
THE
CATALYST
260
10.5.4
OSCILLATORY
BEHAVIOR
261
10.6
CLASSIFICATION
262
10.7
NONLINEAR
WAVE
PROPAGATION
264
10.8
CONTROL
271
10.8.1
CONTROL
STRUCTURE
SELECTION
271
10.8.2
CONTROL
ALGORITHMS
274
10.9
CONCLUSIONS
276
10.10
ACKNOWLEDGMENTS
278
INDEX
283 |
| any_adam_object | 1 |
| author_GND | (DE-588)115051252 |
| building | Verbundindex |
| bvnumber | BV016524420 |
| callnumber-first | T - Technology |
| callnumber-label | TP156 |
| callnumber-raw | TP156.D5 |
| callnumber-search | TP156.D5 |
| callnumber-sort | TP 3156 D5 |
| callnumber-subject | TP - Chemical Technology |
| classification_rvk | VN 7220 |
| classification_tum | CIT 340f CIT 215f |
| ctrlnum | (OCoLC)50527475 (DE-599)BVBBV016524420 |
| dewey-full | 660/.28425 |
| dewey-hundreds | 600 - Technology (Applied sciences) |
| dewey-ones | 660 - Chemical engineering |
| dewey-raw | 660/.28425 |
| dewey-search | 660/.28425 |
| dewey-sort | 3660 528425 |
| dewey-tens | 660 - Chemical engineering |
| discipline | Chemie / Pharmazie Chemie-Ingenieurwesen |
| format | Book |
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| genre | (DE-588)1071861417 Konferenzschrift gnd-content |
| genre_facet | Konferenzschrift |
| id | DE-604.BV016524420 |
| illustrated | Illustrated |
| indexdate | 2024-08-24T00:20:35Z |
| institution | BVB |
| isbn | 3527305793 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-010211803 |
| oclc_num | 50527475 |
| open_access_boolean | |
| owner | DE-91G DE-BY-TUM DE-1046 DE-29T DE-83 |
| owner_facet | DE-91G DE-BY-TUM DE-1046 DE-29T DE-83 |
| physical | XX, 287 S. Ill., graph. Darst. : 25 cm |
| publishDate | 2003 |
| publishDateSearch | 2003 |
| publishDateSort | 2003 |
| publisher | Wiley-VCH |
| record_format | marc |
| spelling | Reactive distillation status and future directions Kai Sundmacher ... (eds.) Weinheim Wiley-VCH 2003 XX, 287 S. Ill., graph. Darst. : 25 cm txt rdacontent n rdamedia nc rdacarrier Literaturangaben Destilação (congressos) larpcal Distillation - Appareils et matériel - Conception et construction Distillation - Congrès Réactivité (Chimie) - Applications industrielles - Congrès Distillation apparatus Design and construction Congresses Distillation Congresses Reactivity (Chemistry) Industrial applications Congresses Reaktivdestillation (DE-588)4491776-4 gnd rswk-swf (DE-588)1071861417 Konferenzschrift gnd-content Reaktivdestillation (DE-588)4491776-4 s DE-604 Sundmacher, Kai 1965- Sonstige (DE-588)115051252 oth DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=010211803&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Reactive distillation status and future directions Destilação (congressos) larpcal Distillation - Appareils et matériel - Conception et construction Distillation - Congrès Réactivité (Chimie) - Applications industrielles - Congrès Distillation apparatus Design and construction Congresses Distillation Congresses Reactivity (Chemistry) Industrial applications Congresses Reaktivdestillation (DE-588)4491776-4 gnd |
| subject_GND | (DE-588)4491776-4 (DE-588)1071861417 |
| title | Reactive distillation status and future directions |
| title_auth | Reactive distillation status and future directions |
| title_exact_search | Reactive distillation status and future directions |
| title_full | Reactive distillation status and future directions Kai Sundmacher ... (eds.) |
| title_fullStr | Reactive distillation status and future directions Kai Sundmacher ... (eds.) |
| title_full_unstemmed | Reactive distillation status and future directions Kai Sundmacher ... (eds.) |
| title_short | Reactive distillation |
| title_sort | reactive distillation status and future directions |
| title_sub | status and future directions |
| topic | Destilação (congressos) larpcal Distillation - Appareils et matériel - Conception et construction Distillation - Congrès Réactivité (Chimie) - Applications industrielles - Congrès Distillation apparatus Design and construction Congresses Distillation Congresses Reactivity (Chemistry) Industrial applications Congresses Reaktivdestillation (DE-588)4491776-4 gnd |
| topic_facet | Destilação (congressos) Distillation - Appareils et matériel - Conception et construction Distillation - Congrès Réactivité (Chimie) - Applications industrielles - Congrès Distillation apparatus Design and construction Congresses Distillation Congresses Reactivity (Chemistry) Industrial applications Congresses Reaktivdestillation Konferenzschrift |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=010211803&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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