The essence of chromatography:
Saved in:
| Main Author: | |
|---|---|
| Format: | Book |
| Language: | English |
| Published: |
Amsterdam [u.a.]
Elsevier
2003
|
| Edition: | 1. ed. |
| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Physical Description: | IX, 925 S. Ill., graph. Darst. |
| ISBN: | 0444501983 0444501991 |
Staff View
MARC
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| 100 | 1 | |a Poole, Colin F. |e Verfasser |4 aut | |
| 245 | 1 | 0 | |a The essence of chromatography |c Colin F. Poole |
| 250 | |a 1. ed. | ||
| 264 | 1 | |a Amsterdam [u.a.] |b Elsevier |c 2003 | |
| 300 | |a IX, 925 S. |b Ill., graph. Darst. | ||
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Record in the Search Index
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| adam_text | Contents
Preface ix
Chapter 1. General Concepts in Column Chromatography 1
1.1. Introduction 2
1.2. Family Tree of Chromatographie Methods 2
1.3. Zone Migration 6
1.4. Retention 8
1.5. Band Broadening 24
1.6. Resolution 51
1.7. Separation Time 59
1.8. Principles of Quantification 62
1.9. References 72
Chapter 2. The Column in Gas Chromatography 79
2.1. Introduction 80
2.2. Mobile Phases 83
2.3. Stationary Phases 86
2.4. Retention in Gas-Liquid Chromatography 120
2.5. Preparation and Evaluation of Open Tubular Columns 142
2.6. Preparation and Evaluation ofPacked Columns 156
2.7. References 162
Chapter 3. Instrumental Aspects of Gas Chromatography 171
3.1. Introduction 172
3.2. Pneumatic Systems 172
3.3. Thermal Zones 176
3.4. Sample Handling Devices 177
3.5. Sample Inlets 180
3.6. Supercritical Fluid Inlets 203
VI The Essence of Chromatography
3.7. Vapor Sample Inlets 204
3.8. Coupled-Column Gas Chromatography 216
3.9. Column Connectors and Flow Splitters 224
3.10. Detectors 225
3.11. References 257
Chapter 4. The Column in Liquid Chromatography 267
4.1. Introduction 269
4.2. Column Packing Materials 270
4.3. Retention Mechanisms 300
4.4. Method Development 362
4.5. Column Preparation 393
4.6. References 413
Chapter 5. Instrumental Aspects of Liquid Chromatography 431
5.1. Introduction 432
5.2. Solvent Delivery Systems 434
5.3. Sample Inlets 441
5.4. Guard and Scavenger Columns 449
5.5. Column Temperature Control 449
5.6. Coupled-Column Systems 451
5.7. Detectors 455
5.8. Postcolumn Reaction Systems 487
5.9. Indirect Detection 490
5.10. References 491
Chapter 6. Thin-Layer Chromatography 499
6.1. Introduction 500
6.2. Attributes of Layers and Columns 501
6.3. Theoretical Considerations 504
6.4. Stationary Phases 520
6.5. Sample Application 527
6.6. Multimodal (Coupled Column-Layer) Systems 529
6.7. Development Techniques 531
6.8. Method Development 541
6.9. Detection 552
6.10. References 562
Chapter 7. Supercritical Fluid Chromatography 569
7.1. Introduction 570
7.2. Mobile Phases 573
Contents VÜ
7.3. Stationary Phases 580
7.4. Kinetic Optimization 582
7.5. Retention 587
7.6. Instrumental Aspects 596
7.7. Related Techniques 608
7.8. References 611
Chapter 8. Capillary-Electromigration Separation Techniques 619
8.1. Introduction 620
8.2. Capillary Electrophoresis 623
8.3. Micellar Electrokinetic Chromatography 644
8.4. Capillary Electrochromatography 659
8.5. Capillary Gel Electrophoresis 668
8.6. Capillary Isoelectric Focusing 671
8.7. Capillary Isotachophoresis 673
8.8. Method Development 676
8.9. Instrumental Aspects 684
8.10. References 706
Chapter 9. Spectroscopic Detectors for Identification and Quantification . 719
9.1. Introduction 720
9.2. Mass Spectrometry 721
9.3. Fourier Transform Infrared Spectrometry 767
9.4. Nuclear Magnetic Resonance Spectroscopy 779
9.5. References 785
Chapter 10. Separation of Stereoisomers 793
10.1. Introduction 794
10.2. Enantioselectivity and Absolute Configuration 797
10.3. Separation of Enantiomers 800
10.4. Chiral Stationary Phases 802
10.5. Chiral Mobile Phase Additives 821
10.6. Complexation Chromatography 830
10.7. Separation of Enantiomers as Covalent Diastereomer Derivatives 834
10.8. Liquid-Crystalline Stationary Phases 837
10.9. References 839
Chapter 11. Laboratory-Scale Preparative Chromatography 847
11.1. Introduction 848
11.2. Thin-Layer Chromatography 848
11.3. Column Liquid Chromatography 850
Vlll The Essence of Chromatography
11.4. Supercritical Fluid Chromatography 884
11.5. Gas Chromatography 886
11.6. Countercurrent Chromatography 889
11.7. References 893
Subject Index 901
|
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| dewey-tens | 540 - Chemistry and allied sciences |
| discipline | Chemie / Pharmazie |
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| illustrated | Illustrated |
| indexdate | 2024-07-09T19:05:39Z |
| institution | BVB |
| isbn | 0444501983 0444501991 |
| language | English |
| lccn | 2002034692 |
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| spelling | Poole, Colin F. Verfasser aut The essence of chromatography Colin F. Poole 1. ed. Amsterdam [u.a.] Elsevier 2003 IX, 925 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Chromatographie Chromatographic analysis Chromatographie (DE-588)4010153-8 gnd rswk-swf (DE-588)4123623-3 Lehrbuch gnd-content Chromatographie (DE-588)4010153-8 s DE-604 HBZ Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=009985661&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Poole, Colin F. The essence of chromatography Chromatographie Chromatographic analysis Chromatographie (DE-588)4010153-8 gnd |
| subject_GND | (DE-588)4010153-8 (DE-588)4123623-3 |
| title | The essence of chromatography |
| title_auth | The essence of chromatography |
| title_exact_search | The essence of chromatography |
| title_full | The essence of chromatography Colin F. Poole |
| title_fullStr | The essence of chromatography Colin F. Poole |
| title_full_unstemmed | The essence of chromatography Colin F. Poole |
| title_short | The essence of chromatography |
| title_sort | the essence of chromatography |
| topic | Chromatographie Chromatographic analysis Chromatographie (DE-588)4010153-8 gnd |
| topic_facet | Chromatographie Chromatographic analysis Lehrbuch |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=009985661&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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