Residue analysis in food: principles and applications
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| Format: | Book |
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| Language: | English |
| Published: |
Amsterdam
Harwood
2000
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| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Physical Description: | XVIII, 306 S., 1 Bl. Ill. |
| ISBN: | 9057024411 |
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| 245 | 1 | 0 | |a Residue analysis in food |b principles and applications |c ed. by Michael O'Keefe |
| 264 | 1 | |a Amsterdam |b Harwood |c 2000 | |
| 300 | |a XVIII, 306 S., 1 Bl. |b Ill. | ||
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Record in the Search Index
| _version_ | 1804128172630867968 |
|---|---|
| adam_text | Titel: Residue analysis in food
Autor: O Keeffe, Michael
Jahr: 2000
Preface
Contributors
1 Introduction
Michael O Keeffe
1.1 Chemical Contamination of Food
1.2 Residue Analysis
1.3 Advances in Residue Analysis Methodologies
1.4 The Sample is the Key
1.5 Analytical Methods
1.6 Special Issues in Residue Analysis
1.7 Future
1.8 References
CONTENTS
xv
xvii
1
1
2
3
5
6
9
11
11
Primary Extraction Technologies 17
Marie-Louise Scippo and Guy Maghuin-Rogister
2.1 Introduction 17
2.1.1 Types of residues 17
18
18
2.2 Stages in the Analysis of Residues in Food 19
19
19
20
20
21
21
21
22
22
23
25
25
25
2.1.2 Justification for primary extraction
2.1.3 Difficulties in the analysis of residues
Stages in the Analysis of Residues in Food
2.2.1 Sampling
2.2.2 Transfer to the laboratory and storage
2.2.3 Thawing
2.2.4 Internal standard
2.2.5 Homogenisation
2.2.5.1 Milk
2.2.5.2 Eggs
2.2.5.3 Tissues
2.2.6 Enzyme/acid hydrolysis and digestion
2.2.7 (Primary) Extraction
2.2.8 Clean-up
2.2.8.1 Elimination of water
2.2.8.2 Elimination of fat
CONTENTS
2.2.8.3 Elimination of proteins 25
2.2.8.4 Elimination of co-extractives 26
2.2.9 Solvent removal 26
2.2.10 End point determination 26
2.3 Liquid-Liquid Partitioning 26
±3.1 Theory 26
2.3.1.1 Multiple extraction 27
2.3.1.2 Influence of pH 28
2.3.1.3 Influence of temperature 28
2.3.1.4 Ion-pairing 28
2.3.1.5 Salting-out 28
2.4 Recovery Estimation in Quantitative Analysis 29
2.5 Examples 29
2.5.1 Pesticides 29
2.5.2 P-Agonists 30
2.5.3 Steroid hormones 31
2.5.3.1 Androgens 32
2.5.3.2 Oestrogens 32
2.5.3.3 Progestagens 32
2.5.4 Antibiotics 32
2.5.4.1 Polyethers 32
2.5.4.2 Macrolides 33
2.5.4.3 Chloramphenicol 33
2.5.5 Mycotoxins 33
2.5.6 Further reading 33
2.6 References 34
Sorbent Technologies : Principles and Applications 37
Steven A. Barker
3.1 Introduction 37
3.2 Solid Phase Extraction 38
3.2.1 Adsorption mode 38
3.2.2 Size exclusion or permeation mode 39
3.2.3 Bonded phase partition mode 40
3.3 Sorbent Technologies: Columns, Cartridges and Discs 43
3.4 Solid Phase Microextraction 45
3.5 Matrix Solid Phase Dispersion 45
3.6 Characteristics of the MSPD Process 49
3.6.1 Unique sample interactions 49
3.6.2 The nature of the solid support and bonded phase 49
CONTENTS vii
3.6.3 Matrix modification 50
3.6.4 Solvent elution 51
3.6.5 The matrix effect 51
3.7 Applications 52
3.8 References 58
4 Automated Extraction/Clean-Up Technologies 73
Alida A.M. Stolker, Saskia S. Sterk and Leendert A. van Ginkel
4.1 Introduction 73
4.2 Automated Solid-Phase Extraction Techniques 74
4.2.1 Principle 74
4.2.2 Applications of automated solid-phase extraction techniques 76
4.3 Column Switching Techniques 77
4.3.1 Principle 77
4.3.2 Applications of column-switching techniques 78
4.3.2.1 Sample clean-up 78
4.3.2.2 Sample enrichment 83
4.4. Supercritical Fluid Extraction (SFE) 84
4.4.1 Principle 84
4.4.2 Applications of SFE 88
4.4.2.1 Introduction 88
4.4.2.2 SFE of residues of analytes from non-fatty matrices 89
4.4.2.3 SFE of residues of analytes from fatty matrices 92
4.4.2.4 SFE of residues of analytes from samples of fat 98
4.5 Conclusions 100
4.6 References 101
5 Immunochemical and Receptor Technologies 107
Willem Haasnoot and Robert Schilt
5.1 Introduction 107
5.2 Specific Reagents 108
5.2.1 Antibodies 108
5.2.1.1 Antibody-antigen interaction 109
5.2.1.2 Poly- or monoclonal, recombinant or anti-anti-idiotype 110
antibodies
5.2.1.3 Antibodies towards haptens 112
5.2.2 Receptors 112
5.2.2.1 Receptor binding 112
5.2.2.2 Hormonal receptors 113
5.2.2.3 Steroid hormone receptors 113
i CONTENTS
5.3 Assay Formats and Applications 114
5.3.1 Radioimmunoassay (RIA) 116
5.3.2 Receptor assays 117
5.3.2.1 Radio receptor assay (RRA) 117
5.3.2.2 Microbial receptor assay 118
5.3.2.3 Functional tests 119
5.3.3 Enzyme-linked immunosorbent assay (ELIS A) 119
5.3.4 Sol particle immunoassay (SPIA) 121
5.3.5 Enhanced enzyme immunoassays 123
5.3.5.1 Avidin-biotin systems 123
5.3.5.2 Chemiluminescence enzyme immunoassays (cEIA) 124
5.3.5.3 Electro-chemiluminescence immunoassays 125
5.3.6 Fluorescence immunoassays 125
5.3.6.1 Fluorescence polarisation immunoassay (FPIA) 126
5.3.6.2 Time-resolvedfluoroimmunoassay (TR-FIA) or dissociation 126
enhanced lanthanide fluoroimmunoassay (DELFIA)
5.3.6.3 Solid phase fluorescence immunoassay (SPFIA) 127
5.3.7 Biosensors 127
5.3.7.1 Biosensor applications 128
5.4 Sample Preparation and Screening Assays 129
5.5 Immunoaffinity Chromatography 132
5.5.1 IAC columns 133
5.5.1.1 Commercially available columns 133
5.5.1.2 Column preparation 134
5.5.1.3 Column characteristics 134
5.5.2 IAC procedures 134
5.5.3 IAC applications 135
5.5.3.1 Mycotoxins 135
5.5.3.2 Growth promoters 136
5.5.3.3 Veterinary drugs and other analytes 136
5.5.3.4 Pesticides and contaminants 137
5.6 References 137
High Performance Thin Layer Chromatography for Residue Analysis 145
Hubert F. De Brabander and Katia De Wasch
6.1 Introduction 145
6.2 The Four Steps of TLC 146
6.2.1 Application 146
6.2.2 Development 147
6.2.2.1 The stationary phase 148
6.2.2.2 The solvents 148
6.2.2.3 Automated multiple development (AMD) 149
CONTENTS
6.2.3 Detection
6.2.3.1 The visualisation
6.2.3.2 The documentation
6.2.4 Quantification
Some Special Features of TLC
6.3.1 Two-dimensional TLC
6.3.2 4x4 -TLC
6.3.3 Anti-diagonal development
6.3.4 Coupled layers
6.3.5 Reaction TLC
149
150
151
151
6.3 Some Special Features of TLC 153
153
154
155
156
157
6.3.5.1 Derivatisation at the application site 157
6.3.5.2 Other reactions at the application site 158
6.3.6 Some additional advantages of TLC 158
6.4 Quality Criteria for the Use of TLC in Residue Analysis 158
6.4.1 Introduction 158
6.4.2 Discussion of the quality criteria 159
6.5 Comparison of TLC with other Methods for Residue Analysis 161
6.6 Examples of TLC Methods in Residue Analysis 162
6.6.1 TLC methods for illegal growth promoters 162
6.6.1.1 Thyreostatic drugs 162
6.6.1.2 Anabolic steroids 163
6.6.1.3 Beta-agonists 164
6.6.1.4 Corticosteroids 165
6.6.2 TLC methods for anribacterials 164
6.6.2.1 Sulphonamides 165
6.6.2.2 Tetracyclines 165
6.6.2.3 Poly ether antibiotics 165
6.6.2.4 Macrolide antibiotics 166
6.6.3 TLC methods for other residues 166
6.7 Is There a Future for TLC in Residue Analysis? 166
6.7.1 Automation in TLC 167
6.7.2 Enhancing specificity in TLC 167
6.7.3 TLC/MS 168
6.7.3.1 DirectTLC/MS 168
6.7.3.2 TLC with additional hyphenated MS techniques 168
6.8 Conclusion 169
6.9 References 171
Gas Chromatography 77
Bruno Le Bizec, Marie-Pierre Montrade and Francois Andre
CONTENTS
7.1 Historical 177
7.2 Introduction 178
7.2.1 Definitions 178
7.2.2 Phenomena involved 178
7.2.3 Residue analysis 179
7.3 Carrier Gas 180
7.4 Injector 180
7.4.1 Split injector 180
7.4.2 Splitless injector 181
7.4.3 Cold on-column injector 181
7.4.4 De Ros injector 182
7.4.5 Headspace injector 182
7.4.6 Large volume injector 183
7.5 Columns 184
7.5.1 Three column types 184
7.5.1.1 Packed columns 184
7.5.1.2 Capillary columns 185
7.5.1.3 530 tan columns 185
7.5.2 Stationary phases 186
7.5.2.1 Glycol polyesters 186
7.5.2.2 Glycol polyethers 186
7.5.2.3 Silicones 187
7.5.2.4 Apolar branched hydrocarbons 187
7.5.3 Two dimensional gas chromatography 187
188
189
189
189
190
191
193
195
196
196
197
198
198
198
200
200
200
7.6 Oven
7.7 Detectors
7.7.1 Thermal conductivity detector (TCD)
7.7.2 Flame ionisation detector (FED)
7.7.3 Nitrogen phosphorus (thermionic) detector (NPD)
7.7.4 Electron capture detector (ECD)
7.7.5 Flame photometric detector (FPD)
7.7.6 Other detectors
7.7.7 Infrared detector
7.7.7.1 Infrared spectrometry
7.7.7.2 Coupling ofGC with the IR detector
7.7.8 Atomic detector
7.7.8.1 Atomic spectrometry
7.7.8.2 Coupling ofGC with the atomic (AAS) detector
7.7.9 Mass detector
7.7.9.1 Mass spectrometry
1.1.9.2 Ionisation processes
CONTENTS xi
7.7.9.2.1 Electron impact (El) mode 200
1.13.2.2 Chemical ionisation - positive mode 201
7.7.9.2.3 Chemical ionisation - negative mode 202
7.7.9.3 Mass detectors 204
7.7.9.3.1 Quadrupole 204
7.7.9.3.2 Ion trap 205
7.7.9.3.3 Double focusing spectrometers 207
7.7.9.4 Acquisition methods 208
7.7.9.4.1 SCAN mode 208
7.7.9.4.2 SIM (LR and HR) mode 208
7.7.9.4.3 SRMmode 209
7.8 Derivatisation 211
7.8.1 Principle and effects of derivatisation 211
7.8.1.1 Principle 211
7.8.1.2 Separation effects 211
7.8.1.3 Detection (ECD, NPD, FPD, MS) effects 211
7.8.2 Classical derivatisation reactions 212
7.8.2.1 Alkylation 212
7.8.2.2 Acylation 213
7.8.2.3 Silylation 214
7.8.2.4 Condensation 215
7.9 Conclusion 217
7.10 References 218
High Performance Liquid Chromatography 237
Sharon Porter and Raj Patel
8.1 Introduction 237
8.2 A Race to the Finish: The Chromatographic Process 237
8.2.1 The capacity factor (thermodynamic effects) 238
8.2.2 Efficiency and resolution 239
8.2.3 Band broadening (kinetic effects) 240
8.3 Simplifying the Mixture: Modes of Chromatography 241
8.3.1 Adsorption chromatography 241
8.3.2 Partition chromatography 242
8.3.3 Bonded phase chromatography 242
8.3.3.1 Support material 242
8.3.3.2 Normal phase chromatography 242
8.3.3.3 Reversed phase chromatography 243
8.3.4 Ionic species 243
8.3.4.1 Ion suppression 243
8.3.4.2 Ion pair chromatography 243
CONTENTS
8.3.4.3 Ion-exchange chromatography 244
8.3.5 Affinity chromatography 244
8.4 The Building Blocks: HPLC Instrumentation 244
8.4.1 Pumping systems 244
8.4.1.1 Reciprocating piston pump 244
8.4.1.2 Syringe pumps 245
8.4.1.3 Degassers 245
8.4.2 Sample introduction 245
8.4.2.1 Automated injectors 246
8.4.3 Tubing, in-line filters and guard columns 246
8.4.3.1 Tubing 246
8.4.3.2 In-line filters and guard columns 246
8.4.3.3 Scavenger columns 246
8.4.4 Chromatographic columns 247
8.4.4.1 Conventional columns 247
8.4.4.2 Narrow bore columns 247
8.4.4.3 Microbore columns 247
8.4.4.4 Column switching 247
8.4.4.5 Column ovens 247
8.4.5 Detectors 247
8.4.5.1 Ultraviolet and visible detectors 248
8.4.5.2 Photodiode array detectors 248
8.4.5.3 Fluorescence detectors 248
8.4.5.4 Electrochemical detectors 249
8.4.6 Mass spectrometry 249
8.4.6.1 Direct liquid introduction 250
8.4.6.2 Continuous flow fast atom bombardment (CF-FAB) 250
8.4.6.3 Moving belt interface (MBI) 250
8.4.6.4 Particle beam interface (PBI) 250
8.4.6.5 Thermospray 250
8.4.6.6 Electrospray (ESI) and atmospheric pressure chemical
ionisation (APCI) 251
8.4.6.7 Mass spectrometry/mass spectrometry 252
8.5 Making Analytes Detectable: Derivatisation 252
8.5.1 Pre-column derivatisation 252
8.5.2 Post-column derivatisation 252
8.6 Quantitative or Qualitative Methods? 253
8.6.1 Quantitative methods 253
8.6.2 Qualitative methods 254
8.6.2.1 Qualitative methods giving tentative identification 255
8.6.2.2 Qualitative methods giving increased confidence in the
identity 255
CONTENTS xiii
8.7 Applications of HPLC to Veterinary Drug Residues 255
8.7.1 Aminoglycosides 255
8.7.2 Anthelmintics 256
8.7.2.1 Avermectins 257
8.7.2.2 Benzimidazoles 257
8.7.2.3 Levamisole 258
8.7.3 P-Lactams 258
8.7.4 Chloramphenicol (CAP), florfenicol and thiamphenicol 259
8.7.5 Fluoroquinolone and quinolone antibiotics 259
8.7.6 Ionophores 260
8.7.7 Macrolides and related antibiotics 260
8.7.8 Nitrofurans 261
8.7.9 Nitroimidazoles 261
8.7.10 Sulphonamides 263
8.7.11 Tetracyclines 263
8.8 Applications of HPLC to Residues of Growth Promoters 265
8.8.1 P-Agonists 265
8.8.2 Anabolic steroids 265
8.9 The Future of HPLC in Residue Analysis 266
8.10 References 268
Regulatory Aspects of Residue Analysis 277
James D. MacNeil and Jack F. Kay
9.1 Introduction 277
9.2 Sample Requirements 278
9.3 Method Classification and General Performance Criteria 279
9.3.1 Screening methods 28°
9.3.2 Determinative methods 282
9.3.3 Confirmatory methods 282
9.4 Method Validation Requirements 283
9.5 Codex Requirements 284
9.5.1 Codex Committee on Methods of Analysis and Sampling (CCMAS) 284
9.5.2 Codex Committee on Residues of Veterinary Drugs in Food (CCRVDF) 285
9.5.3 Codex Committee on Pesticide Residues (CCPR) 286
9.6 United States of America Requirements 288
9.7 European Union Requirements 289
9.8 Quality Systems 290
9.8.1 Reference materials 292
9.8.2 Proficiency programs 2^2
9.9 Future Directions/Influences 293
9.10 References 296
Index 301
|
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| id | DE-604.BV013391257 |
| illustrated | Illustrated |
| indexdate | 2024-07-09T18:45:01Z |
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| isbn | 9057024411 |
| language | English |
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| publisher | Harwood |
| record_format | marc |
| spelling | Residue analysis in food principles and applications ed. by Michael O'Keefe Amsterdam Harwood 2000 XVIII, 306 S., 1 Bl. Ill. txt rdacontent n rdamedia nc rdacarrier Aliments - Analyse ram Aliments - Contamination - Mesure ram Aliments - Teneur en polluants ram Pesticide residues in food Veterinary drug residues Lebensmittel (DE-588)4034870-2 gnd rswk-swf Rückstandsanalyse (DE-588)4050855-9 gnd rswk-swf Lebensmittel (DE-588)4034870-2 s Rückstandsanalyse (DE-588)4050855-9 s DE-604 O'Keefe, Michael Sonstige oth HBZ Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=009134906&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Residue analysis in food principles and applications Aliments - Analyse ram Aliments - Contamination - Mesure ram Aliments - Teneur en polluants ram Pesticide residues in food Veterinary drug residues Lebensmittel (DE-588)4034870-2 gnd Rückstandsanalyse (DE-588)4050855-9 gnd |
| subject_GND | (DE-588)4034870-2 (DE-588)4050855-9 |
| title | Residue analysis in food principles and applications |
| title_auth | Residue analysis in food principles and applications |
| title_exact_search | Residue analysis in food principles and applications |
| title_full | Residue analysis in food principles and applications ed. by Michael O'Keefe |
| title_fullStr | Residue analysis in food principles and applications ed. by Michael O'Keefe |
| title_full_unstemmed | Residue analysis in food principles and applications ed. by Michael O'Keefe |
| title_short | Residue analysis in food |
| title_sort | residue analysis in food principles and applications |
| title_sub | principles and applications |
| topic | Aliments - Analyse ram Aliments - Contamination - Mesure ram Aliments - Teneur en polluants ram Pesticide residues in food Veterinary drug residues Lebensmittel (DE-588)4034870-2 gnd Rückstandsanalyse (DE-588)4050855-9 gnd |
| topic_facet | Aliments - Analyse Aliments - Contamination - Mesure Aliments - Teneur en polluants Pesticide residues in food Veterinary drug residues Lebensmittel Rückstandsanalyse |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=009134906&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT okeefemichael residueanalysisinfoodprinciplesandapplications |