Advanced chromatographic and electromigration methods in bioSciences:
Saved in:
| Format: | Book |
|---|---|
| Language: | English |
| Published: |
Amsterdam [u.a.]
Elsevier
1998
|
| Edition: | 1. ed. |
| Series: | Journal of chromatography library
60 |
| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Physical Description: | XVI, 1131 S. Ill., graph. Darst. |
| ISBN: | 0444825940 |
Staff View
MARC
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| 245 | 1 | 0 | |a Advanced chromatographic and electromigration methods in bioSciences |c ed. Zdeněk Deyl |
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| 264 | 1 | |a Amsterdam [u.a.] |b Elsevier |c 1998 | |
| 300 | |a XVI, 1131 S. |b Ill., graph. Darst. | ||
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Record in the Search Index
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| adam_text | Contents
Preface V
List of Contributors VII
Chapter 1 Selection of Chromatographic Methods for Biological Materials .... 1
Toshihiko Hanai
1.1 Introduction 2
1.2 Strategy for chromatographic process selection 2
1.3 Development of packing materials for liquid chromatography of biological
samples 6
1.4 Automated work out of biological samples in liquid chromatography 11
1.5 Drug protein binding assays using liquid chromatography 29
1.6 Quantitative structure retention relationships in reversed phase liquid
chromatography 38
1.7 Conclusions 43
1.8 Abbreviations 46
1.9 References 46
Chapter 2 Strategies for Electromigration Separations of Biological
Macromolecules 53
Hidetoshi Arakawa, Masako Maeda and Toshihiko Hanai
2.1 Introduction 54
2.2 Strategy for the application of electromigration techniques for biological
samples 54
2.3 Analysis of low molecular mass solutes by capillary electrophoresis and
related techniques 55
2.4 Analysis of biological macromolecules 73
2.5 Binding of low molecular mass solutes to proteins 87
2.6 Future of CE as a method for the separation of biological materials
constituents. Conclusions 89
2.7 Abbreviations 90
2.8 References 91
Chapter 3 Sample Preparation 95
Qing Yang, Andy J. Tomlinson and Stephen Nay lor
3.1 Introduction 96
3.2 Sample preparation techniques 97
3.3 Conclusions 135
3.4 Acknowledgements 135
XII Contents
3.5 Abbreviations 135
3.6 References 136
Chapter 4 Selected Derivatization Reactions 141
Zdenek Deyl, Ivan Miksik and Eva Tesafovd
4.1 Introduction 142
4.2 Derivatization approaches according to analyte class 143
4.3 Derivatization approaches according to the functional groups 143
4.4 Specific applications of derivatization techniques 166
4.5 Conclusions 171
4.6 References 179
Chapter 5 Enantioselective Separations 197
Eva Tesafovd and Daniel W. Armstrong
5.1 Introduction .197
5.2 Enantiomers 198
5.3 Chirality in nature and in life sciences 199
5.4 Chiral analysis in biosciences 200
5.5 Basic principles of chiral separation 200
5.6 Methods used for enantioseparation 204
5.7 Conclusion 246
5.8 Abbreviations 247
5.8 References .247
Chapter 6 Carbohydrates, Polymeric Sugars and their Constituents 257
M. Estrella Legaz, Mercedes M. Pedrosa and C. Vicente
6.1 Introduction 258
6.2 HPLC of carbohydrates 260
6.3 HPCE, electrolyte systems 269
6.4 HPCE of underivatized carbohydrates 273
6.5 HPCE of derivatized carbohydrates 284
6.6 HPCEofglycoconjugates 303
6.7 Acknowledgements 307
6.8 Abbreviations 307
6.9 References 308
Chapter 7 Carboxylic Acids 315
Zdenek Deyl and Ivan Miksik
7.1 Introduction 315
7.2 Gas chromatography 316
7.3 Derivatization for GC 316
7.4 Types of gas chromatography used 319
7.5 Detection and identification in GC 321
7.6 Liquid chromatography 323
7.7 Detection, and detection limits in LC 328
7.8 Emerging separation techniques and their application 331
7.9 Conclusions 335
Contents XIII
7.10 Abbreviations 335
7.11 References 336
Chapter 8 Herbal Organic Acids 343
S.Z. Yao, P. Chen,X.Y. Yang, Y.S. Fung and S.H. Si
8.1 Introduction 344
8.2 Carboxylic organic acids in medicinal plants 345
8.3 Sample pre treatment 351
8.4 Chromatographic determination of carboxylic acids in herbal medicines 357
8.5 Acknowledgments 368
8.6 References 368
Chapter 9 Analysis of Lipids by Thin Layer Chromatography 371
Nalur C. Shantha and Guillermo E. Napolitano
9.1 Introduction. Categorization of lipids 372
9.2 Analysis of lipids 374
9.3 Conclusions 398
9.4 Abbreviations 398
9.5 References 399
Chapter 10 Biogenic Amines 403
Zdenek Deyl and Ivan Miksik
10.1 Introduction 403
10.2 Sample preparation 404
10.3 Liquid column chromatography 404
10.4 Micellar electrokinetic chromatography 407
10.5 Detection 408
10.6 Abbreviations 412
10.7 References 412
Chapter 11 Amino Acids 415
Ibolya Molndr Perl
11.1 Introduction 416
11.2 High performance liquid chromatography 417
11.3 Ion exchange chromatography (IEC) 435
11.4 Capillary electrophoresis (CE) 436
11.5 Gas chromatography 444
11.7 Comparison of methods 456
11.8 Conclusion 457
11.9 Abbreviations 457
11.10 References 458
Chapter 12 Peptides 465
Zdenek Deyl and Ivan Miksik
12.1 Chromatography 466
Xjy Contents
12.2 Electromigration techniques *88
12.3 Peptide mapping ^(
12.4 Chiral recognition of peptides 11
12.5 Separation of peptide conformers 512
12.6 Detection 513
12.7 Acknowledgements 515
12.8 Abbreviations 515
12.9 References 516
Chapter 13 Protein Analysis 525
J, Fred Banks
13.1 Introduction 526
13.2 Liquid chromatography (LC) separation techniques 526
13.3 Capillary electrophoresis (CE) separation techniques 548
13.4 Mass spectrometry detection 561
13.5 Conclusions and future directions 566
13.6 Abbreviations 567
13.7 References 567
Chapter 14 Nucleic Acids and Their Constituents 575
Martin Gilar, David L. Smisek and Aharon S. Cohen
14.1 Introduction 576
14.2 Antisense and other modified oligonucleotidcs 578
14.3 Structural and chemical analysis 580
14.4 Relevant separation procedures 584
14.5 Conclusions 602
14.6 Abbreviations 603
14.6 References 603
Chapter 15 Compounds Containing Heterocyclic Nitrogen, Oxygen
and Sulfur 609
Ivan Miksik and Zdenek Deyl
15.1 Introduction 610
15.2 Compounds containing heterocyclic oxygen 611
15.3 Alkaloids 619
15.4 Compounds containing heterocyclic nitrogen 625
15.5 Compounds containing heterocyclic sulfur 641
15.6 References 642
Chapter 16 Vitamins 651
Anna Rizzolo and Stefano Polesello
16.1 Introduction (, $
16.2 Fat soluble vitamins (, p
16.3 Water soluble vitamins 677
16.4 Method validation and intercomparison studies 720
16.5 Abbreviations 723
16.6 References 725
Contents XV
Chapter 17 Antibiotics 737
Steven A. Barker
17.1 Introduction 737
17.2 Classes of antibiotics 739
17.3 Conclusions and future directions for the analysis of antibiotics 761
17.4 Abbreviations 771
17.5 References 771
Chapter 18 Pesticides in Environmental Samples 779
Katalin Fodor Csorba
18.1 Introduction 780
18.2 Analytical procedures for the determination of pesticides in the
environment 780
18.3 Analysis of pesticide residues in soil 786
18.4 Determination of pesticides residues in water samples 810
18.5 Pesticides in air 822
18.6 Pesticides, chemical names 824
18.7 Abbreviations 826
18.8 References 827
Chapter 19 Monitoring of Process Impurities in Drugs 833
Sajid Husain and R. Nageswara Rao
19.1 Introduction 834
19.2 Role of chromatographic techniques in the quality assurance of drugs and
Pharmaceuticals 838
19.3 RoleofCE in quality assurance of drugs and Pharmaceuticals 861
19.4 Conclusions 882
19.5 Acknowledgements 882
19.6 Abbreviations 882
19.7 References 883
Chapter 20 Procedures in Hospital Laboratories 889
Romolo M. Dorizzi
20.1 Introduction 889
20.2 Glycated haemoglobin 890
20.3 Variant haemoglobin 891
20.4 Drugs 893
20.5 Drugs of abuse 899
20.6 Vitamins 902
20.7 Catecholamines and metabolites 903
20.8 Hormones 905
20.9 Miscellanea 907
20.10 Abbreviations 913
20.11 References 914
XVI Contents
Chapter 21 Toxicological and Forensic Applications 917
Franco Tagliaro, Frederick P. Smith, Luciano Tedeschi, Franca
Castagna, Marina Dobosz, Ilaria Boschi and Vincenzo Pascali
21.1 Introduction 918
21.2 Forensic toxicology 919
21.3 Forensic DNA fingerprinting 931
21.4 Capillary electrophoresis, a new tool in forensic science 943
21.5 Criteria for acceptance of new science in court 950
21.6 Conclusions 954
21.7 Abbreviations 955
21.8 References 956
Chapter 22 Inorganic Analysis and Speciation 963
Andrei R. Timerbaev and Wolfgang Buchberger
22.1 Introduction 964
22.2 Sampling, sample storage, clean up, and pretreatment 965
22.3 High performance liquid chromatographic methods 968
22.4 Capillary electrotrophoretic methods 991
22.5 Conclusions 1007
22.6 Acknowledgements 1008
22.7 References 1008
Chapter 23 Common Pitfalls in CE and HPLC 1013
Michel Arellano and Francois Couderc
23.1 Introduction 1014
23.2 Capillary electrophoresis: capillary related pitfalls 1015
23.3 Selected pitfalls in high performance liquid chromatography 1027
23.4 Sample introduction pitfalls 1032
23.5 Temperature effects 1049
23.6 Peak shape and multiple peaks 1055
23.7 Background electrolytes and mobile phases 1070
23.8 Non aqueous media for CE 1079
23.9 Practical hints 1081
23.10 Conclusion 1084
23.11 Abbreviations 1085
23.12 References 1086
Index of Compounds Separated 1093
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| spelling | Advanced chromatographic and electromigration methods in bioSciences ed. Zdeněk Deyl 1. ed. Amsterdam [u.a.] Elsevier 1998 XVI, 1131 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Journal of chromatography library 60 Biomolécules - Analyse ram Biomolécules - Séparation ram Bioquimica larpcal Chromatographie ram Cromatografia em liquido larpcal Cromatografia larpcal Proteinas larpcal Électrophorèse ram Biowissenschaften Chromatographic analysis Chromatography methods Electrophoresis Electrophoresis methods Isoelectric Focusing methods Isoelectric focusing Life sciences Technique Chromatographie (DE-588)4010153-8 gnd rswk-swf Biomolekül (DE-588)4135124-1 gnd rswk-swf Elektromigration (DE-588)4296761-2 gnd rswk-swf (DE-588)4143413-4 Aufsatzsammlung gnd-content Chromatographie (DE-588)4010153-8 s Biomolekül (DE-588)4135124-1 s DE-604 Elektromigration (DE-588)4296761-2 s Deyl, Zdeněk Sonstige (DE-588)126288607 oth Journal of chromatography library 60 (DE-604)BV035916693 60 HBZ Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=009125504&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Advanced chromatographic and electromigration methods in bioSciences Journal of chromatography library Biomolécules - Analyse ram Biomolécules - Séparation ram Bioquimica larpcal Chromatographie ram Cromatografia em liquido larpcal Cromatografia larpcal Proteinas larpcal Électrophorèse ram Biowissenschaften Chromatographic analysis Chromatography methods Electrophoresis Electrophoresis methods Isoelectric Focusing methods Isoelectric focusing Life sciences Technique Chromatographie (DE-588)4010153-8 gnd Biomolekül (DE-588)4135124-1 gnd Elektromigration (DE-588)4296761-2 gnd |
| subject_GND | (DE-588)4010153-8 (DE-588)4135124-1 (DE-588)4296761-2 (DE-588)4143413-4 |
| title | Advanced chromatographic and electromigration methods in bioSciences |
| title_auth | Advanced chromatographic and electromigration methods in bioSciences |
| title_exact_search | Advanced chromatographic and electromigration methods in bioSciences |
| title_full | Advanced chromatographic and electromigration methods in bioSciences ed. Zdeněk Deyl |
| title_fullStr | Advanced chromatographic and electromigration methods in bioSciences ed. Zdeněk Deyl |
| title_full_unstemmed | Advanced chromatographic and electromigration methods in bioSciences ed. Zdeněk Deyl |
| title_short | Advanced chromatographic and electromigration methods in bioSciences |
| title_sort | advanced chromatographic and electromigration methods in biosciences |
| topic | Biomolécules - Analyse ram Biomolécules - Séparation ram Bioquimica larpcal Chromatographie ram Cromatografia em liquido larpcal Cromatografia larpcal Proteinas larpcal Électrophorèse ram Biowissenschaften Chromatographic analysis Chromatography methods Electrophoresis Electrophoresis methods Isoelectric Focusing methods Isoelectric focusing Life sciences Technique Chromatographie (DE-588)4010153-8 gnd Biomolekül (DE-588)4135124-1 gnd Elektromigration (DE-588)4296761-2 gnd |
| topic_facet | Biomolécules - Analyse Biomolécules - Séparation Bioquimica Chromatographie Cromatografia em liquido Cromatografia Proteinas Électrophorèse Biowissenschaften Chromatographic analysis Chromatography methods Electrophoresis Electrophoresis methods Isoelectric Focusing methods Isoelectric focusing Life sciences Technique Biomolekül Elektromigration Aufsatzsammlung |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=009125504&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| volume_link | (DE-604)BV035916693 |
| work_keys_str_mv | AT deylzdenek advancedchromatographicandelectromigrationmethodsinbiosciences |