Molybdenum disulphide lubrication:
Saved in:
| Main Author: | |
|---|---|
| Format: | Book |
| Language: | English |
| Published: |
Amsterdam [u.a.]
Elsevier
1999
|
| Edition: | 1. ed. |
| Series: | Tribology series
35 |
| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Physical Description: | XXVI, 380 S. Ill., graph. Darst. |
| ISBN: | 0444500324 |
Staff View
MARC
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| 245 | 1 | 0 | |a Molybdenum disulphide lubrication |c A. R. Lansdown |
| 250 | |a 1. ed. | ||
| 264 | 1 | |a Amsterdam [u.a.] |b Elsevier |c 1999 | |
| 300 | |a XXVI, 380 S. |b Ill., graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 490 | 1 | |a Tribology series |v 35 | |
| 650 | 4 | |a Molybdenum Disulphide | |
| 650 | 4 | |a Lubrication and lubricants | |
| 650 | 4 | |a Molybdenum disulphide | |
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Record in the Search Index
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| adam_text | XI
CONTENTS
Preface vii
Contents x
List of Figures xv
List of Tables xxi
Chapter 1 History 1
1 1 Early Beginnings 1
1 2 Recorded History 3
1 3 Range of Applications 7
Chapter 2 Occurrence and Extraction 11
2 1 Occurrence 11
2 2 Extraction of Molybdenum Disulphide 13
2 3 Extraction of Molybdenum 17
2 4 Synthesis of Molybdenum Disulphide 19
Chapter 3 Molybdenum and its Compounds 21
3 1 Molybdenum 21
3 2 Oxides of Molybdenum 24
3 3 Sulphides of Molybdenum 26
3 4 Other Compounds of Molybdenum 27
3 5 Molybdenum Compounds in Lubrication 28
3 6 Chemical Uses of Molybdenum 29
Chapter 4 Properties of Molybdenum Disulphide 31
4 1 Physical Properties 31
4 2 Intercalation Compounds 34
4 3 Electrical Properties 35
XII
4 4 Chemical Properties 38
4 5 Effects of Temperature 39
4 6 Oxidation 40
4 7 Effect of Moisture 43
Chapter 5 Mechanism of Lubrication 47
5 1 Fundamentals of Friction 47
5 2 Friction of Molybdenum Disulphide 50
5 3 Effect of Contact Load on Friction 51
5 4 Effects of Vapours and Other Contaminants 56
5 5 Load-Carrying Capacity 58
5 6 Summary 58
Chapter 6 Formation of Molybdenum Disulphide Films 61
6 1 Film Formation 61
6 2 Burnished Films from Powder 62
6 3 Burnishing of Soft Films 66
6 4 Film Formation by Transfer 69
6 5 Structure of Burnished or Run-in Films 69
6 6 Effects of the Substrate on Film Formation 72
6 7 Effects of Moisture and Other Vapours on
Film Formation 77
Chapter 7 Properties of Molybdenum Disulphide Films 79
7 1 Friction 79
7 2 Effects of Moisture and Other Vapours 81
7 3 Effects of Temperature 85
7 4 Effects of Radiation 88
7 5 Effects of Vacuum 89
7 6 Effects of Particle Size and Shape 90
7 7 Effect of Film Thickness 92
7 8 Effects of Sliding Speed 97
7 9 Film Life and Mechanism of Failure 99
7 10 Effects of Additives 104
Chapter 8 Transfer in Lubrication 107
8 1 General Phenomenon of Transfer 107
8 2 Transfer of Molybdenum Disulphide 108
8 3 Applications of Transfer 115
8 4 Composition of the Transfer Source 117
8 5 Nature and Location of the Transfer Source 120
XIII
Chapter 9 Lubrication by Molybdenum Disulphide Alone 129
9 1 Different Techniques of Use 129
9 2 Use in Free Powder Form 131
9 3 Dispersions 134
9 4 Compacts 136
9 5 In-Situ Formation 138
9 6 Burnished Films 148
Chapter 10 Sputtering and Other Physical Deposition Processes 153
10 1 The Sputtering Process 153
10 2 Effects of Sputtering Variables on Film
Structure 156
10 3 Effect of Substrate 161
10 4 Structure of the Sputtered Coating 163
10 5 Performance of Sputtered Coatings 168
10 6 Effects of Co-Sputtering 171
10 7 Effects of Ion Bombardment 174
10 8 Pulsed Laser Deposition 176
Chapter 11 Bonded Films 179
11 1 Types of Bonded Film 179
11 2 Other Components of Bonded Films 186
11 3 Substrate Preparation and Pre-Treatment 187
11 4 Application of the Bonded Film 192
11 5 Curing the Film 195
11 6 Plasma Spraying 195
11 7 Friction and Wear Properties of Bonded Films 196
11 8 Repair and Renewal of Films 204
Chapter 12 Composites 207
12 1 Lubricating Composites 207
12 2 Polymer Composites 208
12 3 Metallic Composites 226
12 4 Ceramic and Inorganic Composites 233
12 5 Transfer Lubrication of Rolling Bearings 235
xvi
Figure 6 2 Structure of a Burnished Molybdenum
Disulphide Film 63
Figure 6 3 Change in Friction with Running Time for a
Rubbed Film of Molybdenum Disulphide 65
Figure 6 4 Arrangement of the Layers During Rotational
or Oscillational Movement 71
Figure 7 1 Effect of Humidity on the Coefficient of Static
Friction of a Rubbed Film of Molybdenum Disulphide 80
Figure 7 2 Change in Friction of a Rubbed Film of
Molybdenum Disulphide with Time of Sliding 81
Figure 7 3 Effect of Load on the Dynamic Friction of a
Rubbed Film of Molybdenum Disulphide 82
Figure 7 4 Variation of Molybdenum Disulphide Friction
with Humidity 83
Figure 7 5 Effect of Humidity and Temperature on Friction
of a Rubbed Film of Molybdenum Disulphide 84
Figure 7 6 Variation of Friction of a Burnished Molybdenum
Disulphide Film with Temperature 85
Figure 7 7 Effect of Temperature on Life of a Burnished Film 86
Figure 7 8 Reduction in Friction of an In Situ Molybdenum
Disulphide Film with Irradiation 89
Figure 7 9 Effect of Initial Film Thickness on Life of a Bonded
Molybdenum Disulphide Film Under High Contact Stress 94
Figure 7 10 Effect of Initial Film Thickness on Wear
Life of a Bonded Molybdenum Disulphide Film
at Low Contact Stress in a Pin-on-Disc Test
95
XVII
Figure 7 11 Effect of Initial Film Thickness on Wear
Life of a Bonded Molybdenum Disulphide Film
at Low Contact Stress in Conformal Contact 96
Figure 7 12 Effect of Speed and Humidity on Friction
of Rubbed-On Molybdenum Disulphide Films 98
Figure 7 13 Variation of Bonded Molybdenum Disulphide
Film Life with Sliding Speed 99
Figure 7 14 Three Stages in the Life and Failure of a
Burnished Molybdenum Disulphide Film 100
Figure 7 15 Blisters Developing in a Burnished
Molybdenum Disulphide Film 102
Figure 8 1 Effect of Substrate Hardness on the Life
of a Transfer Film of Molybdenum Disulphide 114
Figure 8 2 Variation of Structural Strength of a Molybdenum
Disulphide Compact with Compaction Pressure 118
Figure 8 3 Effect of Compacting Pressure on Wear Rate
of a Molybdenum Disulphide Compact 119
Figure 8 4 Some Solid Lubricant Reservoir Designs
for a Small Piston Engine 122
Figure 8 5 Lubricant Reservoir Pattern Used in a
Helicopter Linkage Bearing 123
Figure 8 6 Etched-Pocket Lubricant Reservoirs 125
Figure 8 7 Use of Lubricating Idler Gears to Lubricate a Gear Set 126
Figure 8 8 Transfer Lubrication of a Gear Train 127
Figure 9 1 Effect of Deposition Time on In Situ Thickness 140
XVIII
Figure 9 2 Variation of Friction with Life for
an In-Situ Film at Different Temperatures 142
Figure 9 3 Device Used to Apply Burnished Coatings
to Flat Surfaces 149
Figure 10 1 Schematic Diagram of a Typical D-C Sputtering System 154
Figure 10 2 Schematic Diagram of a Typical R-F Sputtering System 155
Figure 10 3 Effect of Negative DC Bias on Coefficient of Sliding
Friction for Sputtered Molybdenum Disulphide 159
Figure 10 4 Sulphur Content of Sputtered Molybdenum Disulphide
as a Function of Deposition Rate 160
Figure 10 5 Structure of a Type I Sputtered Film 164
Figure 10 6 X-Ray Diffraction Intensities of an As-Sputtered
Molybdenum Disulphide Film and a Wear Track Showing
Re-Orientation of the Crystal Structure 165
Figure 10 7 Fracture of Columnar Sputtered Film 166
Figure 10 8 Variation of Sputtered Molybdenum
Disulphide Film Life with Gold Content 173
Figure 10 9 Effect of Bombarding Current Density on
Sulphur/Molybdenum Ratio in a Sputtered Film 174
Figure 10 10 Schematic Layout of a Pulsed Laser Deposition System 176
Figure 10 11 Effect of Post-Deposition Laser Annealing on the
Crystallinity of a PLD Molybdenum Disulphide 177
Figure 11 1 Effect of Various Surface Finishes on Wear Life
of a Bonded Molybdenum Disulphide Coating 190
XIX
Figure 11 2 Variation of Friction with Time of Sliding
for a Bonded Molybdenum Disulphide Film 197
Figure 11 3 Effect of Load on Wear Life of a Phenolic-
Bonded Film 200
Figure 11 4 Effect of Speed on Wear Life of a Phenolic-
Bonded Film 201
Figure 11 5 Effect of Temperature on Wear Life of Bonded Coatings 203
Figure 12 1 Limiting Pressure/Velocity Curves for
Polymeric Bearing Materials 215
Figure 12 2 Changes to Counterface During Composite Sliding 217
Figure 12 3 Effect of Load on Wear Rate of Nylon With
and Without Molybdenum Disulphide 221
Figure 12 4 Variation of Friction with Applied Load for Various
Polymers Grafted on Molybdenum Disulphide 224
Figure 12 5 Variation of Brush Wear Rate with
Molybdenum Disulphide Content 242
Figure 13 1 Effect of Burnished Film of Molybdenum
Disulphide Powder on Wetted Area 248
Figure 13 2 Variation of Friction with Sommerfeld
Number for a Series of Dispersions of
Molybdenum Disulphide in Mineral Oil 250
Figure 13 3 Effect of Molybdenum Disulphide Addition on Wear
Rate in a Single-Cylinder Diesel Engine 257
Figure 13 4 Four-Ball Machine Load/Wear Scar
Relationships for Oil with Molybdenum
Disulphide or Zinc Dialkyldithiophosphate 258
XX
Figure 13 5 Four-Ball Machine Test Results for Base
Oil Containing Molybdenum Disulphide and
Zinc Di-lsopropyldithiophosphate 260
Figure 13 6 Effect of Molybdenum Disulphide Content in
a Mineral Oil on the Friction in Deformation
of Aluminium Rings 281
Figure 14 1 Three Theoretical Geometries for the
Interaction of Dichalcogenide Molecules 286
Figure 14 2 Crystal Structure of Graphite 289
Figure 14 3 Crystal Structure of Graphite Fluoride 292
Figure 14 4 Oxidation Rates of Molybdenum Disulphide
and Tungsten Disulphide 297
Figure 14 5 Variation of Friction with Temperature
for Molybdenum Disulphide and Tungsten
Disulphide in Air 298
Figure 16 1 Effect of Speed and Load on Choice of Lubricant Type 316
Figure 16 2 Approximate Speed and Load Limits for
Different Classes of Lubricant 317
Figure 16 3 Factors Affecting the Choice of Lubricant Class 318
XXI
TABLES
Table 1 1 Some Spacecraft Applications of Molybdenum Disulphide 8
Table 1 2 Some Applications of Molybdenum Disulphide 9
Table 2 1 Molybdenum-Containing Minerals 12
Table 2 2 Western World Molybdenum Demand and Supply 1973-1989 13
Table 2 3 Analysis of Commercial Lubricant Grade
Molybdenum Disulphide Powder 15
Table 2 4 Relative Abrasiveness of Materials 16
Table 2 5 Chemical Properties of Commercial and
Upgraded Molybdenum Disulphide 17
Table 2 6 Typical Composition of Technical Molybdic Oxide 19
Table 3 1 Electron Orbital Assignments for Some
Transition Elements 22
Table 3 2 Some Physical Properties of Molybdenum 23
Table 3 3 Approximate Breakdown of Molybdenum Utilisation 25
Table 3 4 Properties of Less Common Molybdenum Sulphides 27
Table 4 1 Physical Properties of Molybdenum Disulphide 32
Table 4 2 Electrical Resistance of Molybdenum
Disulphide at Various Temperatures 36
XXII
Table 4 3 Variation of pH with Surface Area of Powders 42
Table 6 1 Wear Life of Different Alloys with a Bonded
Molybdenum Disulphide Film 75
Table 6 2 Wear Lives in Minutes for Metal Sulphides
on Different Metal Substrates 76
Table 7 1 Variation of Wear Life with Sliding Speed 98
Table 7 2 Synergistic Effect of Antimony Trioxide
and Lead Monoxide on Wear Life 106
Table 9 1 Processes Using Molybdenum Disulphide Alone 130
Table 9 2 Lubrication by Molybdenum Disulphide in a Gas Stream 132
Table 9 3 Weight Loss under Fretting Conditions 133
Table 9 4 Friction of In Situ Molybdenum Disulphide 139
Table 9 5 Performance of Different Molybdenum Disulphide Films 141
Table 9 6 Effect of Pretreatment on Wear Resistance
of In Situ Coatings 143
Table 9 7 Some Organo-Molybdenum Compounds Studied
for Lubricant Performance 146
Table 10 1 Sputtering Variables 157
Table 10 2 Friction of Uncontaminated Coatings 169
Table 10 3 Effects of Co-Sputtered Nickel in Different Atmospheres 172
Table 11 1 Bonded Film Components 180
Table 11 2 Some Bonded Film Formulations 182
Table 11 3 Compositions of Two Coatings with
Aluminium Phosphate Binders
XXIII
184
Table 11 4 Composition of a Ceramic-Bonded Film 186
Table 11 5 Effect of Grit-Blasting Pretreatment on Wear Life
of a Silicate-Bonded Molybdenum Disulphide Film 189
Table 11 6 Chemical Conversion Coatings 191
Table 11 7 Spraying Conditions for Bonded Films 194
Table 11 8 Results of Immersion Cleaning Tests of
Molybdenum Disulphide Films 205
Table 12 1 Common Thermosetting Polymers 209
Table 12 2 Common Thermoplastics 211
Table 12 3 Properties of Some Principal Bearing Polymers 212
Table 12 4 Some Components Used in Polymer Composites 213
Table 12 5 Relation Between Glass Fibre Orientation
and Specific Wear Rate for Duroid 5813 215
Table 12 6 Effect of Fillers on the Properties of PTFE 218
Table 12 7 Properties of Two Ternary PTFE Composites 219
Table 12 8 Properties of Nylon With or Without Molybdenum Disulphide 220
Table 12 9 Melting-Points and Possible Sintering
Temperatures of Metals 227
Table 12 10 Composition and Properties of Some
Molybdenum Disulphide/Metal Composites
230
XXIV
Table 12 11 Transfer Lubrication of Ball Bearings with
Polymeric Composite Retainers 237
Table 12 12 Transfer Lubrication of Ball Bearings with
Metallic Composite Retainers 238
Table 12 13 Performance of Some Lubricating Compact Brush Materials
in a Vacuum of 10 8 tolO’9 Torr (0 14 to 1 4/wPa) 241
Table 12 14 Some Composites Tested by Christy for
Small Actuator Motors 243
Table 13 1 Load-Carrying Capacity and Wear Life of
Molybdenum Disulphide in the Falex Tester
With and Without Mineral Oil 246
Table 13 2 Effect of Mineral Oils on the Friction
of a Burnished Film 247
Table 13 3 Improvement in Tool Life with a Molybdenum
Disulphide-Containing Cutting Fluid 264
Table 13 4 Some Commercial Dispersions of Molybdenum
Disulphide in Oils 265
Table 13 5 Effect of Molybdenum Disulphide on Properties of
Lithium-Based and Organo-Clay Based Greases 268
Table 13 6 Typical Load-Carrying Capacity Figures for Lithium
Soap Greases With and Without Molybdenum Disulphide 269
Table 13 7 Increase in Load-Carrying Capacity of a Di-Ester
Grease With Molybdenum Disulphide Content 271
Table 13 8 Some Applications of Molybdenum Disulphide Greases 273
Table 13 9 Some Commercial Molybdenum Disulphide Greases 274
XXV
Table 13 10 Some Commercial Dispersions and Pastes
for Anti-Seize, Assembly and Metalforming 277
Table 13 11 Effect of Lubricants on Thread Friction 278
Table 14 1 Physical Properties of the Lamellar Solid Lubricants 284
Table 14 2 Part of the Periodic Table Showing the Transition
Elements Whose Dichalcogenides Have Lamellar
Crystal Structures and Good Lubricating Properties 285
Table 14 3 Main Characteristics of Graphite as a Lubricant 288
Table 14 4 Some Graphite-Containing Dispersions 291
Table 14 5 Effect of Gaseous Environment on the Wear Lives
of Molybdenum Disulphide and Graphite Fluoride Films 293
Table 14 6 Some Reported Coefficients of Friction for
Transition Metal Dichalcogenides 295
Table 14 7 Limiting Temperatures for Dichalcogenides
in Air and Vacuum 296
Table 14 8 Change in Friction of Dichalcogenides
Tested in a Steam Atmosphere 299
Table 14 9 Endurance of Some Burnished Dichalcogenide Films 300
Table 14 10 Properties of Some Dichalcogenide Composites 302
Table 14 11 Some Composites of Synthetic Dichalcogenides 303
Table 16 1 Advantages and Disadvantages of Solid Lubricants 315
Table 16 2 Comparative Properties of Molybdenum
Disulphide, Graphite and PTFE 319
XXVI
Table 16 3 Approximate Temperature Limits for Some Solid Lubricants 320
Table 16 4 Some Characteristics and Applications
of Less Common Solid Lubricants 321
Table 16 5 Some Techniques for Using Molybdenum Disulphide 324
Table 16 6 Important Factors in Designing for the
Use of Molybdenum Disulphide Films 325
Table 16 7 Guide to Dynamic Friction Coefficients
|
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| author | Lansdown, A. R. |
| author_facet | Lansdown, A. R. |
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| dewey-full | 621.8/9 |
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| dewey-ones | 621 - Applied physics |
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| dewey-search | 621.8/9 |
| dewey-sort | 3621.8 19 |
| dewey-tens | 620 - Engineering and allied operations |
| discipline | Maschinenbau / Maschinenwesen Physik |
| edition | 1. ed. |
| format | Book |
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| id | DE-604.BV013029419 |
| illustrated | Illustrated |
| indexdate | 2024-07-09T18:37:55Z |
| institution | BVB |
| isbn | 0444500324 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-008876644 |
| oclc_num | 41165450 |
| open_access_boolean | |
| owner | DE-703 DE-634 DE-83 |
| owner_facet | DE-703 DE-634 DE-83 |
| physical | XXVI, 380 S. Ill., graph. Darst. |
| publishDate | 1999 |
| publishDateSearch | 1999 |
| publishDateSort | 1999 |
| publisher | Elsevier |
| record_format | marc |
| series | Tribology series |
| series2 | Tribology series |
| spelling | Lansdown, A. R. Verfasser aut Molybdenum disulphide lubrication A. R. Lansdown 1. ed. Amsterdam [u.a.] Elsevier 1999 XXVI, 380 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Tribology series 35 Molybdenum Disulphide Lubrication and lubricants Molybdenum disulphide Festschmierstoff (DE-588)4154197-2 gnd rswk-swf Molybdändisulfid (DE-588)4170411-3 gnd rswk-swf Festschmierstoff (DE-588)4154197-2 s Molybdändisulfid (DE-588)4170411-3 s DE-604 Tribology series 35 (DE-604)BV001900804 35 HEBIS Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=008876644&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Lansdown, A. R. Molybdenum disulphide lubrication Tribology series Molybdenum Disulphide Lubrication and lubricants Molybdenum disulphide Festschmierstoff (DE-588)4154197-2 gnd Molybdändisulfid (DE-588)4170411-3 gnd |
| subject_GND | (DE-588)4154197-2 (DE-588)4170411-3 |
| title | Molybdenum disulphide lubrication |
| title_auth | Molybdenum disulphide lubrication |
| title_exact_search | Molybdenum disulphide lubrication |
| title_full | Molybdenum disulphide lubrication A. R. Lansdown |
| title_fullStr | Molybdenum disulphide lubrication A. R. Lansdown |
| title_full_unstemmed | Molybdenum disulphide lubrication A. R. Lansdown |
| title_short | Molybdenum disulphide lubrication |
| title_sort | molybdenum disulphide lubrication |
| topic | Molybdenum Disulphide Lubrication and lubricants Molybdenum disulphide Festschmierstoff (DE-588)4154197-2 gnd Molybdändisulfid (DE-588)4170411-3 gnd |
| topic_facet | Molybdenum Disulphide Lubrication and lubricants Molybdenum disulphide Festschmierstoff Molybdändisulfid |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=008876644&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| volume_link | (DE-604)BV001900804 |
| work_keys_str_mv | AT lansdownar molybdenumdisulphidelubrication |