Quantitative chemical analysis:
Saved in:
| Main Author: | |
|---|---|
| Format: | Book |
| Language: | English |
| Published: |
New York, NY
Freeman
1999
|
| Edition: | 5. ed., 2. print. |
| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Physical Description: | Getr. Zählung Ill., graph. Darst. 1 CD-ROM (12 cm) |
| ISBN: | 0716728818 |
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| 264 | 1 | |a New York, NY |b Freeman |c 1999 | |
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Contents
Preface
xvii
Chapter 0 The Analytical Process
Actions and Consequences
0-1 Analytical Chemists Are Sleuths—And Sometimes
Life Is Messy! 1
0-2 Sampling and Sample Preparation 7
0-3 General Steps in a Chemical Analysis 8
Box 0-1 Constructing a Representative Sample 9
Chapter 1 Measurements
Measuring the Universe
1-1 SI Units
1-2 Chemical Concentrations
1 -3 Preparing Solutions
1-4 Solutions and Stoichiometry
Chapter 2 Tools of the Trade
13
12
13
16
20
22
29
Weighing Femtomoles of DNA 28
2-1 Safe, Ethical Handling of Chemicals and Waste 29
Box 2-1 Disposal of Chemical Waste
2-2 The Lab Notebook
2-3 Analytical Balance
Box 2-2 Quartz Crystal Microbalance
2-4 Burets
2-5 Volumetric Flasks
2-6 Pipets and Syringes
2-7 Filtration
2-8 Drying
2-9 Calibration of Volumetric Glassware
Chapter 3 Experimental Error
Experimental Error
3-1 Significant Figures
3-2 Significant Figures in Arithmetic
3-3 Significant Figures and Graphs
29
31
31
34
36
38
40
41
43
45
51
50
51
52
55
3-4 Types of Error 56
Box 3-1 Standard Reference Materials 57
3-5 Propagation of Uncertainty 58
Chapter 4 Statistics and Spreadsheets 69
Is My Red Blood Cell Count High Today?
4-1 Gaussian Distribution
4-2 Confidence Intervals
4-3 Comparison of Means with Student's t
4-4 Control Charts
Box 4-1 Analytical Chemistry and the Law
4-5 Q Test for Bad Data
4-6 Spreadsheets
Chapter 5 Calibration Methods
A Historic Calibration Curve
5-1 Finding the "Best" Straight Line
5-2 Calibration Curves
Box 5-1 Using a Nonlinear Calibration Curve
5-3 Standard Addition
5-4 Internal Standards
5-5 A Spreadsheet for Least Squares
68
69
74
77
81
81
82
83
93
92
93
97
99
101
104
106
Chapter 6 Chemical Equilibrium 113
Chemical Equilibrium in the Environment
6-1 The Equilibrium Constant
6-2 Equilibrium and Thermodynamics
6-3 Solubility Product
6-4 The Common Ion Effect
Demonstration 6-1 Common Ion Effect
Box 6-1 The Logic of Approximations
6-5 Separation by Precipitation
6-6 Complex Formation
Box 6-2 Notation for Formation Constants
6-7 Protic Acids and Bases
6-8 pH
112
113
115
118
119
120
121
122
123
124
126
129
XI
XII
Contents
6-9 Strengths of Acids and Bases 131
Demonstration 6-2 The HC1 Fountain 132
Box 6-3 The Strange Behavior of Hydrofluoric
Acid 133
Box 6-4 Carbonic Acid 136
Chapter 7 Let the Titrations Begin 149
Chapter 10 Monoprotic Acid-Base
Equilibria
211
Evolution of the Buret
7-1 Titrations
7-2 Titration Calculations
7-3 Spectrophotometric Titrations
7-4 The Precipitation Titration Curve
7-5 Titration of a Mixture
7-6 Calculating Titration Curves with
a Spreadsheet
7-7 End-Point Detection
Demonstration 7-1 Fajans Titration
Chapter 8 Activity
Hydrated Radii
8-1 The Effect of Ionic Strength on Solubility
of Salts
Demonstration 8-1 Effect of Ionic Strength
on Ion Dissociation
Box 8-1 Salts with Ions of Charge 121 Do
Not Fully Dissociate into Ions in Water
8-2 Activity Coefficients
8-3 Using Activity Coefficients
8-4 pH Revisited
Chapter 9 Systematic Treatment
of Equilibrium
Acid Rain
9-1 Charge Balance
9-2 Mass Balance
9-3 Systematic Treatment of Equilibrium
Box 9-1 Calcium Carbonate Mass Balance
in Rivers
9-4 The Dependence of Solubility on pH
Box 9-2 All Right, Dan, How Would You
Really Solve The CaF2 Problem?
Box 9-3 pH and Tooth Decay
148
149
151
153
155
161
162
164
166
175
174
175
177
178
178
183
185
191
190
191
192
194
195
197
200
202
Measuring pH Inside Single Cells 210
10-1 Strong Acids and Bases 211
10-2 Weak Acids and Bases 214
10-3 Weak-Acid Equilibria 215
Demonstration 10-1 Conductivity of Weak
Electrolytes 218
10-4 Weak-Base Equilibria 219
Box 10-1 Dyeing Fabrics and the Fraction
of Dissociation 220
10-5 Buffers 222
Box 10-2 Strong Plus Weak Reacts
Completely 227
Demonstration 10-2 How Buffers Work 228
Chapter 11 Polyprotic Acid-Base
Equilibria 239
Proteins Are Polyprotic Acids and Bases 238
11-1 Diprotic Acids and Bases 239
Box 11-1 Successive Approximations 246
11-2 Diprotic Buffers 249
11-3 Polyprotic Acids and Bases 250
11-4 Which Is the Principal Species? 252
11-5 Fractional Composition Equations 254
11-6 Isoelectric and Isoionic pH 256
Box 11-2 Isoelectric Focusing 258
Chapter 12 Acid-Base Titrations 265
Acid-Base Titration of a Protein
12-1 Titration of Strong Acid with Strong Base
12-2 Titration of Weak Acid with Strong Base
12-3 Titration of Weak Base with Strong Acid
12-4 Titrations in Diprotic Systems
12-5 Finding the End Point with a pH Electrode
Box 12-1 Alkalinity and Acidity
12-6 Finding the End Point with Indicators
Box 12-2 What Does a Negative pH Mean?
Demonstration 12-1 Indicators and the Acidity
ofCO2
Box 12-3 World Record Small Titration
12-7 Practical Notes
12-8 Titrations in Nonaqueous Solvents
12-9 Calculating Titration Curves
with Spreadsheets
264
265
268
272
274
277
277
282
284
284
287
287
289
292
Contents
xm
Chapter 13 EDTA Titrations
307 Chapter 16 Redox Titrations
A Chelating Ligand Captures Its Prey
13-1 Metal-Chelate Complexes
13-2 EDTA
Box 13-1 Chelation Therapy
and Thalassemia
13-3 EDTA Titration Curves
13-4 Do It with a Spreadsheet
13-5 Auxiliary Complexing Agents
13-6 Metal Ion Indicators
Demonstration 13-1 Metal Ion Indicator
Color Changes
13-7 EDTA Titration Techniques
Box 13-2 Water Hardness
306
307
310
310
316
319
320
323
325
325
328
Chapter 14
Fundamentals
of Electrochemistry
337
An Atomic-Scale Galvanic Cell 336
14-1 Basic Concepts 337
14-2 Galvanic Cells 341
Demonstration 14-1 The Human Salt Bridge 344
14-3 Standard Potentials 345
14-4 Nernst Equation 347
Box 14-1 E° and the Cell Voltage Do Not
Depend on How You Write the Cell Reaction 349
Box 14-2 Larimer Diagrams:
How to Find E° for a New Half-Reaction 351
14-5 E° and the Equilibrium Constant 353
Box 14-3 Concentrations in the Operating Cell 353
14-6 Cells as Chemical Probes 356
14-7 Biochemists Use E°' 359
Chapter 15
Electrodes and
Potentiometry
375
A Heparin Sensor
15-1 Reference Electrodes
15-2 Indicator Electrodes
15-3 What Is a Junction Potential?
15-4 pH Measurement with a Glass Electrode
Demonstration 15-1 Potentiometry with
an Oscillating Reaction
15-5 Ion-Selective Electrodes
Box 15-1 Systematic Error in Rainwater
pH Measurement: The Effect of Junction
Potential
15-6 Using Ion-Selective Electrodes
15-7 Solid-State Chemical Sensors
Chemical Analysis of High-Temperature
Superconductors
16-1 The Shape of a Redox Titration Curve
16-2 Redox Indicators
Demonstration 16-1 Potentiometric Titration
ofFe2+withMnO4
16-3 Adjustment of Analyte Oxidation State
16-4 Oxidation with Potassium Permanganate
16-5 Oxidation with Ce4+
16-6 Oxidation with Potassium Dichromate
16-7 Methods Involving Iodine
Box 16-1 Environmental Carbon Analysis
and Oxygen Demand
Box 16-2 Iodometric Analysis
of High-Temperature Superconductors
Chapter 17 Electrogravimetric and
~~ Coulometric Analyses
How Sweet It Is!
17-1 Electrolysis: Putting Electrons to Work
17-2 Why Voltage Changes When Current Flows
Demonstration 17-1 Electrochemical Writing
17-3 Electrogravimetric Analysis
Demonstration 17-2 Silver and Gold Pennies
17-4 Coulometric Analysis
17-5 Mediators
Box 17-1 Electrical Wiring of Redox
Enzymes
415
414
415
421
422
424
426
428
429
429
430
434
Chapter 18 Voltammetry
443
442
443
445
446
451
455
457
460
462
471
470
374 18-2
375
378 18-3
380 18-4
381 18-5
18-6
382
391
18-7
392 18-8
398
400
Oxygen Sensors for Automobile Pollution Control
18-1 Why We Use a Mercury Electrode
in Polarography 471
Shape of the Polarogram 472
Box 18-1 The Electric Double Layer 477
Polarography in Chemical Analysis 481
Pulse Polarography 483
Stripping Analysis 487
Cyclic Voltammetry 489
Box 18-2 An Optically Transparent
Thin-Layer Electrode 492
Amperometry 493
Box 18-3 Oxygen Electrodes 494
Karl Fischer Titration of H:O 497
Demonstration 18-1 The Karl Fischer Jacks
of a pH Meter 499
XIV
Contents
Chapter 19
Fundamentals of
Spectrophotometry
511
The Ozone Hole 510
19-1 Properties of Light 511
19-2 Absorption of Light 512
Box 19-1 Why Is There a Logarithmic Relation
Between Transmittance and Concentration? 515
Demonstration 19-1 Absorption Spectra 516
19-3 The Spectrophotometer 517
19-4 Beer's Law in Chemical Analysis 521
19-5 What Happens When a Molecule
Absorbs Light? 525
Box 19-2 Fluorescence All Around Us 529
19-6 Luminescence 530
Chapter 20 Applications of
Spectrophotometry 545
Fiber-Optic Glucose Sensor 544
20-1 Analysis of a Mixture 545
20-2 Measuring an Equilibrium Constant:
The Scatchard Plot 550
20-3 The Method of Continuous Variation 551
20-4 Flow Injection Analysis 554
20-5 Immunoassays 556
20-6 Sensors Based on Luminescence Quenching 559
Box 20-1 Converting Light into Electricity 560
Chapter 21 Spectrophotometers 577
The Most Important Photoreceptor
21 -1 Interaction of Light with Matter
Box 21-1 Blackbody Radiation and
the Greenhouse Effect
21-2 The Spectrophotometer
21-3 Lamps and Lasers: Sources of Light
21-4 Monochromators
21-5 Detectors
21-6 Errors in Spectrophotometry
21-7 Optodes
Box 21-2 On the Road to
an "Electronic Nose"
21-8 Fourier Transform Infrared Spectroscopy
21-9 Dealing with Noise
576
577
582
583
584
586
589
594
596
598
600
606
Chapter 22 Atomic Spectroscopy 615
An Anthropology Puzzle 614
22-1 An Overview 615
22-2 Atomization: Flames, Furnaces, and Plasmas 619
22-3 How Temperature Affects Atomic Spectroscopy 625
22-4 Instrumentation 627
22-5 Interference 632
Box 22-1 A Smokestack Metal Emission Monitor:
Challenges in Sampling and Calibration 632
Chapter 23 Introduction to Analytical
Separations 641
Analytical Separations and Chemical Problem
Solving 640
23-1 Solvent Extraction 641
Demonstration 23-1 Extraction with Dithizone 646
23-2 What Is Chromatography? 646
Box 23-1 Crown Ethers 647
23-3 A Plumber's View of Chromatography 649
23-4 Efficiency of Separation 654
23-5 Why Bands Spread 660
Chapter 24 Gas Chromatography 675
674
What Did They Eat in the Year 1000?
24-1 The Separation Process in Gas
Chromatography 675
Box 24-1 Chiral Phases For Separating Optical
Isomers 680
Sample Injection 685
Detectors 689
Sample Preparation 694
Method Development in Gas Chromatography 696
24-2
24-3
24-4
24-5
24-6
24-7
What Is Mass Spectrometry? 699
Box 24-2 How the Magnetic Sector Mass
Spectrometer Separates Ions of Different
Mass 702
Mass Spectrometry in Analytical Chemistry 704
Box 24-3 Isotope Ratio Mass Spectrometry 704
Chapter 25 High-Performance Liquid
Chromatography 713
In Vivo Microdialysis for Measuring Drug
Metabolism 712
25-1 The Chromatographic Process 714
Box 25-1 Designer Stationary Phases 718
Box 25-2 Supercritical Fluid
Chromatography 724
Injection and Detection in HPLC 727
Method Development for Reversed-Phase
Separations 733
Gradient Separations 739
Liquid Chromatography/Mass Spectrometry 742
25-2
25-3
25-4
25-5
Contents
xv
Chapter 26 Chromatographic Methods and
Capillary Electrophoresis 755
The Shape of the Future: Analysis on a Chip 754
26-1 Ion-Exchange Chromatography 755
26-2 Ion Chromatography 762
26-3 Molecular Exclusion Chromatography 766
26-4 Affinity Chromatography 769
26-5 Capillary Electrophoresis 769
Box 26-1 Chemical Analysis of a Single Cell 771
Chapter 27 Gravimetric and Combustion
Analysis 795
Tree Rings and Our Changing Environment 794
27-1 An Example of Gravimetric Analysis 795
27-2 Precipitation 797
Demonstration 27-1 Colloids and Dialysis 798
27-3 Examples of Gravimetric Calculations 803
27-4 Combustion Analysis 806
Chapter 28 Sample Preparation 817
Extraction Membranes
Box 28-1 The Horwitz Trumpet: Variation in
Interlaboratory Tests
28-1 Statistics of Sampling
28-2 Dissolving Samples for Analysis
28-3 Sample Preparation Techniques
28-4 Analytical Standards
Chapter 29 Experiments
29-1 Calibration of Volumetric Glassware
29-2 Gravimetric Determination of Calcium as
CaC2OyH2O
29-3 Gravimetric Determination of Iron as Fe2O3
29-4 Statistical Evaluation of Acid-Base Indicators
29-5 Preparing Standard Acid and Base
29-6 Using a pH Electrode for an Acid-Base
Titration
29-7 Analysis of a Mixture of Carbonate
and Bicarbonate
29-8 Analysis of an Acid-Base Titration Curve:
The Gran Plot
29-9 EDTA Titration of Ca2+ and Mg2+
in Natural Waters
816
818
819
824
831
835
843
843
844
845
846
848
849
850
852
853
29-10 Synthesis and Analysis of Ammonium
Decavanadate 853
29-11 lodimetric Titration of Vitamin C 856
29-12 Preparation and Iodometric Analysis of
High-Temperature Superconductor 856
29-13 Potentiometric Halide Titration with Ag+ 859
29-14 Electrogravimetric Analysis of Copper 861
29-15 Polarographic Measurement of
an Equilibrium Constant 861
29-16 Coulometric Titration of Cyclohexene
with Bromine 862
29-17 Spectrophotometric Determination of Iron
in Vitamin Tablets 863
29-18 Microscale Spectrophotometric Measurement
of Iron in Foods by Standard Addition 864
29-19 Spectrophotometric Measurement of
an Equilibrium Constant 865
29-20 Properties of an Ion-Exchange Resin 866
29-21 Analysis of Sulfur in Coal by Ion
Chromatography 868
29-22 Measuring Carbon Monoxide in Automobile
Exhaust by Gas Chromatography 868
29-23 Amino Acid Analysis by Capillary
Electrophoresis 869
29-24 DNA Composition by High-Performance
Liquid Chromatography 871
Glossary 875
Appendixes AP1
A Logarithms and Exponents API
B Graphs of Straight Lines AP2
C Propagation of Uncertainty AP4
D Oxidation Numbers and Balancing Redox
Equations AP5
E Normality AP10
F Solubility Products AP12
G Acid Dissociation Constants AP15
H Standard Reduction Potentials AP27
I Stepwise Formation Constants AP39
J Logarithm of the Formation Constant for the
Reaction M(aq) + L(aq) ^ ML(aq) AP42
Solutions to Exercises
Answers to Problems
Index
SE1
AN1
11 |
| any_adam_object | 1 |
| author | Harris, Daniel C. 1948- |
| author_GND | (DE-588)172126363 |
| author_facet | Harris, Daniel C. 1948- |
| author_role | aut |
| author_sort | Harris, Daniel C. 1948- |
| author_variant | d c h dc dch |
| building | Verbundindex |
| bvnumber | BV012962788 |
| callnumber-first | Q - Science |
| callnumber-label | QD101 |
| callnumber-raw | QD101.2 H37 1999 |
| callnumber-search | QD101.2 H37 1999 |
| callnumber-sort | QD 3101.2 H37 41999 |
| callnumber-subject | QD - Chemistry |
| classification_rvk | VG 6100 |
| ctrlnum | (OCoLC)300458776 (DE-599)BVBBV012962788 |
| discipline | Chemie / Pharmazie |
| edition | 5. ed., 2. print. |
| format | Book |
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| genre | (DE-588)4123623-3 Lehrbuch gnd-content Matériel didactique |
| genre_facet | Lehrbuch Matériel didactique |
| id | DE-604.BV012962788 |
| illustrated | Illustrated |
| indexdate | 2024-12-06T09:10:44Z |
| institution | BVB |
| isbn | 0716728818 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-008828982 |
| oclc_num | 300458776 |
| open_access_boolean | |
| owner | DE-29T |
| owner_facet | DE-29T |
| physical | Getr. Zählung Ill., graph. Darst. 1 CD-ROM (12 cm) |
| publishDate | 1999 |
| publishDateSearch | 1999 |
| publishDateSort | 1999 |
| publisher | Freeman |
| record_format | marc |
| spelling | Harris, Daniel C. 1948- Verfasser (DE-588)172126363 aut Quantitative chemical analysis Daniel C. Harris 5. ed., 2. print. New York, NY Freeman 1999 Getr. Zählung Ill., graph. Darst. 1 CD-ROM (12 cm) txt rdacontent n rdamedia nc rdacarrier Analyse quantitative (Chimie) Analytische Chemie (DE-588)4129906-1 gnd rswk-swf Quantitative Analyse (DE-588)4125311-5 gnd rswk-swf Chemie (DE-588)4009816-3 gnd rswk-swf (DE-588)4123623-3 Lehrbuch gnd-content Matériel didactique Quantitative Analyse (DE-588)4125311-5 s Chemie (DE-588)4009816-3 s 1\p DE-604 Analytische Chemie (DE-588)4129906-1 s 2\p DE-604 HBZ Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=008828982&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis 1\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk 2\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk |
| spellingShingle | Harris, Daniel C. 1948- Quantitative chemical analysis Analyse quantitative (Chimie) Analytische Chemie (DE-588)4129906-1 gnd Quantitative Analyse (DE-588)4125311-5 gnd Chemie (DE-588)4009816-3 gnd |
| subject_GND | (DE-588)4129906-1 (DE-588)4125311-5 (DE-588)4009816-3 (DE-588)4123623-3 |
| title | Quantitative chemical analysis |
| title_auth | Quantitative chemical analysis |
| title_exact_search | Quantitative chemical analysis |
| title_full | Quantitative chemical analysis Daniel C. Harris |
| title_fullStr | Quantitative chemical analysis Daniel C. Harris |
| title_full_unstemmed | Quantitative chemical analysis Daniel C. Harris |
| title_short | Quantitative chemical analysis |
| title_sort | quantitative chemical analysis |
| topic | Analyse quantitative (Chimie) Analytische Chemie (DE-588)4129906-1 gnd Quantitative Analyse (DE-588)4125311-5 gnd Chemie (DE-588)4009816-3 gnd |
| topic_facet | Analyse quantitative (Chimie) Analytische Chemie Quantitative Analyse Chemie Lehrbuch Matériel didactique |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=008828982&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT harrisdanielc quantitativechemicalanalysis |