Analysis of carbohydrates by capillary electrophoresis:
Saved in:
| Main Authors: | , |
|---|---|
| Format: | Book |
| Language: | German |
| Published: |
Braunschweig ; Wiesbaden
Vieweg
1999
|
| Series: | Chromatographia CE series
3 |
| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Item Description: | Literaturangaben |
| Physical Description: | XIII, 175 S. graph. Darst. |
| ISBN: | 3528068884 |
Staff View
MARC
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|---|---|---|---|
| 001 | BV012300787 | ||
| 003 | DE-604 | ||
| 005 | 20001108 | ||
| 007 | t | ||
| 008 | 981201s1999 gw d||| |||| 00||| ger d | ||
| 016 | 7 | |a 955236533 |2 DE-101 | |
| 020 | |a 3528068884 |c Pp. : DM 168.00 |9 3-528-06888-4 | ||
| 035 | |a (OCoLC)44567336 | ||
| 035 | |a (DE-599)BVBBV012300787 | ||
| 040 | |a DE-604 |b ger |e rakddb | ||
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| 049 | |a DE-703 |a DE-355 | ||
| 050 | 0 | |a QP701 | |
| 084 | |a VK 8580 |0 (DE-625)147542:253 |2 rvk | ||
| 100 | 1 | |a Paulus, Aran |e Verfasser |4 aut | |
| 245 | 1 | 0 | |a Analysis of carbohydrates by capillary electrophoresis |c Aran Paulus ; Antje Klockow-Beck |
| 264 | 1 | |a Braunschweig ; Wiesbaden |b Vieweg |c 1999 | |
| 300 | |a XIII, 175 S. |b graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 490 | 1 | |a Chromatographia CE series |v 3 | |
| 500 | |a Literaturangaben | ||
| 650 | 4 | |a Capillary electrophoresis | |
| 650 | 4 | |a Carbohydrates |x Analysis | |
| 650 | 0 | 7 | |a Kohlenhydrate |0 (DE-588)4164517-0 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Kapillarelektrophorese |0 (DE-588)4290002-5 |2 gnd |9 rswk-swf |
| 689 | 0 | 0 | |a Kohlenhydrate |0 (DE-588)4164517-0 |D s |
| 689 | 0 | 1 | |a Kapillarelektrophorese |0 (DE-588)4290002-5 |D s |
| 689 | 0 | |5 DE-604 | |
| 700 | 1 | |a Klockow-Beck, Antje |e Verfasser |4 aut | |
| 830 | 0 | |a Chromatographia CE series |v 3 |w (DE-604)BV011568238 |9 3 | |
| 856 | 4 | 2 | |m DNB Datenaustausch |q application/pdf |u http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=008340325&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |3 Inhaltsverzeichnis |
Record in the Search Index
| _version_ | 1805068197356896256 |
|---|---|
| adam_text |
VII
TABLE
OF
CONTENTS
PREFACE.
.
V
TABLE
OF
CONTENTS
.
VII
LIST
OF
ABBREVIATIONS
.
X
1
INTRODUCTION
.
1
REFERENCES
.
8
2
CAPILLARY
ELECTROPHORESIS,
INSTRUMENTATION
AND
MODES
.
9
2.1
ELECTROPHORETIC
MOBILITY
.
10
2.2
FUSED
SILICA
SURFACE
AND
ELECTROOSMOTIC
FLOW
.
10
2.3
PLATE
NUMBER,
MIGRATION
TIME
AND
RESOLUTION
.
13
2.4
INSTRUMENTATION
.
14
2.4.1
POWER
SUPPLY
AND
COOLING
SYSTEM
.
14
2.4.2
CAPILLARIES
.
15
2.4.3
DETECTION
.
15
2.4.3.1
UV
DETECTION
.
15
2.4.3.2
LIF
DETECTION
.
17
2.4.3.3
INDIRECT
OPTICAL
DETECTION
METHODS
.
19
2.4.3.4
ELECTROCHEMICAL
DETECTION
.
20
2.4.3.5
REFRACTIVE
INDEX
DETECTION
.
20
2.4.3.6
MASS
SPECTROMETRY
DETECTION
.
20
2.5
CE
MODES
.
20
2.5.1
CAPILLARY
ELECTRO
CHROMATOGRAPHY
.
.
21
2.5.2
MICELLAR
ELECTROKINETIC
CAPILLARY
CHROMATOGRAPHY
.
21
2.5.3
CAPILLARY
ZONE
ELECTROPHORESIS
.
23
2.5.4
ISOTACHOPHORESIS
.
23
2.5.5
CAPILLARY
ISOELECTRIC
FOCUSING
.
.
23
2.5.6
CAPILLARY
GEL
ELECTROPHORESIS
.
;
.
24
REFERENCES
.
;
.
24
YIU
TABLE
OF
CONTENTS
3
STRUCTURES
AND
PROPERTIES
OF
CARBOHYDRATES
.
28
3.1
MONOSACCHARIDES
.
28
3.2
OLIGOSACCHARIDES
.
30
3.3
POLYSACCHARIDES
.
34
3.4
GLYCOPROTEINS
.
39
3.5
GLYCOSAMINOGLYCANS
AND
PROTEOGLYCANS
.
42
3.6
GLYCOLIPIDS
.
45
REFERENCES
.
47
4
SEPARATION
AND
DETECTION
OF
CARBOHYDRATES
IN
CAPILLARY
ELECTROPHORESIS.
.
49
4.1
SEPARATION
AND
DETECTION
OF
NON-DERIVATIZED
CARBOHYDRATES
.
50
4.1.1
ELECTROPHORESIS
OF
NATIVE
CARBOHYDRATES
WITH
DIRECT
UV
DETECTION
.
50
4.1.1.1
CZE
AND
MECC
SEPARATION
CONDITIONS
.
50
4.1.1.2
CZE
AFTER
ON-COLUMN
COMPLEXATION
WITH
BORATE
.
50
4.1.1.3
CZE
OF
GLYCOPEPTIDES
AND
GLYCOPROTEINS
.
53
4.1.2
ELECTROPHORESIS
OF
NATIVE
CARBOHYDRATES
AT
EXTREME
ALKALINE
PH
.
54
4.1.2.1
ELECTROPHORESIS
OF
NATIVE
CARBOHYDRATES
AT
EXTREME
ALKALINE
PH
WITH
INDIRECT
DETECTION
.
54
4.1.2.2
ELECTROPHORESIS
OF
NATIVE
CARBOHYDRATES
AT
EXTREME
ALKALINE
PH
WITH
AMPEROMETRIC
DETECTION
.
56
4.1.2.3
ELECTROPHORESIS
OF
NATIVE
CARBOHYDRATES
AT
EXTREME
ALKALINE
PH
WITH
REFRACTIVE
INDEX
DETECTION
.
58
4.1.3
CONCLUDING
REMARKS
.
58
4.2
SEPARATION
AND
DETECTION
OF
DERIVATIZED
CARBOHYDRATES
.
59
4.2.1
LABELING
OF
CARBOHYDRATES
.
59
4.2.1.1
REDUCTIVE
ANIMATION
.
60
4.2.1.2
LABELING
BY
CONDENSATION
WITH
L-PHENYL-3-METHYL-5-PYRAZOLONE
.
65
4.2.1.3
LABELING
BY
CONDENSATION
OF
ACIDIC
SACCHARIDES
WITH
AMINES
.
66
4.2.1.4
ESTERFICATION
OF
AMINOALDITOLS
.
66
4.2.2
DETECTION
OF
LABELED
CARBOHYDRATES
.
67
4.2.2.1
MASS
AND
CONCENTRATION
DETECTION
LIMITS
AND
MINIMAL
DERIVATIZATION
VOLUME
.
67
4.2.2.2
DETECTION
SENSITIVITY
OF
UV
DERIVATIZED
CARBOHYDRATES
.
67
4.2.2.3
DETECTION
SENSITIVITY
OF
FLUORESCENT
DERIVATIZED
CARBOHYDRATES
.
68
4.2.3
SEPARATION
OF
LABELED
CARBOHYDRATES
.
72
4.2.3.1
SEPARATION
IN
ACIDIC
ELECTROLYTES
UNDER
LOW
EOF
CONDITIONS
.
72
4.2.3.2
SEPARATION
UNDER
HIGH
EOF
CONDITIONS
.
78
4.2.3.3
MECC
SEPARATIONS
.
84
4.2.3.4
GEL
SEPARATIONS
.
87
REFERENCES
.
88
TABLE
OF
CONTENTS
IX
5
APPLICATIONS.
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
93
5.1
MONO
AND
DISACCHARIDES
.
93
5.2
OLIGOSACCHARIDES
.
-
.
'.
.
;
.
.,.
96
5.2.1
UNDERIVATIZED
OLIGOSACCHARIDES
.
96
5.2.2
DERIVATIZED
OLIGOSACCHARIDES
.
97
5.2.3
ENZYME
ACTION
ON
LABELED
OLIGOSACCHARIDES
.
101
5.2.4
LIPOOLIGOSACCHARIDES
.
104
5.3
HIGH
MOLECULAR
WEIGHT
POLYSACCHARIDES
.
105
5.4
GLYCOPEPTIDES
AND
GLYCOPROTEINS
.
108
5.4.1
GLYCOFORMS
.
108
5.4.1.1
ERYTHROPOIETIN
.
ILL
5.4.1.2
RIBONUCLEASE
.
115
5.4.1.3
OVALBUMIN
.
115
5.4.1.4
CHORIONIC
GONADOTROPIN
.
117
5.4.1.5
TISSUE
PLASMINOGEN
ACTIVATOR
.
117
5.4.1.6
TRANSFERRIN
.
120
5.4.1.7
INTERFERON
.
121
5.4.1.8
IMMUNOGLOBULINS
.
123
5.4.1.9
AI-ACID
GLYCOPROTEIN
.
123
5.4.1.10
VARIOUS
GLYCOPROTEINS
.
124
5.4.1.11
NEW
APPROACHES
IN
CE
GLYCOFORM
ANALYSIS
.
124
5.4.1.12
CE-MS
OF
GLYCOFORMS
.
126
5.4.2
GLYCOPEPTIDES
.
127
5.4.3
COMPLEX
OLIGOSACCHARIDES
.
130
5.4.3.1
UV
DETECTION
OF
DERIVATIZED
COMPLEX
OLIGOSACCHARIDES
.
130
5.4.3.2
UV
DETECTION
OF
UNDERIVATIZED
COMPLEX
OLIGOSACCHARIDES
.
135
5.4.3.3
LASER
INDUCED
FLUORESCENCE
DETECTION
(LIF)
OF
COMPLEX
OLIGOSACCHARIDES
.
137
5.5
GLYCOSAMINOGLYCANS
.
145
5.5.1
HEPARINS
.
147
5.5.2
CHONDROITIN
AND
DERMATAN
.
151
5.5.3
HYALURONAN
.
-
.
151
5.5.4
DERIVATIZED
GLYCOSAMINOGLYCANS
.
153
5.6
GLYCOLIPIDS
.
154
5.7
OTHER
GLYCOCONJUGATES
.
157
REFERENCES
.160
SUBJECT
INDEX
.
171 |
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| id | DE-604.BV012300787 |
| illustrated | Illustrated |
| indexdate | 2024-07-20T03:46:17Z |
| institution | BVB |
| isbn | 3528068884 |
| language | German |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-008340325 |
| oclc_num | 44567336 |
| open_access_boolean | |
| owner | DE-703 DE-355 DE-BY-UBR |
| owner_facet | DE-703 DE-355 DE-BY-UBR |
| physical | XIII, 175 S. graph. Darst. |
| publishDate | 1999 |
| publishDateSearch | 1999 |
| publishDateSort | 1999 |
| publisher | Vieweg |
| record_format | marc |
| series | Chromatographia CE series |
| series2 | Chromatographia CE series |
| spelling | Paulus, Aran Verfasser aut Analysis of carbohydrates by capillary electrophoresis Aran Paulus ; Antje Klockow-Beck Braunschweig ; Wiesbaden Vieweg 1999 XIII, 175 S. graph. Darst. txt rdacontent n rdamedia nc rdacarrier Chromatographia CE series 3 Literaturangaben Capillary electrophoresis Carbohydrates Analysis Kohlenhydrate (DE-588)4164517-0 gnd rswk-swf Kapillarelektrophorese (DE-588)4290002-5 gnd rswk-swf Kohlenhydrate (DE-588)4164517-0 s Kapillarelektrophorese (DE-588)4290002-5 s DE-604 Klockow-Beck, Antje Verfasser aut Chromatographia CE series 3 (DE-604)BV011568238 3 DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=008340325&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Paulus, Aran Klockow-Beck, Antje Analysis of carbohydrates by capillary electrophoresis Chromatographia CE series Capillary electrophoresis Carbohydrates Analysis Kohlenhydrate (DE-588)4164517-0 gnd Kapillarelektrophorese (DE-588)4290002-5 gnd |
| subject_GND | (DE-588)4164517-0 (DE-588)4290002-5 |
| title | Analysis of carbohydrates by capillary electrophoresis |
| title_auth | Analysis of carbohydrates by capillary electrophoresis |
| title_exact_search | Analysis of carbohydrates by capillary electrophoresis |
| title_full | Analysis of carbohydrates by capillary electrophoresis Aran Paulus ; Antje Klockow-Beck |
| title_fullStr | Analysis of carbohydrates by capillary electrophoresis Aran Paulus ; Antje Klockow-Beck |
| title_full_unstemmed | Analysis of carbohydrates by capillary electrophoresis Aran Paulus ; Antje Klockow-Beck |
| title_short | Analysis of carbohydrates by capillary electrophoresis |
| title_sort | analysis of carbohydrates by capillary electrophoresis |
| topic | Capillary electrophoresis Carbohydrates Analysis Kohlenhydrate (DE-588)4164517-0 gnd Kapillarelektrophorese (DE-588)4290002-5 gnd |
| topic_facet | Capillary electrophoresis Carbohydrates Analysis Kohlenhydrate Kapillarelektrophorese |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=008340325&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| volume_link | (DE-604)BV011568238 |
| work_keys_str_mv | AT paulusaran analysisofcarbohydratesbycapillaryelectrophoresis AT klockowbeckantje analysisofcarbohydratesbycapillaryelectrophoresis |