Modern techniques in raman spectroscopy:
Gespeichert in:
| Format: | Buch |
|---|---|
| Sprache: | English |
| Veröffentlicht: |
Chichester [u.a.]
Wiley
1996
|
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | XVIII, 427 S. Ill., zahlr. graph. Darst. |
| ISBN: | 0471957747 |
Internformat
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Datensatz im Suchindex
| _version_ | 1809946424949866496 |
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MODERN TECHNIQUES IN RAMAN SPECTROSCOPY EDITED BY J.J. LASERNA
UNIVERSITY OF MALAGA, SPAIN JOHN WILEY & SONS CHICHESTER * NEW YORK *
BRISBANE * TORONTO * SINGAPORE CONTENTS LIST OF CONTRIBUTORS XV PREFACE
XVII CHAPTER 1 SIGNAL EXPRESSIONS IN RAMAN SPECTROSCOPY C.L. STEVENSON
AND T. VO-DINH 1 INTRODUCTION 1 2 THEORY: RAMAN SCATTERING INTENSITY 2
2.1 CLASSICAL THEORY OF LIGHT SCATTERING FROM MOLECULES 2 2.1.1 SCATTER
FROM ISOTROPIC MOLECULES 3 2.1.2 SCATTER FROM ANISOTROPIC MOLECULES 7
2.1.3 RAMAN SCATTER 12 2.2 QUANTUM-MECHANICAL THEORY OF LIGHT SCATTERING
FROM MOLECULES 16 2.3 SELECTION RULES FOR RAMAN SCATTER 19 2.4 ENHANCED
RAMAN SCATTERING 21 2.4.1 INTRODUCTION: RAMAN SCATTERING EFFICIENCY 21
2.4.2 RESONANCE RAMAN SCATTERING 22 2.4.3 SURFACE-ENHANCED RAMAN
SCATTERING (SERS) 23 3 MEASUREMENTS OF RAMAN SCATTER 26 3.1 THE
MEASUREMENT PROCESS 26 3.2 SIGNAL COLLECTION AND DETECTION 27 3.3
SIGNAL-TO-NOISE RATIO OF RAMAN MEASUREMENTS 30 3.4 SOURCES OF NOISE IN
RAMAN MEASUREMENTS 33 4 RAMAN INSTRUMENTATION: EFFECT ON S/N 35 5
CONCLUSIONS. 37 6 ACKNOWLEDGMENTS 37 7 REFERENCES 38 VI CONTENTS CHAPTER
2 INSTRUMENTATION FOR DISPERSIVE RAMAN SPECTROSCOPY R.L. MCCREERY 1
INTRODUCTION 41 2 RAMAN DETECTION PRINCIPLES 42 2.1 THE RAMAN DETECTION
PROBLEM 42 2.2 SIGNAL TO NOISE RATIO EXPRESSIONS 45 2.3 GENERAL DESIGN
CONSIDERATIONS 47 2.3.1 CHOICE OF LASER WAVELENGTH 47 2.3.2 DETECTOR
AREA 47 2.3.3 RESOLUTION/SPECTRAL COVERAGE TRADE-OFF 47 3
CHARACTERISTICS OF INSTRUMENT COMPONENTS 48 3.1. LASERS 48 3.2 SAMPLING
MODES AND COLLECTION OPTICS 51 3.2.1 THE 90 COLLECTION GEOMETRY 52
3.2.2 THE 180 GEOMETRY 53 3.2.3 FIBER OPTIC SAMPLING 54 3.3
SPECTROGRAPHS AND FILTERS 56 3.3.1 DOUBLE MONOCHROMATORS 56 3.3.2 TRIPLE
MONOCHROMATORS 57 3.3.3 SINGLE SPECTROGRAPHS 58 3.4 DETECTORS 59 4
CALIBRATION 61 4.1 FREQUENCY CALIBRATION 61 4.1.1 WAVELENGTH STANDARDS
62 4.1.2 RAMAN SHIFT STANDARDS 62 4.2 INTENSITY CALIBRATION 65 5 FT
RAMAN COMPARED WITH DISPERSIVE RAMAN 66 6 SUPPLIERS 70 7 REFERENCES 72
CHAPTER 3 FOURIER TRANSFORM RAMAN SPECTROSCOPY P.J. HENDRA 1
INTRODUCTION 73 2 EXPERIMENTAL ARRANGEMENTS 73 2.1 SAMPLING SYSTEMS 74
2.2 OPERATIONAL CONDITIONS 77 2.3 DATA PROCESSING AND LIBRARY SEARCHING
77 2.4 QUANTITATIVE RAMAN STUDIES 78 2.5 FT RAMAN MICROSCOPY 79 2.6
GASES 80 2.7 REMOTE SAMPLING 82 VII 2.8 ALTERNATIVE LASERS TO NDYAG 83 3
APPLICATIONS OF FOURIER TRANSFORM RAMAN SPECTROSCOPY 84 3.1 THE ANALYSIS
OF ORGANIC COMPOUNDS 84 3.2 POLYMERS 91 3.3 INORGANIC MATERIALS 93 3.4
SURFACES 96 3.4.1 CATALYSTS 97 3.4.2 TLC PLATES 100 3.4.3 METALLIC
SURFACES 100 3.5 BIOLOGICAL AND BIOMEDICAL APPLICATIONS 102 4
CONCLUSIONS 103 5 SOURCES OF INFORMATION 106 6 REFERENCES 106 CHAPTER 4
MICRO-RAMAN SPECTROSCOPY G. TURRELL AND P. DHAMELINCOURT 1 INTRODUCTION
109 2 INSTRUMENTAL CONSIDERATIONS 110 2.1 EXCITATION FOCUSING 110 2.2
COLLECTION OPTICS 112 2.3 POLARIZATION MEASUREMENTS 113 2.4 CONFOCAL
MICROSPECTROSCOPY 116 2.5 RAMAN IMAGING TECHNIQUES 120 2.5.1 BASIC
PRINCIPLES 120 2.5.2 VARIOUS MAPPING CONFIGURATIONS 121 2.5.3 CONFOCAL
RAMAN LINE-SCANNING IMAGING 123 2.5.4 MODES OF OPERATION 126 2.5.5
DIGITAL IMAGE RESTORATION 126 3 APPLICATIONS. 128 3.1 FILMS, SURFACES
AND ADSORBED SPECIES 128 3.1.1 GLANCING INCIDENCE 128 3.1.2 INTEGRATED
OPTICS 128 3.1.3 BACKSCATTERING GEOMETRY 132 3.2 MATERIALS SCIENCE 134
3.3 GEOLOGY AND ENVIRONMENT 135 3.3.1 GEOLOGY 135 3.3.2 ENVIRONMENT 136
3.4 BIOLOGY AND MEDICINE 136 3.5 THE ARTS 137 4 GONCLUSIONS 140 5
REFERENCES 140 VIII CONTENTS CHAPTER 5 HADAMARD TRANSFORM RAMAN
SPECTROMETRY R.M. HAMMAKER, A.P. BOEHLKE, R.D. FREEMAN, J.A. GRAHAM, J.M.
JARVIS, K.J. LATAS, D. LIN-VIEN, A.N. MORTENSEN, E.A. ORR, J.D. TAETE,
D.C. TILOTTA, J.S. WHITE, S.L. WRIGHT, J. V. PAUKSTELIS AND W.G. FATELEY
1 BACKGROUND 143 2 INTRODUCTION TO HTS 145 2.1 THE MULTIPLEX ADVANTAGE
145 2.2 A GENERIC DESCRIPTION OF HTS 146 2.3 AN EXAMPLE HTS SYSTEM 147
2.4 THE HADAMARD ENCODING MASK 150 2.4.1 THE FIRST GENERATION STATIONARY
HADAMARD ENCODING MASK 152 2.4.2 THE SECOND GENERATION STATIONARY
HADAMARD ENCODING MASK 152 2.5 COMPARISON OF FTS AND HTS FOR NIR RAMAN
SPECTROMETRY. . 155 3 VISIBLE HT RAMAN SPECTROMETRY 157 3.1 EXPERIMENTAL
157 3.1.1 THE OPTICAL DESIGN OF THE INSTRUMENT 157 3.1.2 THE
EXPERIMENTAL ARRANGEMENT 158 3.2 RESULTS 160 3.2.1 THE ENCODEGRAM AND
SPECTRUM 160 3.2.2 THE SPECTRAL OBSERVATION WINDOW AND RESOLUTION 160
3.2.3 THE EFFECT OF RAYLEIGH LINE REJECTION ON MULTIPLEXING. . 163 3.2.4
THE APPLICATION OF THE ENCODING MASK AS A TUNABLE FILTER 164 3.2.5 THE
MEASUREMENT OF DEPOLARIZATION RATIOS 165 3.2.6 SPECTRAL SUBTRACTION OF
LIQUIDS 166 4 THE FIRST GENERATION OF NIR HT RAMAN SPECTROMETRY 168 4.1
EXPERIMENTAL 168 4.1.1 CONVERSION FROM THE VISIBLE TO THE NIR SPECTRAL
REGION 168 4.1.2 DATA ACQUISITUM 168 4.2 RESULTS 169 4.2.1 SPECTRA AND
POLARIZATION EFFECTS 169 4.2.2 SPECTRAL SUBTRACTION OF SOLIDS 173 5 THE
SECOND GENERATION OF NIR HT RAMAN SPECTROMETRY 174 5.1 EXPERIMENTAL 175
5.1.1 CONVERSION FROM THE FIRST TO THE SECOND GENERATION OF NIR HT RAMAN
SPECTROMETRY 175 IX 5.1.2 A COMPARISON BETWEEN THE FIRST AND SECOND
GENERATION STATIONARY HADAMARD ENCODING MASKS 176 5.2 RESULTS 178 5.2.1
POLARIZATION EFFECTS 178 5.2.2 RESOLUTION 180 5.2.3 THE MULTIPLEX
ADVANTAGE 180 5.2.4 THE SELECTIVE MULTIPLEX ADVANTAGE 182 6 QUANTITATIVE
NIR HT RAMAN SPECTROMETRY IN THE ENCODEGRAM DOMAIN 184 6.1 INTRODUCTION
184 6.2 EXPERIMENTAL 186 6.3 RESULTS 187 7 STRATEGIES FOR DECREASING
DATA ACQUISITION TIME USING STATIONARY HADAMARD ENCODING MASKS 191 7.1
INTRODUCTION 191 7.2 CORRECTION OF THE ENCODEMENT MATRIX FOR TEMPORAL
SYSTEMATIC ERRORS RESULTING FROM FAILURE TO REACH EQUILIBRIUM 192 7.2.1
INTRODUCTION TO TEMPORAL SYSTEMATIC ERRORS 192 7.2.2 EXPERIMENTAL 196
7.2.3 RESULTS 196 7.3 USE OF ENCODING MASK TEMPERATURE FOR DECREASING
DATA ACQUISITION TIME USING ELECTRO-OPTIC HADAMARD ENCODING MASKS 203
7.3.1 INTRODUCTION 203 7.3.2 CHARACTERIZATION OF THE HEATED PDLC MASK
205 7.3.3 TESTING OF THE HEATED PDLC MASK 205 8 RAMAN IMAGING AS A FORM
OF MULTI-DIMENSIONAL SPECTROMETRY 208 8.1 INTRODUCTION TO
MULTI-DIMENSIONAL SPECTROMETRY 208 8.2 EXPERIMENTAL 211 8.2.1 THE 2D
STATIONARY HADAMARD ENCODING MASK 211 8.2.2 INSTRUMENT DESIGN FOR
VISIBLE HT RAMAN IMAGING . . 211 8.2.3 SPATIAL RESOLUTION 212 8.2.4
VISIBLE HT RAMAN IMAGING SAMPLE 213 8.2.5 IMAGE COLLECTION 213 8.3
VISIBLE HT RAMAN IMAGING 213 9 SOME SUGGESTIONS FOR THE FUTURE 217 10
ACKNOWLEDGMENTS 220 11 REFERENCES 221 12 APPENDIX: LIST OF ABBREVIATIONS
225 X CONTENTS CHAPTER 6 SURFACE-ENHANCED RAMAN SPECTROSCOPY A. RUPEREZ
AND J.J. LASERNA 1 INTRODUCTION 227 2 THEORETICAL BACKGROUND 228 2.1
ELECTROMAGNETIC MECHANISM 228 2.2 CHARGE TRANSFER MECHANISM 235 3 METAL
SUBSTRATES FOR SERS 240 4 INSTRUMENTAL DESIGNS SPECIFIC TO SERS 242 5
MOLECULAR RECOGNITION AND QUALITATIVE ANALYSIS APPLICATIONS 248 6
QUANTITATIVE ANALYSIS BY SERS 254 7 SERS IN FLOWING STREAMS: FLOW
INJECTION AND LIQUID CHROMATOGRAPHIC APPLICATIONS 259 8 CONCLUSIONS 261
9 REFERENCES 261 CHAPTER 7 RAMAN OPTICAL ACTIVITY L. HECHT AND L.D.
BARRON 1 INTRODUCTION 265 2 FUNDAMENTAL THEORY OF ROA 267 2.1 LIGHT
SCATTERING FROM CHIRAL MOLECULES 267 2.1.1 DISTINCTION BETWEEN OPTICAL
ROTATION AND ROA 267 2.1.2 THE POLARIZABILITY AND OPTICAL ACTIVITY
TENSORS 268 2.1.3 OPTICAL ROTATION IN ISOTROPIC AND ORIENTED SAMPLES. .
. . 269 2.1.4 THE ORIGIN OF ROA 270 2.2 THE ROA OBSERVABLES 270 2.3
VIBRATIONAL RAMAN TRANSITION TENSORS 273 2.4 THE BOND POLARIZABILITY
THEORY OF ROA 275 2.4.1 THE TWO-GROUP MODEL 275 2.4.2 A GENERAL BOND
POLARIZABILITY THEORY 277 2.4.3 POLARIZED ROA 279 2.4.4 BACKSCATTERED
ROA 279 2.5 AB INITIO CALCULATIONS 280 3 ROA INSTRUMENTATION 282 3.1
GENERAL ASPECTS 282 3.2 ARTEFACTS AND POLARIZED ROA MEASUREMENTS 283 3.3
BACKSCATTERING WITH CCD DETECTION: THE ULTIMATE ROA INSTRUMENT 284 3.4
THE CURRENT GLASGOW ROA INSTRUMENTS 285 4 RECENT EXPERIMENTAL STUDIES OF
NATURAL ROA . 288 4.1 TESTS OF THE BOND POLARIZABILITY THEORY 288 4.2
TESTS OF THE AB INITIO THEORY 292 CONTENTS XI 4.3 CHIRAL CRYSTALS 295
4.4 BIOLOGICAL MOLECULES 295 5 MAGNETIC ROA 298 6 ROA FROM CHIRAL
SURFACES 299 7 ACKNOWLEDGEMENTS 300 8 REFERENCES 300 CHAPTER 8 COHERENT
RAMAN SPECTROSCOPY J. SANTOS GOMEZ 1 INTRODUCTION 305 2 THEORY 307 2.1.1
TIME DOMAIN NONLINEAR RESPONSE FUNCTION 308 2.1.2 MACROSCOPIC NONLINEAR
SUSCEPTIBILITY 309 2.1.3 MONOCHROMATIC WAVES 310 2.1.4 SPATIAL SYMMETRY
313 2.1.5 QUASI-MONOCHROMATIC FIELDS 313 2.2 MICROSCOPIC DESCRIPTION OF
THE NONLINEAR SUSCEPTIBILITY 315 2.2.1 MICROSCOPIC EXPRESSIONS FOR THE
NONLINEAR SUSCEPTIBILITY 317 2.2.2 RAMAN RESONANCES IN THE NONLINEAR
SUSCEPTIBILITY . 320 2.3 NONLINEAR WAVE PROPAGATION 323 3 CRS
TECHNIQUES 326 3.1 ENERGY LEVEL DIAGRAMS 326 3.2 STIMULATED RAMAN GAIN
AND LOSS SPECTROSCOPIES 328 3.2.1 THE SRS EXPERIMENT 331 3.3 CARS 331
3.3.1 THE CARS EXPERIMENT 335 3.4 POLARIZATION VARIANTS 336 3.4.1 RIKES;
OHD-RIKES 336 3.4.2. POLARIZATION CARS; CARS ELLIPSOMETRY 337 4 SURVEY
OF APPLICATIONS 338 5 REFERENCES 340 CHAPTER 9 TIME-RESOLVED RESONANCE
RAMAN SPECTROSCOPY M.R. ONDRIAS, M. C. SIMPSON AND R. W. LARSEN 1
TRANSIENT AND TIME-RESOLVED RESONANCE RAMAN SPECTROSCOPY 343 1.1 GENERAL
PROTOCOLS FOR ULTRAFAST RESONANCE RAMAN STUDIES . 344 1.1.1 TRANSIENT
RESONANCE RAMAN (TRR) SPECTROSCOPY 344 1.1.2 TIME-RESOLVED RESONANCE
RAMAN (TRRR) SPECTROSCOPY 345 XII CONTENTS 2 INSTRUMENTATION FOR
TRANSIENT AND TIME-RESOLVED RESONANCE RAMAN SPECTROSCOPY. 345 2.1
EXCITATION SOURCES 346 2.1.1 NANOSECOND SYSTEMS 346 2.1.2 PICOSECOND
SYSTEMS 346 2.2 DISPERSION DEVICES 348 2.3 DETECTORS 349 3 TRANSIENT AND
TIME-RESOLVED RAMAN SPECTROMETERS: REPRESENTATIVE EXAMPLES 349 3.1
NANOSECOND INSTRUMENT 349 3.2 PICOSECOND INSTRUMENT 350 4 RECENT
ADVANCES IN TRANSIENT AND TIME-RESOLVED RAMAN INSTRUMENTATION 353 5
SELECTED APPLICATIONS OF TRANSIENT AND TIME-RESOLVED RAMAN SPECTROSCOPY
TO BIOPHYSICS AND CHEMISTRY 354 5.1 NANOSECOND PROCESSES 354 5.1.1
LIGATION DYNAMICS OF HEMOGLOBIN 354 5.1.2 DYNAMICS AND REACTIVITY OF
CHEMICALLY MODINED HUMAN HEMOGLOBIN 355 5.1.3 TRANSIENT AND
TIME-RESOLVED RESONANCE RAMAN SPECTROSCOPY OF RU(II)(L) 3 COMPLEXES 358
5.2 PICOSECOND PROCESSES 363 5.2.1 TIME-RESOLVED UV RESONANCE RAMAN OF
SMALL RING COMPOUNDS 363 5.2.2 TIME-RESOLVED STUDIES OF
BACTERIORHODOPSIN 366 5.2.3 SOLVENT-SOLUTE INTERACTIONS 368 5.2.4
EXCITED-STATE STRUCTURES OF METALLOPORPHYRINS AND HEMES 372 5.3
PICOSECOND PROCESSES WITH NANOSECOND PULSES 377 5.3.1 STEADY-STATE
MEASUREMENTS OF PICOSECOND-SCALE VIBRATIONAL ENERGY REDISTRIBUTIONS 378
6 SUMMARY 382 7 ACKNOWLEDGMENT 383 8 REFERENCES 383 CHAPTER 10
APPLICATIONS OF FIBER OPTICS IN NIR RAMAN SPECTROSCOPY SM. ANGEL, T.F.
COONEY AND H. T. SKINNER 1 INTRODUCTION 387 2 THE USE OF FIBER OPTICS
FOR RAMAN SPECTROSCOPY . 388 2.1 SETUP OF FIBER OPTIC REMOTE RAMAN
SPECTROMETER 388 CONTENTS XIII 2.2 FIBER OPTIC RAMAN PROBES 389 2.3
PROBLEMS ASSOCIATED WITH THE USE OF FIBER OPTICS FOR RAMAN SPECTROSCOPY
392 2.4 THEORETICAL PREDICTIONS OF FIBER OPTIC RAMAN PROBE PERFORMANCE
394 3 THE USE OF NEAR-INFRARED DIODE LASERS FOR RAMAN SPECTROSCOPY 404
3.1 MODE HOPPING 405 3.2 EXTERNAL CAVITY DIODE LASERS 406 4 REAL-WORLD
APPLICATIONS OF REMOTE RAMAN SPECTROSCOPY 408 4.1 POLYMER CURE
MONITORING 408 4.2 INDUSTRIAL CHEMICAL AND WASTE MONITORING 412 4.2.1
DISTILLATION MONITORING 412 4.2.2 IDENTIFICATION OF SOLVENT WASTES IN
GROUNDWATER AND SOIL 412 5 FUTURE DEVELOPMENTS 415 5.1 NON-POINT-SOURCE
RAMAN PROBES 415 5.2 ON-LINE DATA ANALYSIS 417 6 REFERENCES 417 INDEX
421 |
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| illustrated | Illustrated |
| indexdate | 2024-09-12T00:03:39Z |
| institution | BVB |
| isbn | 0471957747 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-007526939 |
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| spelling | Modern techniques in raman spectroscopy ed. by J. J. Laserna Chichester [u.a.] Wiley 1996 XVIII, 427 S. Ill., zahlr. graph. Darst. txt rdacontent n rdamedia nc rdacarrier Raman spectroscopy Technique Raman-Spektroskopie (DE-588)4176916-8 gnd rswk-swf Raman-Spektroskopie (DE-588)4176916-8 s DE-604 Laserna, Javier J. Sonstige (DE-588)1158344392 oth GBV Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=007526939&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Modern techniques in raman spectroscopy Raman spectroscopy Technique Raman-Spektroskopie (DE-588)4176916-8 gnd |
| subject_GND | (DE-588)4176916-8 |
| title | Modern techniques in raman spectroscopy |
| title_auth | Modern techniques in raman spectroscopy |
| title_exact_search | Modern techniques in raman spectroscopy |
| title_full | Modern techniques in raman spectroscopy ed. by J. J. Laserna |
| title_fullStr | Modern techniques in raman spectroscopy ed. by J. J. Laserna |
| title_full_unstemmed | Modern techniques in raman spectroscopy ed. by J. J. Laserna |
| title_short | Modern techniques in raman spectroscopy |
| title_sort | modern techniques in raman spectroscopy |
| topic | Raman spectroscopy Technique Raman-Spektroskopie (DE-588)4176916-8 gnd |
| topic_facet | Raman spectroscopy Technique Raman-Spektroskopie |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=007526939&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT lasernajavierj moderntechniquesinramanspectroscopy |