Flow injection analysis of pharmaceuticals: automation in the laboratory
Saved in:
| Main Author: | |
|---|---|
| Format: | Book |
| Language: | English |
| Published: |
London [u.a.]
Taylor & Francis
1996
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| Series: | The Taylor & Francis series in pharmaceutical sciences
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| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Physical Description: | XI, 394 S. graph. Darst. |
| ISBN: | 0748404457 |
Staff View
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Record in the Search Index
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| adam_text | . , R... / . -** . FLOW INJECTION ANALYSIS OF PHARMACEUTICALS
AUTOMATION IN THE LABORATORY PROFESSOR JOSE MARTINEZ CALATAYUD PROFESSOR
OF ANALYTICAL CHEMISTRY AND HEAD OF COLLEGE OF PHARMACY - CEU UNIVERSITY
OF VALENCIA SPAIN TAYLOR &FRANCIS J PUBLISHERS SINCE 1798 CONTENTS
PREFACE PAGE XI PART ONE INTRODUCTION 1 1 AUTOMATION IN THE ANALYTICAL
LABORATORY 3 1.1 FUNDAMENTALS AND OBJECTIVES OF ANALYTICAL AUTOMATION 3
1.2 DISCRETE OR BATCH METHODS 6 1.3 FLOW METHODS 6 1.4 ROBOTS IN THE
ANALYTICAL PROCESS 10 1.5 CONCLUDING REMARKS 16 1.6 A BRIEF HISTORY OF
FIA DEFINITIONS 17 PART TWO FLOW INJECTION ANALYSIS 23 2 FUNDAMENTALS OF
FLOW INJECTION ANALYSIS 25 2.1 FIA TRANSIENT SIGNALS 25 2.2 THEORETICAL
BACKGROUND: DISPERSION OF A SOLUTE IN A FLOWING STREAM 26 2.3 EMPIRICAL
ASSESSMENT OF THE SAMPLE DISPERSION 31 2.4 OPTIMIZATION OF AN FIA SYSTEM
38 2.5 USE OF FIA SIGNALS 4(1 3 ESSENTIAL ELEMENTS OF AN FIA ASSEMBLY 49
3.1 INTRODUCTION 49 3.2 THE PROPULSION SYSTEM 49 3.3 THE SAMPLE
INTRODUCTION SYSTEM 54 3.4 THE DETECTION SYSTEM 60 4 FIA MODES 71 4.1
MULTI-DETERMINATIONS (AND SPECIATION) IN FIA 71 4.2 REVERSED FIA 79
CONTENTS 4.3 MINIATURE SYSTEMS 80 4.4 MONITORING INDUSTRIAL PROCESSES 82
4.5 DIALYSIS: MEMBRANE SEPARATION 85 4.6 TREATMENT OF SAMPLES FOR THEIR
ANALYTICAL MEASUREMENT 90 4.7 GASES IN FIA REACTIONS AND ASSEMBLIES 100
PART THREE DETECTION BASED ON THE INTERACTION BETWEEN RADIANT ENERGY AND
MATTER 113 5 ABSORPTION IN THE UV-VISIBLE REGION 115 5.1 GENERAL
FEATURES 115 5.2 FIA MULTI-DETERMINATIONS 119 5.3 FIA-MOLECULAR
ABSORPTION SPECTROSCOPIC APPLICATION TO PHARMACEUTICAL ANALYSIS: AN
OVERVIEW 121 5.4 OTHER FIA MODES 134 5.5 LIGHT SCATTERING
(TURBIDIMETRIC) METHODS 135 5.6 DISSOLUTION TESTS FOR PHARMACEUTICAL
FORMULATIONS 137 6 INFRARED ABSORPTION 147 6.1 GENERAL FEATURES 147 6.2
APPLICATION OF FIA-IR SPECTROSCOPY TO DRUG ANALYSIS 149 7 FLUORIMETRY
151 7.1 GENERAL FEATURES 151 7.2 LASER FLUORIMETRY 153 7.3 INFLUENCE OF
THE MOLECULAR ENVIRONMENT: SOLVENTS, MICELLAR MEDIA AND SOLID PHASES 154
7.4 FIA FLUORIMETRY IN DRUG ANALYSIS 158 8 CHEMILUMINESCENCE 171 8.1
INTRODUCTION 171 8.2 BASIC CHEMILUMINESCENCE SYSTEMS 172 8.3 ANALYTICAL
PROCEDURES 179 8.4 APPLICATIONS TO PHARMACEUTICAL ANALYSIS 183 9
PHOTOCHEMICAL REACTIONS 203 9.1 INTRODUCTION 203 9.2 GENERAL FEATURES OF
THE LIGHT SOURCE 204 9.3 ANALYTICAL APPLICATIONS 204 9.4 MATERIALS AND
DESIGNS IN FIA PHOTOCHEMICAL SYSTEMS 206 9.5 EXPERIMENTAL VARIABLES 210
9.6 CHEMICAL VARIABLES 214 9.7 REACTION MECHANISMS 216 9.8 DETERMINATION
OF DRUGS IN PHARMACEUTICAL PREPARATIONS 218 9.9 FORESEEABLE TRENDS 218
10 ATOMIC ABSORPTION SPECTROMETRY 223 10.1 GENERAL CONSIDERATIONS 223
10.2 PRACTICAL PROCEDURES IN PHARMACEUTICAL ANALYSIS 228 VIII CONTENTS
PART FOUR HETEROGENEOUS SYSTEMS 239 11 LIQUID-LIQUID EXTRACTION 241 11.1
GENERAL REMARKS 241 11.2 ELEMENTS OF LIQUID-LIQUID EXTRACTION SYSTEM 242
11.3 DETECTORS 254 11.4 TYPES OF FIA EXTRACTION SYSTEM: DETERMINATION OF
PHARMACEUTICALS 255 12 SOLID-PHASE REACTORS 263 12.1 INTRODUCTION 263
12.2 FEATURES OF IMMOBILIZED REAGENTS AND SUPPORTS 264 12.3 PERFORMANCE
CHARACTERISTICS OF SOLID-PHASE REACTORS 265 12.4 ANALYTICAL FUNCTION OF
THE SOLID-PHASE REACTOR AND LOCATION IN THE FIA ASSEMBLY 266 12.5
STRATEGIES FOR THE IMMOBILIZATION OF REAGENTS 277 12.6 FUTURE TRENDS 282
PART FIVE ELECTROANALYTICAL METHODS 289 13 FUNDAMENTALS OF
ELECTROANALYTICAL MEASUREMENT: CONDUCTIMETRY AND COULOMETRY 291 13.1
INTRODUCTION 291 13.2 CONTINUOUS-FLOW MEASUREMENTS 292 13.3
CONDUCTIMETRY 293 13.4 COULOMETRY 293 14 POTENTIOMETRY 299 299 300 301
306 310 15 VOLTAMMETRY (POLAROGRAPHY) AND AMPEROMETRY 313 15.1
INTRODUCTION 313 15.2 ELECTRODES 314 15.3 FIA ASSEMBLIES 329 15.4
CONTINUOUS-FLOW VOLTAMMETRY 330 15.5 CONTINUOUS-FLOW AMPEROMETRY 333
15.6 POLAROGRAPHY 341 PART SIX BIOCHEMICAL METHODS 351 16 FLOW
INJECTION-ENZYMATIC ANALYSIS 353 16.1 INTRODUCTION 353 16.2 ENZYMES IN
CONTINUOUS-FLOW SYSTEMS 354 16.3 DISSOLVED ENZYME SYSTEMS 355 16.4
IMMOBILIZED ENZYME SYSTEMS 356 IX POTENTIOMETRY 14. 14. 14. 14. 14. .1
.2 ,3 .4 ,5 INTRODUCTION CELLS ELECTRODES APPLICATIONS TO PHARMACEUTICAL
ANALYSIS CONCLUSIONS CONTENTS 16.5 USE OF IMMOBILIZED ENZYME REACTORS
FOR DETERMINING SUBSTRATES OF PHARMACEUTICAL INTEREST 363 17
IMMUNOASSAYS 373 17.1 INTRODUCTION 373 17.2 COMPETITIVE BINDING
IMMUNOANALYTICAL TECHNIQUES 374 17.3 FLOW INJECTION IMMUNOASSAY
TECHNOLOGY 376 INDEX 385
|
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| callnumber-first | R - Medicine |
| callnumber-label | RS189 |
| callnumber-raw | RS189.5.F56 |
| callnumber-search | RS189.5.F56 |
| callnumber-sort | RS 3189.5 F56 |
| callnumber-subject | RS - Pharmacy |
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| dewey-full | 615/.1901 |
| dewey-hundreds | 600 - Technology (Applied sciences) |
| dewey-ones | 615 - Pharmacology and therapeutics |
| dewey-raw | 615/.1901 |
| dewey-search | 615/.1901 |
| dewey-sort | 3615 41901 |
| dewey-tens | 610 - Medicine and health |
| discipline | Chemie / Pharmazie Medizin |
| format | Book |
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| illustrated | Illustrated |
| indexdate | 2024-07-09T18:04:31Z |
| institution | BVB |
| isbn | 0748404457 |
| language | English |
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| physical | XI, 394 S. graph. Darst. |
| publishDate | 1996 |
| publishDateSearch | 1996 |
| publishDateSort | 1996 |
| publisher | Taylor & Francis |
| record_format | marc |
| series2 | The Taylor & Francis series in pharmaceutical sciences |
| spelling | Martínez Calatayud, José Verfasser aut Flow injection analysis of pharmaceuticals automation in the laboratory José Martínez Calatayud London [u.a.] Taylor & Francis 1996 XI, 394 S. graph. Darst. txt rdacontent n rdamedia nc rdacarrier The Taylor & Francis series in pharmaceutical sciences Drugs Analysis Flow Injection Analysis methods Flow injection analysis Pharmaceutical Preparations analysis Automation (DE-588)4003957-2 gnd rswk-swf Pharmazeutische Analyse (DE-588)4174139-0 gnd rswk-swf Fließinjektionsanalyse (DE-588)4154671-4 gnd rswk-swf Fließinjektionsanalyse (DE-588)4154671-4 s Pharmazeutische Analyse (DE-588)4174139-0 s Automation (DE-588)4003957-2 s DE-604 GBV Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=007460130&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Martínez Calatayud, José Flow injection analysis of pharmaceuticals automation in the laboratory Drugs Analysis Flow Injection Analysis methods Flow injection analysis Pharmaceutical Preparations analysis Automation (DE-588)4003957-2 gnd Pharmazeutische Analyse (DE-588)4174139-0 gnd Fließinjektionsanalyse (DE-588)4154671-4 gnd |
| subject_GND | (DE-588)4003957-2 (DE-588)4174139-0 (DE-588)4154671-4 |
| title | Flow injection analysis of pharmaceuticals automation in the laboratory |
| title_auth | Flow injection analysis of pharmaceuticals automation in the laboratory |
| title_exact_search | Flow injection analysis of pharmaceuticals automation in the laboratory |
| title_full | Flow injection analysis of pharmaceuticals automation in the laboratory José Martínez Calatayud |
| title_fullStr | Flow injection analysis of pharmaceuticals automation in the laboratory José Martínez Calatayud |
| title_full_unstemmed | Flow injection analysis of pharmaceuticals automation in the laboratory José Martínez Calatayud |
| title_short | Flow injection analysis of pharmaceuticals |
| title_sort | flow injection analysis of pharmaceuticals automation in the laboratory |
| title_sub | automation in the laboratory |
| topic | Drugs Analysis Flow Injection Analysis methods Flow injection analysis Pharmaceutical Preparations analysis Automation (DE-588)4003957-2 gnd Pharmazeutische Analyse (DE-588)4174139-0 gnd Fließinjektionsanalyse (DE-588)4154671-4 gnd |
| topic_facet | Drugs Analysis Flow Injection Analysis methods Flow injection analysis Pharmaceutical Preparations analysis Automation Pharmazeutische Analyse Fließinjektionsanalyse |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=007460130&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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