Spectroscopic methods in organic chemistry:
Saved in:
| Main Authors: | , , |
|---|---|
| Format: | Book |
| Language: | German English |
| Published: |
Stuttgart [u.a.]
Thieme
1997
|
| Series: | Thieme foundations of organic chemistry series
|
| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Physical Description: | VIII, 365 S. graph. Darst. |
| ISBN: | 3131060417 3131060611 0865776679 0865776687 |
Staff View
MARC
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| 100 | 1 | |a Hesse, Manfred |d 1935-2011 |e Verfasser |0 (DE-588)101805281X |4 aut | |
| 240 | 1 | 0 | |a Spektroskopische Methoden in der organischen Chemie |
| 245 | 1 | 0 | |a Spectroscopic methods in organic chemistry |c Manfred Hesse ; Herbert Meier ; Bernd Zeeh |
| 264 | 1 | |a Stuttgart [u.a.] |b Thieme |c 1997 | |
| 300 | |a VIII, 365 S. |b graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 490 | 0 | |a Thieme foundations of organic chemistry series | |
| 650 | 7 | |a Espectroscopia |2 larpcal | |
| 650 | 7 | |a Organische verbindingen |2 gtt | |
| 650 | 7 | |a Spectrometrie |2 gtt | |
| 650 | 4 | |a Organic compounds |x Analysis | |
| 650 | 4 | |a Spectrum analysis | |
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Record in the Search Index
| _version_ | 1815597405806002176 |
|---|---|
| adam_text |
CONTENTS
CHAPTER
1
YY
:
UWVIS
SPECTROSCOPY
.
.
I
1.
THEORETICAL
INTRODUCTION.
1
1.1
ELECTRONIC
TRANSITIONS
.
1
1.2
LIGHT
ABSORPTION
AND
THE
SPECTRUM
.
4
2.
SAMPLE
PREPARATION
AND
MEASUREMENT
OF
SPECTRA
.
7
3.
CHROMOPHORES
.
9
3.1
INDIVIDUAL
CHROMOPHORIC
GROUPS
AND
THEIR
INTERACTIONS
.
9
3.2
OLEFINS,
POLYENES
.
10
3.3
BENZENE
AND
BENZENOID
AROMATICS
.
14
3.4
CARBONYL
COMPOUNDS
.
17
4.
APPLICATIONS
OF
UV/VIS
SPECTROSCOPY
.
20
5.
DERIVATIVE
SPECTROSCOPY
.
22
6.
CHIROOPTICAL
METHODS
.
22
LITERATURE
.
26
CHAPTER
2
INFRARED
AND
RAMAN
SPECTROSCOPY
.
29
1.
INTRODUCTION
.
29
2.
BASIC
PRINCIPLES
AND
SELECTION
RULES
.
30
3.
IR
SPECTROMETERS
.
32
3.1
CLASSICAL
(SCANNING)
IR
SPECTROMETERS
.
32
3.2
FOURIER-TRANSFORM
IR
SPECTROMETERS
.
33
4.
SAMPLE
PREPARATION
.
34
4.1
MEASUREMENTS
IN
THE
GAS
PHASE
.
34
4.2
MEASUREMENTS
ON
LIQUIDS
.
35
4.3
MEASUREMENTS
IN
SOLUTION
.
35
4.4
MEASUREMENTS
IN
THE
SOLID
STATE
.
35
5.
THE
IR
SPECTRUM
.36
6.
OVERVIEW
OF
CHARACTERISTIC
ABSORPTIONS
.
40
7.
IR
ABSORPTIONS
OF
SINGLE
BONDS
TO
HYDROGEN
.
44
7.1
C-H
ABSORPTIONS
.
44
7.2
(O-H)
AND
(N-H)
ABSORPTIONS
.
45
8.
IR
ABSORPTIONS
OF
TRIPLE
BONDS
AND
CUMULATED
DOUBLE
BONDS
.
47
9.
IR
ABSORPTIONS
OF
DOUBLE
BONDS
.
48
10.
TYPICAL
IR
ABSORPTIONS
OF
AROMATIC
COMPOUNDS
.
52
11.
IR
ABSORPTIONS
IN
THE
FINGERPRINT
REGION
.
53
12.
EXAMPLES
OF
IR
SPECTRA
.
55
13.
INFORMATION
TECHNOLOGY
AS
AN
AID
TO
IR
SPECTROSCOPY
.
65
14.
QUANTITATIVE
IR
SPECTROSCOPY
.
65
15.
RAMAN
SPECTROSCOPY
.
66
15.1
THE
RAMAN
EFFECT
.
66
15.2
SELECTION
RULES
.
67
15.3
RAMAN
SPECTROMETERS
.
69
15.4
APPLICATIONS
.
69
LITERATURE
.
70
CHAPTER
3
NUCLEAR
MAGNETIC
RESONANCE
SPECTROSCOPY
.
71
1.
FUNDAMENTAL
PHYSICAL
PRINCIPLES
.
71
1.1
THE
RESONANCE
PHENOMENON
.
71
1.2
CHEMICAL
SHIFT
.
73
1.3
SPIN-SPIN
COUPLING
.
74
1.4
LINE
WIDTHS
.
83
1.5
INTENSITY
.
84
2.
NMR
SPECTRA
AND
MOLECULAR
STRUCTURE
.
86
2.1
MOLECULES
WITH
"
RIGID
"
ATOMIC
POSITIONS
.
86
2.2
INTRAMOLECULAR
MOTION
.
88
2.3
CHEMICAL
EXCHANGE
PROCESSES
.
95
3.
*H
NMR
SPECTROSCOPY
.
100
3.1
SAMPLE
PREPARATION
AND
MEASUREMENT
OF
SPECTRA
(CW
AND
PFT
TECHNIQUES)
.
100
3.2
'H
CHEMICAL
SHIFTS
.
103
3.3
'H,
*H
COUPLING
.
106
3.4
COUPLING
TO
OTHER
NUCLEI
.
112
3.5
CORRELATION
OF
*H
SHIFTS
WITH
STRUCTURAL
FEATURES
.
113
3.6
INCREMENT
SYSTEMS
FOR
ESTIMATING
'
H
SHIFTS
.
121
3.7
'
H
NMR
DATA
OF
REPRESENTATIVES
OF
THE
COMMONER
CLASSES
OF
COMPOUNDS
.
124
3.8
SPECIALISED
TECHNIQUES
.
124
4.
13
C
NMR
SPECTROSCOPY
.
142
4.1
SAMPLE
PREPARATION
AND
MEASUREMENT
OF
SPECTRA
.
142
4.2
13
C
CHEMICAL
SHIFTS
.
145
4.3
13
C,
*H
COUPLINGS
.
149
4.4
COUPLING
OF
13
C
TO
OTHER
NUCLEI
(D,
F,
N,
P)
.
152
4.5
13
C,
13
C
COUPLINGS
.
154
4.6
CORRELATION
OF
13
C
SHIFTS
WITH
STRUCTURAL
FEATURES
.
157
4.7
INCREMENT
SYSTEMS
FOR
THE
ESTIMATION
OF
13
C
SHIFTS
.
159
4.8
SPECIAL
METHODS
.
163
5.
*H
AND
13
C
NMR
DATA:
REPRESENTATIVE
EXEMPLES
OF
THE
MOST
IMPORTANT
CLASSES
OF
COMPOUNDS
.
185
6.
NMR
SPECTROSCOPY
OF
OTHER
NUCLEI
.
202
6.1
"
F
NMR
SPECTROSCOPY
.
202
6.2
31
P
NMR
SPECTROSCOPY
.
204
6.3
15
N
NMR
SPECTROSCOPY
.
208
6.4
OTHER
NUCLEI
.
214
LITERATURE
.
215
CHAPTER
4
MASS
SPECTRA
.
219
1.
INTRODUCTION.
219
2.
INSTRUMENTATION
AND
THE
RECORDING
OF
SPECTRA
.
220
2.1
THE
PRINCIPLE
OF
THE
MASS
SPECTROMETER
.
220
3.
FRAGMENTATION
OF
ORGANIC
COMPOUNDS.
222
4.
THE
MAIN
FRAGMENTATION
REACTIONS
OF
ORGANIC
COMPOUNDS
.
226
4.1
A-CLEAVAGE
.
226
4.2
BENZYL
AND
ALLYL
CLEAVAGE
.
232
4.3
THE
CLEAVAGE
OF
"
NON-ACTIVATED
"
BONDS
.
234
4.4
THE
RETRO
DIELS-ALDER
REACTION
(RDA
REACTION)
.
236
4.5
THE
MCLAFFERTY
REARRANGEMENT
.
240
4.6
THE
ONIUM
REACTION
.
241
4.7
LOSS
OF
CO
.
244
5.
THERMAL
REACTIONS
IN
THE
MASS
SPECTROMETER
.
246
5.1
THE
MOST
IMPORTANT
TYPES
OF
THERMAL
REACTIONS
.
246
5.2
RECOGNITION
OF
THERMAL
REACTIONS
.
249
5.3
PREVENTION
OF
THERMAL
REACTIONS
IN
THE
MASS
SPECTROMETER
.
250
6.
MASS
SPECTRA
OF
CONTAMINATED
SAMPLES
AND
MIXTURES
.
251
6.1
SOLVENT
.
252
6.2
FOREIGN
SUBSTANCES
IN
SOLVENTS
.
252
6.3
FOREIGN
SUBSTANCES
IN
REAGENTS
.
253
6.4
MATERIALS
FROM
LABORATORY
APPARATUS
.
253
6.5
CONTAMINANTS
FROM
THIN-LAYER
CHROMATOGRAPHY
PLATES
.
253
7.
ISOTOPIC
LABELLING
REACTIONS
.
254
7.1
H/D
EXCHANGE
REACTIONS
.
254
7.2
TRANSFORMATIONS
OF
FUNCTIONAL
GROUPS
UNDER
DEUTERATING
CONDITIONS
.
255
7.3
DETERMINATION
OF
THE
DEGREE
OF
LABELLING
.
256
8.
ADDITIONAL
METHODS
AND
CONCEPTS
.
258
8.1
CHEMICAL
IONISATION
(CI)
.
258
8.2
DIRECT
CHEMICAL
IONISATION
(DCI)
.
259
8.3
ELECTROSPRAY
IONISATION
(ESI)
.
259
8.4
FAST
ATOM
BOMBARDMENT
(FAB)
.
260
8.5
FIELD
DESORPTION
(FD)
.
261
8.6
FIELD
IONISATION
(FI)
.
261
8.7
FIELD
IONISATION
KINETIC
(FIK)
.
261
8.8
MEASUREMENT
OF
HIGH
MASSES
.
261
VIII
CONTENTS
8.9
IONIZATION
METHODS
.
263
8.10
CATION
ADDITION
MASS
SPECTROSCOPY
.
265
8.11
THE
COUPLING
OF
OTHER
INSTRUMENTS
TO
MASS
SPECTROMETERS
.
266
8.12
LASER
DESORPTION
I
IONISATION
MASS
SPECTROMETRY
(LDI)
.
268
8.13
MULTIPLY
CHARGED
IONS
.
268
8.14
THE
MEMORY
EFFECT
.
269
8.15
NEIGHBOURING
GROUP
PARTICIPATION
REACTIONS
.
269
8.16
PHOTOIONISATION
(PI)
.
272
8.17
QUADRUPOLE
MASS
ANALYSERS
.
272
8.18
SECONDARY
ION
MASS
SPECTROMETRY
(SIMS)
.
273
8.19
SPECTRAL
LIBRARIES
.
273
8.20
STEREOISOMERS
.
273
8.21
COLLISION
ACTIVATION
(CA)
.
274
8.22
TANDEM
MASS
SPECTROMETRY
.
275
8.23
THERMAL
DESORPTION
MASS
SPECTROMETRY
(TD)
.
277
8.24
THE
THERMOSPRAY
IONISATION
PROCEDURE
(TSI)
.
277
8.25
METASTABLE
SIGNALS
.
277
9.
TABLES
FOR
USE
IN
MASS
SPECTROMETRY
.
279
9.1
LIST
OF
FREQUENTLY
OCCURRING
IONS
AND
CHARACTERISTIC
MASS
DIFFERENCES
RESULTING
FROM
MASS
SPECTROMETRIC
AND
CHEMICAL
REACTIONS
.
279
9.2
MASS
DIFFERENCES
BETWEEN
THE
REACTANT
AND
PRODUCT
OF
FREQUENTLY
USED
CHEMICAL
REACTIONS
.
292
9.3
ISOTOPIC
RATIOS
IN
COMPOUNDS
CONTAINING
CLANDBR
.
294
9.4
MASS
SPECTRA
OF
SOLVENTS
.
297
9.5
MASS
SPECTRA
OF
VOLATILE
CONTAMINANTS
.
301
9.6
MASS
NUMBERS
AND
ABUNDANCES
OF
THE
ISOTOPES
OF
NATURALLY
OCCURRING
ELEMENTS
.
304
LITERATURE
.
307
CHAPTER
5
;
COMBINED
EXAMPLES
.
313
INDEX
.
335
CONCEPTS
.
335
TYPES
OF
COMPOUNDS
AND
FUNCTIONAL
GROUPS
.
342
SPECIFIC
COMPOUNDS
.
352 |
| any_adam_object | 1 |
| author | Hesse, Manfred 1935-2011 Meier, Herbert 1939- Zeeh, Bernd |
| author_GND | (DE-588)101805281X (DE-588)13810817X |
| author_facet | Hesse, Manfred 1935-2011 Meier, Herbert 1939- Zeeh, Bernd |
| author_role | aut aut aut |
| author_sort | Hesse, Manfred 1935-2011 |
| author_variant | m h mh h m hm b z bz |
| building | Verbundindex |
| bvnumber | BV010897008 |
| callnumber-first | Q - Science |
| callnumber-label | QD272 |
| callnumber-raw | QD272.S6 |
| callnumber-search | QD272.S6 |
| callnumber-sort | QD 3272 S6 |
| callnumber-subject | QD - Chemistry |
| classification_rvk | VG 8900 VG 8901 VK 5661 |
| ctrlnum | (OCoLC)35280639 (DE-599)BVBBV010897008 |
| dewey-full | 547.3/0858 |
| dewey-hundreds | 500 - Natural sciences and mathematics |
| dewey-ones | 547 - Organic chemistry |
| dewey-raw | 547.3/0858 |
| dewey-search | 547.3/0858 |
| dewey-sort | 3547.3 3858 |
| dewey-tens | 540 - Chemistry and allied sciences |
| discipline | Chemie / Pharmazie |
| format | Book |
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| genre | 1\p (DE-588)4123623-3 Lehrbuch gnd-content |
| genre_facet | Lehrbuch |
| id | DE-604.BV010897008 |
| illustrated | Illustrated |
| indexdate | 2024-11-13T09:03:33Z |
| institution | BVB |
| isbn | 3131060417 3131060611 0865776679 0865776687 |
| language | German English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-007287783 |
| oclc_num | 35280639 |
| open_access_boolean | |
| owner | DE-29T DE-703 DE-19 DE-BY-UBM DE-634 DE-11 DE-188 |
| owner_facet | DE-29T DE-703 DE-19 DE-BY-UBM DE-634 DE-11 DE-188 |
| physical | VIII, 365 S. graph. Darst. |
| publishDate | 1997 |
| publishDateSearch | 1997 |
| publishDateSort | 1997 |
| publisher | Thieme |
| record_format | marc |
| series2 | Thieme foundations of organic chemistry series |
| spelling | Hesse, Manfred 1935-2011 Verfasser (DE-588)101805281X aut Spektroskopische Methoden in der organischen Chemie Spectroscopic methods in organic chemistry Manfred Hesse ; Herbert Meier ; Bernd Zeeh Stuttgart [u.a.] Thieme 1997 VIII, 365 S. graph. Darst. txt rdacontent n rdamedia nc rdacarrier Thieme foundations of organic chemistry series Espectroscopia larpcal Organische verbindingen gtt Spectrometrie gtt Organic compounds Analysis Spectrum analysis Organische Chemie (DE-588)4043793-0 gnd rswk-swf Organische Verbindungen (DE-588)4043816-8 gnd rswk-swf Spektroskopie (DE-588)4056138-0 gnd rswk-swf 1\p (DE-588)4123623-3 Lehrbuch gnd-content Organische Verbindungen (DE-588)4043816-8 s Spektroskopie (DE-588)4056138-0 s DE-604 Organische Chemie (DE-588)4043793-0 s 2\p DE-604 Meier, Herbert 1939- Verfasser (DE-588)13810817X aut Zeeh, Bernd Verfasser aut DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=007287783&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis 1\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk 2\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk |
| spellingShingle | Hesse, Manfred 1935-2011 Meier, Herbert 1939- Zeeh, Bernd Spectroscopic methods in organic chemistry Espectroscopia larpcal Organische verbindingen gtt Spectrometrie gtt Organic compounds Analysis Spectrum analysis Organische Chemie (DE-588)4043793-0 gnd Organische Verbindungen (DE-588)4043816-8 gnd Spektroskopie (DE-588)4056138-0 gnd |
| subject_GND | (DE-588)4043793-0 (DE-588)4043816-8 (DE-588)4056138-0 (DE-588)4123623-3 |
| title | Spectroscopic methods in organic chemistry |
| title_alt | Spektroskopische Methoden in der organischen Chemie |
| title_auth | Spectroscopic methods in organic chemistry |
| title_exact_search | Spectroscopic methods in organic chemistry |
| title_full | Spectroscopic methods in organic chemistry Manfred Hesse ; Herbert Meier ; Bernd Zeeh |
| title_fullStr | Spectroscopic methods in organic chemistry Manfred Hesse ; Herbert Meier ; Bernd Zeeh |
| title_full_unstemmed | Spectroscopic methods in organic chemistry Manfred Hesse ; Herbert Meier ; Bernd Zeeh |
| title_short | Spectroscopic methods in organic chemistry |
| title_sort | spectroscopic methods in organic chemistry |
| topic | Espectroscopia larpcal Organische verbindingen gtt Spectrometrie gtt Organic compounds Analysis Spectrum analysis Organische Chemie (DE-588)4043793-0 gnd Organische Verbindungen (DE-588)4043816-8 gnd Spektroskopie (DE-588)4056138-0 gnd |
| topic_facet | Espectroscopia Organische verbindingen Spectrometrie Organic compounds Analysis Spectrum analysis Organische Chemie Organische Verbindungen Spektroskopie Lehrbuch |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=007287783&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT hessemanfred spektroskopischemethodeninderorganischenchemie AT meierherbert spektroskopischemethodeninderorganischenchemie AT zeehbernd spektroskopischemethodeninderorganischenchemie AT hessemanfred spectroscopicmethodsinorganicchemistry AT meierherbert spectroscopicmethodsinorganicchemistry AT zeehbernd spectroscopicmethodsinorganicchemistry |