High-speed countercurrent chromatography:
Gespeichert in:
| Format: | Buch |
|---|---|
| Sprache: | English |
| Veröffentlicht: |
New York [u.a.]
Wiley
1996
|
| Schriftenreihe: | Chemical analysis
132 |
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | XXIII, 454 S. Ill., graph. Darst. |
| ISBN: | 0471637491 |
Internformat
MARC
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Datensatz im Suchindex
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| adam_text | HIGH-SPEED COUNTERCURRENT CHROMATOGRAPHY EDITED BY YOICHIRO ITO
LABORATORY OF BIOPHYSICAL CHEMISTRY NATIONAL INSTITUTES OF HEALTH
BETHESDA, MARYLAND WALTER D. CONWAY DEPARTMENT OF PHARMACEUTICS SUNY
BUFFALO BUFFALO, NEW YORK A WILEY-INTERSCIENCE PUBLICATION JOHN WILEY &
SONS NEW YORK / CHICHESTER / BRISBANE / TORONTO / SINGAPORE HIGH-SPEED
COUNTERCURRENT CHROMATOGRAPHY EDITED BY YOICHIRO ITO LABORATORY OF
BIOPHYSICAL CHEMISTRY NATIONAL INSTITUTES OF HEALTH BETHESDA, MARYLAND
WALTER D. CONWAY DEPARTMENT OF PHARMACEUTICS SUNY BUFFALO BUFFALO, NEW
YORK A WILEY-INTERSCIENCE PUBLICATION JOHN WILEY & SONS NEW YORK /
CHICHESTER / BRISBANE / TORONTO / SINGAPORE CONTENTS PREFACE XVII
CUMULATIVE LISTING OF VOLUMES IN SERIES XIX INSTRUMENTATION CHAPTER 1
PRINCIPLE, APPARATUS, AND METHODOLOGY OF HIGH-SPEED COUNTERCURRENT
CHROMATOGRAPHY 3 YOICHIRO ITO 1.1. INTRODUCTION 3 1.2. PRINCIPLE OF
HIGH-SPEED COUNTERCURRENT CHROMATOGRAPHY 5 1.2.1. TWO-PHASE DISTRIBUTION
IN A ROTATING COIL IN UNIT GRAVITY 5 1.2.2. FLOW-THROUGH COIL PLANET
CENTRIFUGE FREE OF ROTARY SEALS 11 1.2.3. MECHANISM OF HIGH-SPEED
COUNTERCURRENT CHRMATOGRAPHY 13 1.3. HIGH-SPEED COUNTERCURRENT
CHROMATOGRAPH INSTRUMENTATION 16 1.3.1. MULTILAYER COIL PLANET
CENTRIFUGE (TYPE J) 16 1.3.2. CROSS-AXIS SYNCHRONOUS FLOW-THROUGH COIL
PLANET CENTRIFUGE 22 1.4. PHASE DISTRIBUTION DIAGRAMS 26 1.4.1.
RETENTION OF STATIONARY PHASE IN TYPE J COIL PLANET CENTRIFUGE 28 1.4.2.
RETENTION OF STATIONARY PHASE IN CROSS- AXIS COIL PLANET CENTRIFUGES 31
1.4.3. SETTLINGTIME 34 1.5. GENERAL METHODOLOGY OF HIGH-SPEED
COUNTERCURRENT CHROMATOGRAPHY 36 1.5.1. PARTITION COEFFICIENT 36 1.5.2.
PREPARATION OF SAMPLE SOLUTION 39 VN VLLL CONTENTS 1.5.3. ELUTION 1.5.4.
DETECTION REFERENCES 40 41 42 CHAPTER 2 ANALYTICAL HIGH-SPEED
COUNTERCURRENT CHROMATOGRAPHY DANIEL E. SCHAUFELBERGER 2.1. INTRODUCTION
2.2. DEVELOPMENT OF ANALYTICAL HIGH-SPEED COUNTERCURRENT CHROMATOGRAPHY
2.3. THEORY 2.4. PRACTICAL CONSIDERATIONS 2.4.1. INSTRUMENTATION 2.4.2.
SOLVENT SYSTEMS 2.4.3. HANDLING 2.4.4. DETECTION 2.5. APPLICATIONS
2.5.1. METHODS DEVELOPMENT 2.5.2. MEASUREMENT OF PARTITION COEFFICIENTS
2.5.3. NATURAL PRODUCTS ISOLATION 2.6. DISCUSSION REFERENCES 45 45 45 46
51 51 56 56 57 60 60 62 63 66 68 SPECIAL TECHNIQUES CHAPTER 3 HIGH-SPEED
COUNTERCURRENT CHROMATOGRAPHY/MASS SPECTROMETRY 73 HISAO OKA 3.1.
INTRODUCTION 73 3.2. PREVIOUS INTERFACING OF HSCCC WITH THERMOSPRAY MASS
SPECTROMETRY 75 3.3. DIRECT INTERFACING OF HSCCC WITH FRIT ELECTRON
IONIZATION, CHEMICAL IONIZATION, AND FAST ATOM BOMBARDMENT MASS
SPECTROMETRY 75 3.4. HSCCC/FRITEIMSOFLNDOLEAUXINS 78 3.5. HSCCC/FRIT
CIMS OF MYCINAMICINS 80 3.6. HSCCC/FRIT FABMSOF COLISTIN COMPLEX 85 3.7.
CONCLUSION 90 REFERENCES 90 CONTENTS IX CHAPTER 5 CHAPTER 4 DUAL
COUNTERCURRENT CHROMATOGRAPHY 93 Y. W. LEE 4.1. INTRODUCTION 93 4.2.
PRINCIPLES AND MECHANISM 94 4.3. METHODS AND APPARATUS 95 4.4.
APPLICATIONS 97 4.5. CONCLUSION 104 REFERENCES 104 FOAM COUNTERCURRENT
CHROMATOGRAPHY OF BACITRACIN COMPLEX 107 HISAO OKA 5.1. INTRODUCTION 107
5.2. APPARATUS OF FOAM COUNTERCURRENT CHROMATOGRAPHY 108 5.3. PREVIOUS
FOAM COUNTERCURRENT CHROMATOGRAPHY WORK 109 5.4. SEPARATION OF
BACITRACIN COMPONENTS WITH NITROGEN AND ADDITIVE-FREE WATER 110 5.5.
CONTINUOUS ENRICHMENT AND STRIPPING OF BACITRACIN COMPONENTS 117 5.6.
CONCLUSION 118 REFERENCES 120 CHAPTER 6 PH-PEAK-FOCUSING AND PH-ZONE-
REFINING COUNTERCURRENT CHROMATOGRAPHY 121 YOICHIRO ITO 6.1.
INTRODUCTION 121 6.2. PH-PEAK-FOCUSING COUNTERCURRENT CHROMATOGRAPHY 121
6.2.1. RESEARCH FOR THE CAUSATIVE AGENT SHARPENING THE BRACT 3 PEAK 121
CHEMOHYDRODYNAMIC MECHANISM OF PH- PEAK-FOCUSING 126 ADVANCED
PEAK-FOCUSING TECHNIQUE 136 CONCLUSION 140 6.3. PH-ZONE-REFINING
COUNTERCURRENT CHROMATOGRAPHY 141 6.2.2. 6.2.3. 6.2.4. X CONTENTS 6.3.1.
CHARACTERISTIC FEATURES OF PH-ZONE- REFININGCCC 6.3.2. CHEMOHYDRODYNAMIC
MECHANISM OF PH-ZONE-REFINING CCC 6.3.3. SIMPLE MATHEMATICAL MODEL OF
PH- ZONE-REFINING CCC 6.3.4. DISPLACEMENT PH-ZONE-REFINING CCC 6.3.5.
PH-ZONE-REFINING CCC VERSU S DISPLACEMENT CHROMATOGRAPHY 6.3.6.
APPLICATIONS OF PH-ZONE-REFINING CCC 6.3.7. CONCLUSION REFERENCES 141
143 147 155 158 163 173 174 APPLICATIONS CHAPTER 7 HIGH-SPEED
COUNTERCURRENT CHROMATOGRAPHY OF NATURAL PRODUCTS 179 MARC MAILLARD,
ANDREW MARSTON, AND KURT HOSTETTMANN 7.1. INTRODUCTION 7.1.1.
INSTRUMENTS 7.1.2. SOLVENT SYSTEMS 7.2. PREPARATIVE APPLICATIONS 7.2.1.
FLAVONOIDS 7.2.2. XANTHONES 7.2.3. TANNINS 7.2.4. LIGNANS 7.2.5.
MONOTERPENE GLYCOSIDES 7.2.6. SAPONINS 7.2.7. ALKALOIDS 7.2.8.
CAROTENOIDS 7.2.9. GINGEROLS 7.2.10. POLYACETYLENIC ALCOHOLS 7.2.11.
MARINE NATURAL PRODUCTS 7.2.12. ANTIBIOTICS 7.3. ANALYTICAL APPLICATIONS
7.3.1. ALKALOIDS 7.3.2. ANTHRAQUINONES 7.3.3. COUMARINS 7.3.4.
FLAVONOIDS 179 181 184 189 190 195 195 198 200 202 203 204 204 205 206
210 211 212 215 215 215 CONTENTS XI 7.3.5. LIGNANS 216 7.3.6. MACROLIDES
216 7.3.7. TRITERPENOIDS 217 7.4. CONCLUSIONS 218 REFERENCES 218
HIGH-SPEED COUNTERCURRENT CHROMATOGRAPHY ON MEDICINAL HERBS 225 TIAN-
YOU ZHANG 8.1. INTRODUCTION 225 8.2. THE PRESENT STATUS OF HIGH-SPEED
COUNTERCURRENT CHROMATOGRAPHY ON ISOLATION OF MEDICINAL HERBS 226 8.3.
SEPARATIONS OF SUBSTANCES PREPARED FROM MEDICINAL HERBS BY THE
HORIZONTAL FLOW- THROUGH COIL PLANET CENTRIFUGE 227 8.3.1. APPARATUS AND
EXPERIMENTAL PROCEDURES 227 8.3.2. SEPARATIONS OF A GROUP OF SIMILAR
SUBSTANCES 228 8.3.3. STUDIES ON THE PREPARATIVE CAPABILITY OF CPC AND
HPLC IN THE SEPARATION OF POLAR COMPOUNDS 231 8.4. SEPARATION OF
ALKALOIDS, HYDROXYANTHRAQUINONES, AND FLAVONOIDS BY ANALYTICAL HSCCC 236
8.4.1. APPARATUS AND EXPERIMENTAL PROCEDURES 236 8.4.2. SEPARATION OF
ALKALOIDS EXTRACTED FROM STEPHANIA TETRANDA S. MOORE 236 8.4.3.
SEPARATION OF HYDROXYANTHRAQUINONE DERIVATIVES EXTRACTED FROM RHUBARB
240 8.4.4. RAPID SEPARATION OF FLAVONOIDS EXTRACTED FROM SEA BUCKTHORN
(HIPPOPHAE RHAMNOIDES) 242 8.5. SEPARATIONS OF FLAVONOIDS AND ALKALOIDS
BY MULTILAYER COIL SEPARATOR AND EXTRACTOR 245 8.5.1. APPARATUS AND
EXPERIMENTAL PROCEDURES 245 CONTENTS 8.5.2. SEPARATION OF DAPHNE GENKWA
FLAVONOIDS 247 8.5.3. SEPARATION OF FLAVONOIDS FROM CRUDE EXTRACTS OF
SEA BUCKTHORN (HIPPOPHAE RHAMNOIDES) 249 8.5.4. SEPARATION OF ALKALOIDS
FROM ANISODUS TANGULICUS (MAXIN) PASCH 250 8.6. SEMIPREPARATIVE
SEPARATION OF ALKALOIDS BY GS-10A HSCCC 252 8.6.1. APPARATUS AND
EXPERIMENTAL PROCEDURES 252 8.6.2. SEPARATION OF ALKALOIDS FROM SOPHORA
FLAVESCENS AIT AND DATURA METE L. 252 8.6.3. SEPARATION OF ALKALOIDS
FROM CEPHALOTAXUSFORTUNEI HOOK F. 255 8.6.4. SEPARATION OF ALKALOIDS
FROM SENECIO FUBERI HEMSL 256 8.6.5. SEPARATION OF VINCAMINE AND VINCINE
259 8.7. CONCLUSION 262 REFERENCES 263 CHAPTER 9 ISOLATION OF MARINE
NATURAL PRODUCTS BY HIGH-SPEED COUNTERCURRENT CHROMATOGRAPHY 265 NANCY
L. FREGEAU AND KENNETH L. RINEHART 9.1. INTRODUCTION 265 9.2.
ALTERNATIVE SEPARATION TECHNIQUES 267 9.3. COUNTERCURRENT CHROMATOGRAPHY
268 9.4. EXAMPLES OF MARINE NATURAL PRODUCT ISOLATIONS USING HIGH-SPEED
COUNTERCURRENT CHROMATOGRAPHY 268 9.4.1. MACROLIDES 269 9.4.2.
POLYETHERS 273 9.4.3. OTHER ACETATE-DERIVED METABOLITES 275 9.4.4.
TERPENES AND STEROIDS 276 9.4.5. PEPTIDES 278 9.4.6. NITROGEN-CONTAINING
HETEROCYCLES 280 9.5. CONCLUSION 296 REFERENCES 297 CONTENTS XLLL
CHAPTER 10 SEPARATION OF COMPLICATED ANTIBIOTICS BY HIGH-SPEED
COUNTERCURRENT CHROMATOGRAPHY 301 KEN-ICHI HARADA 10.1. INTRODUCTION 301
10.2. SELECTED ANTIBIOTICS 302 10.3. OPERATION OF HSCCC 304 10.4.
ESTABLISHMENT OF HPLC FOR SVD AND BC 304 10.5. SELECTION OF PROPER
TWO-PHASE SOLVENT SYSTEM 307 10.6. SEPARATION OF SVD AND BC COMPONENTS
BY HSCCC 314 10.7. COMPARISON OF ELUTION BEHAVIOR OF SVD AND BC BETWEEN
HPLC AND HSCCC 314 10.8. CONCLUSION 317 REFERENCES 318 CHAPTER 11
N-BROMOACETYL-3,3 5-TRIIODO-L- THYRONINE AND JV-BROMOACETYL-L-
THYROXINE: SYNTHESIS AND CHARACTERIZATION 321 HANS J. CAHNMANN 11.1.
11.2. 11.3. 11.4. 11.5. REFE INTRODUCTION SYNTHESIS 11.2.1. SYNTHESIS OF
BRACT 3 11.2.2. SYNTHESIS OF BRACT 4 PURIFICATION 11.3.1. HIGH-SPEED
COUNTERCURRENT CHROMATOGRAPHY 11.3.2. SOLVENTS 11.3.3. ELUTION 11.3.4.
ELUATE SCANNING 11.3.5. STORAGE OF HSCCC-PURIFIED BRACT 3 AND BRACT 4
VERIFICATION OF IDENTITY AND PURITY 11.4.1. HPLC 11.4.2. TLC 11.4.3.
ABSORPTION SPECTRA IN THE NEAR UV SUMMARY RENCES 321 322 324 325 326 326
328 330 330 330 331 331 331 333 334 335 XIV CONTENTS CHAPTER 12
SEPARATION AND PURIFICATION OF DYES BY CONVENTIONAL HIGH-SPEED
COUNTERCURRENT CHROMATOGRAPHY AND PH-ZONE-REFINING COUNTERCURRENT
CHROMATOGRAPHY 337 ADRIAN WEISZ 12.1. INTRODUCTION 337 12.2.
INSTRUMENTATION 338 12.3. CONVENTIONAL HSCCC SEPARATIONS 338 12.3.1.
SULFORHODAMINE B 338 12.3.2. TETRABROMOTETRACHLOROFLUORESCEIN AND
PHLOXINE B 340 12.3.3. COMPLEMENTARY USE OF HSCCC AND PREPARATIVE HPLC
IN THE SEPARATION OF A SYNTHETIC MIXTURE OF DYES 342 12.4.
PH-ZONE-REFINING COUNTERCURRENT CHROMATOGRAPHY 347 12.4.1. INTRODUCTION
347 12.4.2. PRINCIPLE 347 12.4.3. PRELIMINARY REQUIREMENTS FOR PH-
ZONE-REFINING CCC 350 12.4.4. PREPARATIVE SEPARATIONS OF BROMINATED AND
CHLORINATED FLUORESCEINS 352 12.4.5. PREPARATIVE SEPARATIONS OF
IODINATED FLUORESCEINS 375 12.5. CONCLUSIONS 381 REFERENCES 382 CHAPTER
13 SEPARATION OF PROTEINS BY HIGH-SPEED COUNTERCURRENT CHROMATOGRAPHY
385 YOICHI SHIBUSAWA 13.1. INTRODUCTION 385 13.2. APPARATUS 386 13.3.
POLYMER PHASE SYSTEMS FOR PROTEIN SEPARATION 391 13.4. COUNTERCURRENT
CHROMATOGRAPHY FRACTIONATION OF PROTEINS 391 13.4.1. PEG-POTASSIUM
PHOSPHATE SYSTEMS 391 13.4.2. PEG-DEXTRAN POLYMER PHASE SYSTEM 404 13.5.
CONCLUSION 412 REFERENCES 413 CONTENTS XV CHAPTER 14 SEPARATION OF RARE
EARTH AND CERTAIN INORGANIC ELEMENTS BY HIGH- SPEED COUNTERCURRENT
CHROMATOGRAPHY 415 EIICHI KITAZUME 14.1. INTRODUCTION 415 14.2.
SEPARATION OF RARE EARTH ELEMENTS BY HIGH- SPEED COUNTERCURRENT
CHROMATOGRAPHY 416 14.2.1. DESCRIPTION OF THE INSTRUMENT 416 14.2.2.
PREPARATION OF TWO-PHASE SOLVENT AND SAMPLE SOLUTIONS 419 14.2.3.
SEPARATION PROCEDURE 419 14.2.4. MEASUREMENT OF PARTITION COEFFICIENTS K
T AND K E 419 14.2.5. PARTITION EFFICIENCIES 422 14.2.6. GRADIENT
ELUTION OF FOURTEEN RARE EARTH ELEMENTS 426 14.3. ANALYTICAL CAPABILITY
OF HIGH-SPEED COUNTERCURRENT CHROMATOGRAPHY FOR RARE EARTH ELEMENTS 427
14.3.1. REPRODUCIBILITY OF CHROMATOGRAM 428 14.3.2. QUANTITATIVE
DETERMINATION OF CERIUM IMPURITIES IN ERBIUM CHLORIDE 430 14.4.
SEPARATION OF OTHER INORGANIC ELEMENTS BY HIGH-SPEED COUNTERCURRENT
CHROMATOGRAPHY 430 14.4.1. SEPARATION OF ORTHO-AND PYROPHOSPHATE IONS
431 14.4.2. SEPARATION OF CESIUM AND STRONTIUM 432 14.4.3. SEPARATION OF
ZIRCONIUM AND HAFNIUM 432 14.4.4. SEPARATION OF CADMIUM AND ZINC 435
14.4.5. SEPARATION OF NICKEL, COBALT, MAGNESIUM, AND COPPER 435 14.4.6.
SEPARATION OF COPPER, CADMIUM, AND MANGANESE 437 14.4.7. SEPARATION OF
IRON(II) AND IRON(III) 438 14.4.8. PRECONCENTRATION OF TRACE ELEMENTS
FROM CERTAIN ROCK MACROCOMPONENTS 438 REFERENCES 441 INDEX 445
|
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| id | DE-604.BV010861302 |
| illustrated | Illustrated |
| indexdate | 2024-07-09T18:00:07Z |
| institution | BVB |
| isbn | 0471637491 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-007259677 |
| oclc_num | 832680882 |
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| owner | DE-355 DE-BY-UBR DE-20 DE-91G DE-BY-TUM DE-83 |
| owner_facet | DE-355 DE-BY-UBR DE-20 DE-91G DE-BY-TUM DE-83 |
| physical | XXIII, 454 S. Ill., graph. Darst. |
| publishDate | 1996 |
| publishDateSearch | 1996 |
| publishDateSort | 1996 |
| publisher | Wiley |
| record_format | marc |
| series | Chemical analysis |
| series2 | Chemical analysis |
| spelling | High-speed countercurrent chromatography ed. by Yoichiro Ito ... New York [u.a.] Wiley 1996 XXIII, 454 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Chemical analysis 132 Gegenstromchromatographie (DE-588)4241437-4 gnd rswk-swf Gegenstromchromatographie (DE-588)4241437-4 s DE-604 Ito, Yoichiro Sonstige oth Chemical analysis 132 (DE-604)BV000008780 132 GBV Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=007259677&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | High-speed countercurrent chromatography Chemical analysis Gegenstromchromatographie (DE-588)4241437-4 gnd |
| subject_GND | (DE-588)4241437-4 |
| title | High-speed countercurrent chromatography |
| title_auth | High-speed countercurrent chromatography |
| title_exact_search | High-speed countercurrent chromatography |
| title_full | High-speed countercurrent chromatography ed. by Yoichiro Ito ... |
| title_fullStr | High-speed countercurrent chromatography ed. by Yoichiro Ito ... |
| title_full_unstemmed | High-speed countercurrent chromatography ed. by Yoichiro Ito ... |
| title_short | High-speed countercurrent chromatography |
| title_sort | high speed countercurrent chromatography |
| topic | Gegenstromchromatographie (DE-588)4241437-4 gnd |
| topic_facet | Gegenstromchromatographie |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=007259677&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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| work_keys_str_mv | AT itoyoichiro highspeedcountercurrentchromatography |