NMR spectroscopy and stereoregularity of polymers:
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| Main Authors: | , , |
|---|---|
| Format: | Book |
| Language: | English |
| Published: |
Tokyo
Japan Scientif. Soc. Press
1996
Basel [u.a.] Karger |
| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Physical Description: | XVII, 275 S. graph. Darst. |
| ISBN: | 4762287989 3805562985 |
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MARC
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Record in the Search Index
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| adam_text | NMR SPECTROSCOPY AND STEREOREGULARITY OF POLYMERS KEI MATSUZAKI,
TOSHIYUKI URYU, AND TETSUO ASAKURA WITH 148 FIGURES AND 80 TABLES JAPAN
SCIENTIFIC SOCIETIES PRESS TOKYO KARGEH BASEL-FREIBURG-PARIS-LONDON-NEW
YORK-NEW DELHI- BANGKOK * SINGAPORE * TOKYO*SYDNEY CONTENTS PREFACE V
ACKNOWLEDGEMENTS XV ABBREVIATIONS X I I. NMR SPECTROSCOPY AND
STEREOREGULARITY OF VINYL POLYMERS AND POLY(ALKYLENE OXIDE)S CHAPTER 1
INTRODUCTION 2 1.1 CONFIGURATION OF POLYMERS 2 1.2 H NMR SPECTRA OF
VINYL POLYMERS 9 1.3 DEUTERATION OF MONOMERS AND POLYMERS 11 1.4 OPENING
MODE OF VINYL DOUBLE BONDS AND DITACTIC POLY- MERS 12 1.5 MODEL
COMPOUNDS 13 1.6 13 C NMR SPECTRA OF VINYL POLYMERS 13 1.7 13 C
SIDE-BAND SPECTRA . . 14 1.8 CONFORMATION OF VINYL POLYMERS 18 1.9 RATE
PROCESSES OBSERVED WITH NMR SPECTROSCOPY . . . 21 CHAPTER 2 POLYOLEFINS
25 2.1 POLYETHYLENE 25 VLLL 2.2 POLYPROPYLENE . 26 2.3 POLY(L-BUTENE) 32
2.4 POLY(L-PENTENE), POLY(L-HEXENE), POLY(L-HEPTENE), POLY(L- OCTENE)
ANDPOLY(L-NONENE) 37 2.5 POLY(3-METHYL-L-BUTENE) 38 CHAPTER 3 POLYDIENES
41 3.1 POLYBUTADIENE 41 3.2 POLYISOPRENE 46 3.3 POLYCHLOROPRENE 51
CHAPTER 4 POLY(METHYL METHACRYLATE) AND RELATED ESTER DE- RIVATIVES 57
4.1 SYNTHESIS OF STEREOREGULAR POLYMETHACRYLATES 57 4.2 H AND 13 C NMR
SPECTROSCDPY OF POLY(METHYL METHACRY- LATE) 58 4.3 STEREOREGULARITY OF
RELATED ESTER DERIVATIVES 63 4.4 POLYMERIZATION OF OPTICALLY ACTIVE
MONOMERS AND THE STE- REOREGULARITY OF POLYMERS . . ; 67 4.5 TWO PHASE
POLYMERIZATION OF POLY(METHYL METHACRYLATE); POLYMERIZATION WITH
GRIGNARD REAGENT AS CATALYST ... 69 4.6 STEREOREGULARITY OF POLY(METHYL
METHACRYLATE) OBTAINED IN MATRIX POLYMERIZATION 71 4.7 OPTICALLY ACTIVE
DERIVATIVES WITH HELICAL STRUCTURE . . . , 74 CHAPTER 5 POLY(METHYL
ACRYLATE) AND RELATED ESTER DERIVA- TIVES 80 5.1 SYNTHESIS OF
STEREOREGULAR POLYACRYLATES 80 5.2 STEREOREGULARITY OF POLYACRYLATES
DETERMINED BY H NMR SPECTROSCOPY 80 5.3 13 C NMR SPECTROSCOPY OF
POLYACRYLATES 84 5.4 DOUBLE BOND OPENING MODE OF ACRYLATES IN
POLYMERIZA- TION 87 5.5 ASYMMETRIC EFFECTS OF OPTICALLY ACTIVE SIDE
GROUPS IN THE POLYMERIZATION OF OPTICALLY ACTIVE ACRYLATES 88 CONTENTS
IX 5.6 CONFORMATION OF POLY(METHYL ACRYLATE) 89 CHAPTER 6
POLY(A-CHLOROACRYLATE)S 94 6.1 INTRODUCTION 94 6.2 SYNTHESIS OF
STEREOREGULAR POLY(A-CHLOROACRYLATE)S ... 94 6.3 H NMR SPECTROSCOPY OF
POLY(A-CHLOROACRYLATE)S ... 95 6.4 STEREOCOMPLEX FORMATION OF
POLY(A-CHLOROACRYLATE)S . . 97 CHAPTER 7 POLY(VINYL ETHER)S 98 7.1
INTRODUCTION 98 7.2 SYNTHESIS OF STEREOREGULAR POLY(VINYL ETHER)S 98 7.3
H NMR SPECTROSCOPY OF POLY(VINYL ETHER)S 98 7.4 13 C NMR SPECTROSCOPY
OF POLY(VINYL ETHER)S 102 7.5 STEREOCHEMISTRY IN THE CATIONIC
POLYMERIZATION OF VINYL ETHERS 103 7.6 OPTICALLY ACTIVE COPOLYMERS OF
POLY(VINYL ETHER)S . . . 108 CHAPTER 8 POLY(A-METHYL VINYL ETHER)S 113
CHAPTER 9 POLY(VINYL KETONE)S AND POLY(ISOPROPENYL KETONE)S 118 9.1 H
AND 13 C NMR SPECTROSCOPY OF POLY(VINYL KETONE)S . 118 9.2 13 C NMR
SPECTROSCOPY OF POLY(ISOPROPENYL KETONE)S . . 120 CHAPTER 10
POLYACRYLONITRILE 123 10.1 SYNTHESIS OF POLYACRYLONITRILE 123 10.2 H
NMR SPECTROSCOPY OF POLYACRYLONITRILE 123 10.3 13 C NMR SPECTROSCOPY OF
POLYACRYLONITRILE 128 CHAPTER 11 POLYMETHACRYLONITRILE 131 11.1
SYNTHESIS OF POLYMETHACRYLONITRILE 131 X 11.2 H NMR SPECTROSCOPY AND
STEREOREGULARITY OF POLY- METHACRYLONITRILE 131 11.3 13 C NMR
SPECTROSCOPY OF POLYMETHACRYLONITRILE . . . . 132 CHAPTER 12 POLYSTYRENE
AND ITS DERIVATIVES 137 12.1 SYNTHESIS OF STEREOREGULAR POLYSTYRENE 137
12.2 H NMR SPECTROSCOPY OF POLYSTYRENE 138 12.3 13 C NMR SPECTROSCOPY
OF POLYSTYRENE 139 12.4 STEREOREGULARITY OF POLYSTYRENES OBTAINED BY
ANIONIC PO- LYMERIZATION 141 12.5 STEREOREGULARITY OF POLYSTYRENES
OBTAINED WITH BUTYL- LITHIUM-WATER 145 12.6 STEREOREGULARITY OF
POLYSTYRENES OBTAINED WITH ALFIN CATALYST 146 12.7 STEREOREGULARITY OF
POLYSTYRENES OBTAINED WITH CATIONIC CATALYSTS 147 12.8 STEREOREGULARITY
OF POLYSTYRERFES OBTAINED BY RADIATION-IN- DUCED POLYMERIZATION 147 12.9
SYNTHESIS AND STEREOREGULARITY OF POLY(METHYLSTYRENE)S 149 12.10
SYNTHESIS AND STEREOREGULARITY OF POLY(METHOXYSTYRENE)S 152 CHAPTER 13
POLY(A-METHYLSTYRENE) 157 13.1 SYNTHESIS OF POLY(OE-METHYLSTYRENE) 157
13.2 ] H NMR SPECTROSCOPY OF POLY(A-METHYLSTYRENE) . ... 158 13.3 13 C
NMR SPECTROSCOPY OF POLY(A-METHYLSTYRENE) ... 158 13.4 STEREOREGULARITY
OF POLY(A-METHYLSTYRENE) OBTAINED WITH ANIONIC CATALYSTS 158 13.5
STEREOREGULARITY OF POLY(OE-METHYLSTYRENE) PREPARED WITH CATIONIC
CATALYSTS . 161 CHAPTER 14 POLY(VINYLPYRIDINE)S 163 14.1 SYNTHESIS OF
POLY(VINYLPYRIDINE)S 163 14.2 H AND 13 C NMR SPECTROSCOPY OF
POLY(VINYLPYRIDINE)S . 163 CONTENTS XI 14.3 MECHANISM OF ISOTACTIC
POLYMERIZATION OF POLY(2- VINYLPYRIDINE) 168 CHAPTER 15
POLY(N-VINYLCARBAZOLE) 173 15.1 SYNTHESIS OF POLY(N-VINYLCARBAZOLE) 173
15.2 H AND 13 C NMR SPECTROSCOPY OF POLY(N-VINYLCARBAZOLE) 173 15.3 THE
STRUCTURE OF POLY(N-VINYLCARBAZOLE) OBTAINED WITH ELECTRON ACCEPTORS AS
CATALYSTS 175 CHAPTER 16 POLY (VINYL ACETATE) 179 16.1 SYNTHESIS OF
POLY(VINYL ACETATE) 179 16.2 H AND 13 C NMR SPECTROSCOPY OF POLY(VINYL
ACETATE) . . 179 CHAPTER 17 POLY(ISOPROPENYL ACETATE) 182 17.1 SYNTHESIS
OF POLY(ISOPROPENYL ACETATE) 182 17.2 H AND 13 C NMR SPECTROSCOPY OF
POLY(ISOPROPENYL AC- ETATE) 182 CHAPTER 18 POLYETHYLENE OXIDE) 185 18.1
SYNTHESIS OF POLYETHYLENE OXIDE) 185 18.2 CONFORMATION OF POLY(ETHYLENE
OXIDE) DETERMINED BY H NMR SPECTROSCOPY . 185 18.3 OPENING MODE IN THE
POLYMERIZATION OF ETHYLENE OXIDE 193 CHAPTER 19 POLY(PROPYLENE OXIDE)
198 19.1 SYNTHESIS OF POLY(PROPYLENE OXIDE) 198 19.2 NMR SPECTROSCOPY
AND STEREOREGULARITY OF POLY(PRO- PYLENE OXIDE) 199 XII CHAPTER 20
POLY(PROPENYL ETHER)S 203 20.1 INTRODUCTION 203 20.2 H AND 13 C NMR
SPECTROSCOPY OF POLY(J3-SUBSTITUTED VINYL ETHER)S 204 20.3
STEREOCHEMISTRY IN THE PROCESS OF POLYMERIZATION . . . 206 CHAPTER 21
POLY (VINYL ALCOHOL) 212 21.1 SYNTHESIS OF POLY (VINYL ALCOHOL) 212 21.2
H AND 13 C NMR SPECTROSCOPY OF POLY(VINYL ALCOHOL) . 212 CHAPTER 22
POLY (VINYL CHLORIDE) 216 22.1 SYNTHESIS OF POLY(VINYL CHLORIDE) 216
22.2 H AND 13 C NMR SPECTROSCOPY OF POLY(VINYL CHLORIDE) . 216 CHAPTER
23 FACTORS AFFECTING STEREOREGULARITY OF VINYL POLY- MERS 221 23.1
RADICAL POLYMERIZATION 222 23.2 CATIONIC POLYMERIZATION 224 23.3 ANIONIC
POLYMERIZATION 225 II. REACTIONS CORRELATED TO THE STEREOREGULARITY OF
POLYMERS CHAPTER 24 THERMAL REACTION AND HYDROLYSIS OF POLYMETHACRY-
LATES AND POLYACRYLATES 228 24.1 THERMAL REACTION AND ANHYDRIDE
FORMATION OF POLY- METHACRYLATES 228 24.2 HYDROLYSIS AND ANHYDRIDE
FORMATION OF POLYMETHACRYLATES 230 24.3 HYDROLYSIS AND ANHYDRIDE
FORMATION OF POLYACRYLATES . 231 CONTENTS XIII CHAPTER 25 THERMAL
REACTION OF POLY(METHYL VINYL KETONE) AND POLY(ISOPROPENYL METHYL
KETONE) 234 25.1 THERMAL REACTION OF POLY (METHYL VINYL KETONE) . . . .
234 25.2 THERMAL REACTION OF POLY(ISOPROPENYL METHYL KETONE) . 235
CHAPTER 26 RACEMIZATION OF POLYACRYLONITRILE 239 III. NMR SPECTROSCOPY
OF LIVING POLYMERS AND QUANTUM CHEMICAL ANALYSIS CHAPTER 27 LIVING
POLYSTYRENE 242 27.1 NMR SPECTROSCOPY OF POLYSTYRYL ANIONS AND THEIR
MODEL COMPOUNDS 242 27.2 NMR SPECTROSCOPY OF POLYSTYRYLLITHIUM AND ITS
MODEL COMPOUNDS 244 27.3 NMR SPECTROSCOPY OF POLYSTYRYLPOTASSIUM AND ITS
MODEL COMPOUNDS 245 27.4 EFFECT OF COUNTER CATION ON THE EXCESS CHARGE
DISTRIBUTION 245 27.5 EFFECT OF THE KIND OF SOLVENT ON THE EXCESS CHARGE
DISTRI- BUTION 247 27.6 ROTATION OF CA-CL BOND OF POLYSTYRYLLITHIUM AND
ITS MODEL COMPOUNDS 248 27.7 QUANTUM CHEMICAL TREATMENT OF POLYSTYRYL
ANIONS . . 248 27.8 SPIN-LATTICE RELAXATION TIMES T X OF LIVING ANION
... 251 CHAPTER 28 LIVING POLY(A-METHYLSTYRENE) 253 28.1 H AND 13 C NMR
SPECTROSCOPY OF LIVING POLY(A- METHYLSTYRENE) 253 28.2 QUANTUM CHEMICAL
CALCULATION OF POLY(A-METHYLSTYRYL) ANION 256 28.3 ROTATION OF CA-C 1
BOND OF POLY (A-METHYLSTYRYL) LITHIUM 257 XIV CHAPTER 29 LIVING
POLY(METHYLSTYRENE)S 258 29.1 INTRODUCTION 258 29.2 NMR SPECTROSCOPY OF
LIVING POLY(O-METHYLSTYRENE) AND ITS MODEL COMPOUND 259 29.3 NMR
SPECTROSCOPY OF LIVING POLY(M-METHYLSTYRENE) AND ITS MODEL COMPOUND 261
29.4 NMR SPECTROSCOPY OF LIVING POLY(P-METHYLSTYRENE) . . 263 CHAPTER 30
LIVING POLY(O-METHOXYSTYRENE) 265 SUBJECT INDEX 269 ABOUT THE AUTHORS
277
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| id | DE-604.BV010807483 |
| illustrated | Illustrated |
| indexdate | 2024-07-09T17:59:13Z |
| institution | BVB |
| isbn | 4762287989 3805562985 |
| language | English |
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| physical | XVII, 275 S. graph. Darst. |
| publishDate | 1996 |
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| publisher | Japan Scientif. Soc. Press Karger |
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| spelling | Matsuzaki, Kei Verfasser aut NMR spectroscopy and stereoregularity of polymers Kei Matsuzaki, Toshiyuki Uryu, and Tetsuo Asakura Tokyo Japan Scientif. Soc. Press 1996 Basel [u.a.] Karger XVII, 275 S. graph. Darst. txt rdacontent n rdamedia nc rdacarrier Polymères - Analyse Polymères - Structure ram Spectroscopie de la résonance magnétique nucléaire Spectroscopie de la résonance magnétique nucléaire ram Nuclear magnetic resonance spectroscopy Polymers Analysis Stereoreguläre Polymere (DE-588)4411652-4 gnd rswk-swf NMR-Spektroskopie (DE-588)4075421-2 gnd rswk-swf Stereoreguläre Polymere (DE-588)4411652-4 s NMR-Spektroskopie (DE-588)4075421-2 s DE-604 Uryu, Toshiyuki Verfasser aut Asakura, Tetsuo Verfasser aut GBV Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=007219917&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Matsuzaki, Kei Uryu, Toshiyuki Asakura, Tetsuo NMR spectroscopy and stereoregularity of polymers Polymères - Analyse Polymères - Structure ram Spectroscopie de la résonance magnétique nucléaire Spectroscopie de la résonance magnétique nucléaire ram Nuclear magnetic resonance spectroscopy Polymers Analysis Stereoreguläre Polymere (DE-588)4411652-4 gnd NMR-Spektroskopie (DE-588)4075421-2 gnd |
| subject_GND | (DE-588)4411652-4 (DE-588)4075421-2 |
| title | NMR spectroscopy and stereoregularity of polymers |
| title_auth | NMR spectroscopy and stereoregularity of polymers |
| title_exact_search | NMR spectroscopy and stereoregularity of polymers |
| title_full | NMR spectroscopy and stereoregularity of polymers Kei Matsuzaki, Toshiyuki Uryu, and Tetsuo Asakura |
| title_fullStr | NMR spectroscopy and stereoregularity of polymers Kei Matsuzaki, Toshiyuki Uryu, and Tetsuo Asakura |
| title_full_unstemmed | NMR spectroscopy and stereoregularity of polymers Kei Matsuzaki, Toshiyuki Uryu, and Tetsuo Asakura |
| title_short | NMR spectroscopy and stereoregularity of polymers |
| title_sort | nmr spectroscopy and stereoregularity of polymers |
| topic | Polymères - Analyse Polymères - Structure ram Spectroscopie de la résonance magnétique nucléaire Spectroscopie de la résonance magnétique nucléaire ram Nuclear magnetic resonance spectroscopy Polymers Analysis Stereoreguläre Polymere (DE-588)4411652-4 gnd NMR-Spektroskopie (DE-588)4075421-2 gnd |
| topic_facet | Polymères - Analyse Polymères - Structure Spectroscopie de la résonance magnétique nucléaire Nuclear magnetic resonance spectroscopy Polymers Analysis Stereoreguläre Polymere NMR-Spektroskopie |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=007219917&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT matsuzakikei nmrspectroscopyandstereoregularityofpolymers AT uryutoshiyuki nmrspectroscopyandstereoregularityofpolymers AT asakuratetsuo nmrspectroscopyandstereoregularityofpolymers |