Multidimensional NMR in liquids: basic principles and experimental methods
"Multidimensional NMR in Liquids offers a lucid treatment of basic NMR phenomena, building up to today's most sophisticated NMR experiments from first principles. Using easy-to-grasp product-operator formalism, diagrams, and practical examples, one-, two-, and N-dimensional NMR experiments...
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Buch |
| Sprache: | German |
| Veröffentlicht: |
New York, NY [u.a.]
VCH
1995
|
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Zusammenfassung: | "Multidimensional NMR in Liquids offers a lucid treatment of basic NMR phenomena, building up to today's most sophisticated NMR experiments from first principles. Using easy-to-grasp product-operator formalism, diagrams, and practical examples, one-, two-, and N-dimensional NMR experiments are explained with minimal recourse to quantum mechanics. Separate theoretical sections are provided for readers interested in spin-quantum mechanics, as are the appendices providing theoretical backgrounds in linear algebra, quantum mechanics, and angular momentum." "Multidimensional NMR in Liquids is intended for chemists, biochemists, and others interested in studying molecular structure and dynamics with NMR spectroscopy. It also is suitable for use as a text in advanced undergraduate and graduate courses in NMR."--BOOK JACKET. |
| Beschreibung: | Literaturangaben |
| Beschreibung: | XVII, 399 S. graph. Darst. |
| ISBN: | 1560816651 |
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Datensatz im Suchindex
| _version_ | 1822490823064813568 |
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| adam_text |
MULTIDIMENSIONAL NMR IN LIQUIDS BASIC PRINCIPLES AND EXPERIMENTAL
METHODS FRANK J. M. VAN DE VEN WILEY-VCH NEW YORK * CH1CHESTER *
WEINHEIM * BRISBANE * SINGAPORE * TORONTO CONTENTS SYMBOLS AND
ABBREVIATIONS XV 1 BASIC PRINCIPLES 1 1.1 INTRODUCTION , 1 1.2 NUCLEAR
MAGNETIC DIPOLE 2 1.3 EFFECT OF A RADIO-FREQUENCY FIELD 4 1.3.1 ROTATING
REFERENCE FRAME 5 1.3.2 RADIO-FREQUENCY PULSE 7 1.4 RELAXATION, THE
BLOCH EQUATIONS 7 1.4.1 FREE PRECESSION 9 1.5 OFF-RESONANCE EFFECT 10
1.5.1 PULSE EXCITATION PROFILE 13 1.5.2 "BLOCH-SIEGERT" EFFECT 15 1.6
SATURATION 16 1.7 THE NMR SPECTROMETER 17 1.7.1 THE MAGNET 17 1.7.2 THE
PROBE 18 1.7.3 THE SYNTHESIZER 19 1.7.4 THE TRANSMITTER 19 1.7.5 THE
RECEIVER 20 1.7.6 THE ANALOG-TO-DIGITAL CONVERTER 21 1.7.7 THE COMPUTER
23 1.8 SOME BASIC EQUATIONS 24 1.9 FOURIER TRANSFORMATION 25 1.9.1 PHASE
CORRECTION 27 1.9.2 REAL FT, RECEIVER PHASE 28 1.9.3 QUADRATURE
DETECTION 29 1.9.4 SOME FOURIER PAIRS 30 1.9.5 MODULATION AND
CONVOLUTION 33 1.9.6 WINDOW FUNCTIONS 34 1.9.7 DISCRETE FT 36 1.10
QUANTUM DESCRIPTION IN HILBERT SPACE 40 1.10.1 FREE PRECESSION 40 IX
CONTENTS 1.10.2^ EFFECT OF A RADIO-FREQUENCY PULSE 42 1.11 DESCRIPTION
IN LIOUVILLE SPACE 45 REFERENCES 47 MULTISPIN SYSTEMS 49 2.1 CHEMICAL
SHIFT 49 2.1.1 SPECTRUM CALIBRATION 53 2.2 J COUPLING 53 2.2.1 KARPLUS
EQUATION 54 2.3 PRODUCT-OPERATOR FORMALISM: PRACTICE 55 2.3.1 THE
STARTING SITUATION 56 2.3.2 EFFECTS OF RF PULSES 57 2.3.3 FREE LARMOR
PRECESSION 58 2.3.4 COMMUTATION OF ROTATIONS 59 2.3.5 J MODULATION 61
2.3.6 COHERENCE SPACE 62 2.3.7 COMMUTATIONS IN COHERENCE SPACE 62 2.3.8
MASTER EQUATION 65 2.3.9 FREE PRECESSION WITH J MODULATION 68 2.3.10 THE
THREE BASIC ROTATIONS 70 2.3.11 THREE OR MORE SPINS 72 2.3.12 FORMAL
NOMENCLATURE 73 2.3.13 MATRIX NOTATION 74 2.4 RELAXATION OF COHERENCES
76 2.4.1 CROSS-RELAXATION 76 2.4.2 NUCLEAR OVERHAUSER ENHANCEMENT 77 2.5
CHEMICAL EXCHANGE 78 2.6 PRODUCT-OPERATOR FORMALISM: THEORY 83 2.6.1
TERMS OF THE SPIN HAMILTONIAN 83 2.6.2 SPIN HAMILTONIAN IN ROTATING
FRAME \. 86 2.6.3 PRODUCT-OPERATOR BASIS 87 2.6.4 BASIC NMR EXPERIMENT
90 2.6.5 STRONG COUPLING 92 REFERENCES 98 ONE-DIMENSIONAL NMR 99 3.1 NMR
TOOL: 90 PULSE 99 3.2 NMR TOOL: 180 PULSE 100 3.2.1 REFOCUSING LARMOR
PRECESSION 101 3.2.2 EFFECT ON J MODULATION 102 3.2.3 COMBINATION OF J
MODULATION AND LARMOR PRECESSION 105 3.3 A DEMO MOLECULE: HISVALTYR 107
3.4 MEASURING RELAXATION TIMES 108 3.4.1 INVERSION RECOVERY 110 3.4.2
SPIN ECHO 112 CONTENTS XI 3.5 RF PULSE CALIBRATION 116 3.6 INEPT 119
3.6.1 REFOCUSED INEPT 123 3.7 DEPT 127 3.8 NMR TOOL: COMPOSITE PULSES
132 3.8.1 OFF-RESONANCE PULSE 136 3.8.2 BAND-SELECTIVE RADIO FREQUENCY
PULSES 139 3.9 NMR TOOL: DECOUPLING 140 3.9.1 ON RESONANCE-DECOUPLING
143 3.9.2 OFF-RESONANCE DECOUPLING 145 3.9.3 BROADBAND DECOUPLING 151
3.9.4 MODULATION SIDEBANDS 155 3.9.5 SEVERAL DECOUPLING SCHEMES 156
REFERENCES 159 4 TWO-DIMENSIONAL NMR 163 4.1 2D CORRELATED SPECTROSCOPY:
COSY 165 4.1.1 FINE STRUCTURE OF COSY CROSS-PEAK MULTIPLETS . 171
4.1.2 HETERONUCLEAR COSY 173 4.2 2D J-RESOLVED NMR 177 4.3 2D NOE
SPECTROSCOPY 181 4.3.1 SPIN DIFFUSION 187 4.4 LINE SHAPES OF 2D NMR
PEAKS 190 4.4.1 PHASE-SENSITIVE 2D NMR 193 4.4.2 PHASE CORRECTION AND
ALIASING 195 4.4.3 TPPI 198 4.5 SIGNAL-TO-NOISE RATIO OF 2D NMR 201 4.6
NMR TOOL: PHASE CYCLING 203 4.6.1 DOUBLE-QUANTUM FILTERED COSY 205 4.6.2
PULSE IMPERFECTIONS AND PHASE CYCLING '. . 207 4.7 NMR TOOL: X-FILTERS
210 4.7.1 BIRD PULSES 211 4.8 NMR TOOL: PULSED FIELD GRADIENTS 211 4.8.1
DEPHASING COHERENCES 212 4.8.2 APPLICATIONS OF PULSED FIELD GRADIENTS
217 4.8.3 APPLICATION OF RF INHOMOGENEITY 223 4.9 VARIANTS OF COSY 224
4.9.1 /3-COSY 225 4.9.2 E.COSY 226 4.9.3 P.E.COSY 227 4.9.4 RELAYED COSY
232 4.9.5 MULTIPLE-QUANTUM SPECTROSCOPY 235 4.9.6 TOTAL CORRELATION
SPECTROSCOPY (TOCSY) 241 4.10 VARIANT OF NOESY: ROESY 249 4.11 VARIANTS
OF HETERONUCLEAR COSY 255 XII CONTENTS 4.11.1 HSQC 255 4.11.2 HMQC 257
4.11.3 SENSITIVITY ENHANCED HSQC 259 4.11.4 CONSTANT-TIME HSQC 262 4.12
NMR TOOL: HARTMANN-HAHN TRANSFER 265 4.12.1 THE HARTMANN-HAHN CONDITION
266 4.12.2 THE EFFECT OF OFFSETS 268 4.12.3 BROADBAND HARTMANN-HAHN
MATCHING 273 4.12.4 NUMERICAL SIMULATIONS 279 4.13 COHERENCE-ORDER
PATHWAYS 281 REFERENCES 288 5 N-DIMENSIONAL NMR 295 5.1 NOESY-HMQC 295
5.1.1 VARIANTS OF 3D NOESY-HMQC 301 5.1.2 4D HMQC-NOESY-HMQC 303 5.2
TOCSY-HMQC 306 5.2.1 HCCH-TOCSY 307 5.3 HOMONUCLEAR 3D NMR 311 5.4
TRIPLE-RESONANCE EXPERIMENTS 314 5.4.1 HNCO 316 5.4.2 HN(CO)CA 323 5.4.3
CBCA(CO)NH 324 5.4.4 EXAMPLE: SUBTILISIN 328 REFERENCES 330 6 RELAXATION
335 6.1 THE BASICS OF RELAXATION 335 6.1.1 RANDOM FIELDS 339 6.1.2
DIPOLAR RELAXATION 340 6.1.3 OTHER RELAXATION MECHANISMS 344 6.2 DENSITY
OPERATOR RELAXATION THEORY 345 6.2.1 DIPOLAR RELAXATION REVISITED 352
6.2.2 CHEMICAL SHIELDING ANISOTROPY 356 6.2.3 CORRELATION FUNCTION 358
REFERENCES 361 A LINEAR ALGEBRA 363 A.I VECTOR SPACE 363 A.2 BASIS 364
A.3 INPRODUCT 364 A.4 OPERATORS 365 A.5 VECTOR AND MATRIX
REPRESENTATIONS 366 A.6 EIGENKETS AND EIGENVALUES 367 A.7 TRACE 367
CONTENTS XIII A.8 OPERATOR ALGEBRA 368 A.8.1 OPERATOR BASIS 368 A.8.2
CYCLIC COMMUTATION 369 B RECIPES OF QUANTUM MECHANICS 371 B.I BASIC
RECIPE IN HILBERT SPACE 371 B.2 RECIPE IN LIOUVILLE SPACE: DENSITY
MATRIX 374 B.2.1 BOLTZMANN DENSITY MATRIX 375 B.3 SPIN-LATTICE
DISCONNECTION 377 C ANGULAR MOMENTUM 379 C.I ANGULAR MOMENTUM OPERATORS
379 C.I.I ROTATION SUPEROPERATOR 381 C.1.2 SPIN OPERATORS 382 C.2
EIGENKETS AND EIGENVALUES 382 C.2.1 SPIN OPERATOR MATRICES 385 C.2.2
SPIN 1 = 1/2 386 C.3 MORE ABOUT ROTATIONS 387 C.3.1 EULER ANGLES 388
C.3.2 WIGNER ROTATION MATRIX 388 C.3.3 SPHERICAL HARMONICS 389 FURTHER
READING 393 INDEX 395 |
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| id | DE-604.BV010756144 |
| illustrated | Illustrated |
| indexdate | 2025-01-28T11:11:28Z |
| institution | BVB |
| isbn | 1560816651 |
| language | German |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-007183873 |
| oclc_num | 845033160 |
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| owner_facet | DE-703 DE-20 DE-91G DE-BY-TUM DE-355 DE-BY-UBR DE-634 DE-83 |
| physical | XVII, 399 S. graph. Darst. |
| publishDate | 1995 |
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| spelling | Ven, Frank J. M. van de 1953- Verfasser (DE-588)122850211 aut Multidimensional NMR in liquids basic principles and experimental methods Frank J. M. van de Ven New York, NY [u.a.] VCH 1995 XVII, 399 S. graph. Darst. txt rdacontent n rdamedia nc rdacarrier Literaturangaben "Multidimensional NMR in Liquids offers a lucid treatment of basic NMR phenomena, building up to today's most sophisticated NMR experiments from first principles. Using easy-to-grasp product-operator formalism, diagrams, and practical examples, one-, two-, and N-dimensional NMR experiments are explained with minimal recourse to quantum mechanics. Separate theoretical sections are provided for readers interested in spin-quantum mechanics, as are the appendices providing theoretical backgrounds in linear algebra, quantum mechanics, and angular momentum." "Multidimensional NMR in Liquids is intended for chemists, biochemists, and others interested in studying molecular structure and dynamics with NMR spectroscopy. It also is suitable for use as a text in advanced undergraduate and graduate courses in NMR."--BOOK JACKET. NMR gtt Ressonancia nuclear magnetica (medicina) larpcal Magnetic Resonance Spectroscopy methods Nuclear magnetic resonance spectroscopy Mehrdimensionale NMR-Spektroskopie (DE-588)4346802-0 gnd rswk-swf Lösung Chemie (DE-588)4036159-7 gnd rswk-swf Lösung Chemie (DE-588)4036159-7 s Mehrdimensionale NMR-Spektroskopie (DE-588)4346802-0 s DE-604 GBV Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=007183873&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Ven, Frank J. M. van de 1953- Multidimensional NMR in liquids basic principles and experimental methods NMR gtt Ressonancia nuclear magnetica (medicina) larpcal Magnetic Resonance Spectroscopy methods Nuclear magnetic resonance spectroscopy Mehrdimensionale NMR-Spektroskopie (DE-588)4346802-0 gnd Lösung Chemie (DE-588)4036159-7 gnd |
| subject_GND | (DE-588)4346802-0 (DE-588)4036159-7 |
| title | Multidimensional NMR in liquids basic principles and experimental methods |
| title_auth | Multidimensional NMR in liquids basic principles and experimental methods |
| title_exact_search | Multidimensional NMR in liquids basic principles and experimental methods |
| title_full | Multidimensional NMR in liquids basic principles and experimental methods Frank J. M. van de Ven |
| title_fullStr | Multidimensional NMR in liquids basic principles and experimental methods Frank J. M. van de Ven |
| title_full_unstemmed | Multidimensional NMR in liquids basic principles and experimental methods Frank J. M. van de Ven |
| title_short | Multidimensional NMR in liquids |
| title_sort | multidimensional nmr in liquids basic principles and experimental methods |
| title_sub | basic principles and experimental methods |
| topic | NMR gtt Ressonancia nuclear magnetica (medicina) larpcal Magnetic Resonance Spectroscopy methods Nuclear magnetic resonance spectroscopy Mehrdimensionale NMR-Spektroskopie (DE-588)4346802-0 gnd Lösung Chemie (DE-588)4036159-7 gnd |
| topic_facet | NMR Ressonancia nuclear magnetica (medicina) Magnetic Resonance Spectroscopy methods Nuclear magnetic resonance spectroscopy Mehrdimensionale NMR-Spektroskopie Lösung Chemie |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=007183873&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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