Chirale, tripodale Neopentyl-Tris(phosphan)-Liganden: Synthese und Koordinationschemie
Saved in:
| Main Author: | |
|---|---|
| Format: | Microfilm Book |
| Language: | German |
| Published: |
1994
|
| Edition: | [Mikrofiche-Ausg.] |
| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Item Description: | Heidelberg, Univ., Diss., 1994. - Mikrofiche-Ausg.: 3 Mikrofiches : 24x |
| Physical Description: | IV, 153 Bl. graph. Darst. |
Staff View
MARC
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| 100 | 1 | |a Seitz, Thomas |e Verfasser |4 aut | |
| 245 | 1 | 0 | |a Chirale, tripodale Neopentyl-Tris(phosphan)-Liganden |b Synthese und Koordinationschemie |c von Thomas Seitz |
| 250 | |a [Mikrofiche-Ausg.] | ||
| 264 | 1 | |c 1994 | |
| 300 | |a IV, 153 Bl. |b graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b h |2 rdamedia | ||
| 338 | |b he |2 rdacarrier | ||
| 500 | |a Heidelberg, Univ., Diss., 1994. - Mikrofiche-Ausg.: 3 Mikrofiches : 24x | ||
| 650 | 0 | 7 | |a Neopentylgruppe |0 (DE-588)4336495-0 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Phosphine |0 (DE-588)4174379-9 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Tripodmetallkomplexe |0 (DE-588)4283671-2 |2 gnd |9 rswk-swf |
| 655 | 7 | |0 (DE-588)4113937-9 |a Hochschulschrift |2 gnd-content | |
| 689 | 0 | 0 | |a Phosphine |0 (DE-588)4174379-9 |D s |
| 689 | 0 | 1 | |a Neopentylgruppe |0 (DE-588)4336495-0 |D s |
| 689 | 0 | 2 | |a Tripodmetallkomplexe |0 (DE-588)4283671-2 |D s |
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| 943 | 1 | |a oai:aleph.bib-bvb.de:BVB01-006952566 | |
Record in the Search Index
| _version_ | 1812453927408369664 |
|---|---|
| adam_text |
I
INHALTSVERZEICHNIS
1
2
2.1
2.2
2.3
2.4
2.4.1
2.4.2
2.4.3
2.4.4
2.4.5
ALLGEMEINER
3.1
3.2
3.3
3.4
3.5
3.5.1
EINLEITUNG.
KENNTNISSTAND. .1
EPC-SYNTHESE. .3
LIGAND-TYPEN FUER DIE UEBERGANGSMETALLKATALYSE .
Q-SYMMETRISCHE, CHIRALE TRIPOD-LIGANDEN. .
4
UEBERGANGSMETALLKOMPLEX-KATALYSIERTE REAKTIONEN
HYDRIERUNG VON ALKENEN UND ALKINEN
HY DROFORMYLIERUNG.
ACETALISIERUNG.
MICHAEL-ADDITION.
ALLYLISCHE ALKYLIERUNG.
TEIL.
VORBEMERKUNGEN.
S V^
656 ^ CH*RAKYY TTLPOED'LIGANDEN MIT HILFE DER SCHUTZGRUPPENTECHNIK ,6
SYNTHESE VON CHIRALEN ''HYDROXY-TRIPOD-LIGANDEN".
'16
FUNKUEONALISIERUNGSMOEGLICHKEITEN AM TRIPOD-RUECKGRA,
EINGRENZUNG DER MOEGLICHKEITEN
FUER
EINE ENANTIOMERENTRENNUNG
ANALYTISCHE HPLC.
MIT "TRIPHOS". 9
.9
.
11
.12
.12
.13
.14
.14
.23
27
44
4.1
4.2
4.3
5.1
5.2
.44
.45
.48
.51
.51
.53
3-5.2 UEBERFUEHRUNG IN DIASTEREOMERE DERIVATE.'.'.'.'^
P
YY 3'5'3 STEMOSEITENDIFFERENZIERENDE QXETANSPALTUNE
KONFORMATIONSANALYSEN
ALLGEMEINE VORBEMERKUNGEN.
MASCHINENDATEN UND EINSTELLUNGEN.
EXNEH
MK0^RATI0NSA"ALYSEN V" "^(COB-KOMPLEXEN'T'. YY
EXPERIMENTELLER UND ANALYTISCHER TEIL. 53
ALLGEMEINE ANGABEN. .
59
.59
.59
.61
3-HYDROXYMETHYI-3-METHYL-OXETAN (
2
|.
.
3-METHYL-3-(METHYLSULFONYIOXYMETHYI)-OXETAN (3). ".
3 F
BA^HOSPH0'YLMCTHYL)'3'ME,HYL-OXETA" (* .64
D!
71PHOSPHA"0METHY')'1'PR0PANO1 WH*
SA).
.65
^P^ENY^P*10SE^AN0METHYL)-L-
.66
5.1.1 APPARATUREN, GERAETE UND ALLGEMEINE ARBEITSTECHNIK.
REAGENZIEN.
SYNTHESEVORSCHRIFTEN UND ANALYTISCHE DATEN
5.2.1
5.2.2
5.2.3
5.2.4
5.2.5
PROPANOL (5C).
EN.
BIBLIOGRAFISCHE INFORMATIONEN
HTTP://D-NB.INFO/942438264
II
5.2.6
5.2.7
5.2.8
5.2.9
67
"" ."
5J1!
C _ PHOSPHANMETHY])-1
-PROPYLESTER-BIS(BORAN)
(7B)
YY
2.13 METHAMUIFONSAEURE-2-(5-DIBENZOPHOSPHOLYIMETHYL)-2-.(DIPHENY|
YY
2.14 M^SULFOYYSAEURE-2 5-DIBEMOPHOSPHOLYTAE.HYI)-2-(DI-M-.
X
YIYLPHOSPHANOMC.HYL)-L-PROPYI.ESTER.BIS(BORAIL) (7D).
-(DIPHENYL-
73
.74
.76
5.2.15
5.2.16
5.2.17
5.2.18
5.2.19
5.2.20
5.2.21
TRIS(DIPHENYLPHOSPHANOMETHYL)-ETHAN
.77
("TRIPHOS")
(8A).
::
HR,TAZ^
METHYL)-DI-M-XYLYLPHOSPHANO
TRIPHOS-TRIS(BORAN) (9).
YY
PROPAN (8B). JG
5.2.22
5.2.23
3-BROMMETHYJ-3-H
YDROXYMETHYL-OXETAN
(1
IH.
.83
.
OXR^R
PH"PHO, ;METH ;! 84
3,3-BIS(5-DIBENZOPHOSPHOL
YLMETHYL)-OXETAN (13D).!,
Y ( PHEN
YIPHOSPHANO)
1
-PROPANO] (
14
B)
YY
UEWN3^NZPLLOSPHC'LYINLETLLYL)'2'(DIPHENYIPHOSPHANO'.
5 2 25 MC YY. ^
YY2.25 - C
YY
PHANSAEURE-2.2-BIS(DIPHENYLPHOSPHANOMETHYL,- .
,, ( 'P ENYLPHOSPHA"0'-1 -PROPYLESTER (15A).
YY
.26 -^HANSTO.2,W.
3-(5-DIBENZOPHOSPHOLYL
)-1 -PROPYLESTER (15B). 93
5.2.24 RAC.
M
5.2.27 ((-)-CAMPHANSAEURE-2,2-BIS(5-DIBENZOPHOSPHOLYLMETHYL)-
3-(5-DIBENZOPHOSPHOLYL
)-1
-PROPYLESTER)-MOLYBDAENTRICARBONYL
((P)- UND (M)-16).
95
5.2.28 PHTHALSAEURE-(2,2-BIS(DIPHENYLPHOSPHANOMETHYL)-
3-(DIPHENYLPHOSPHANOPROPYL)-MONOESTER
(17A)
.96
5.2.29 GLUTARSAEURE-(2,2-BIS(DIPHENYLPHOSPHANOMETHYL)-
3-(DIPHENYLPHOSPHANOPROPYL)-MONOESTER (17B).98
5.2.30 (PHTHALSAEURE-(2,2-BIS(DIPHENYLPHOSPHANOMETHYL)-3-DIPHENYL-
PHOSPHANOPROPYL)-MONOESTER)-MOLYBDAENTRICARBONYL (18).99
5.2.31 HYDROXYTRIPOD-TRIS(BORAN)
(19)
.
101
5.2.32 2,2-BIS(DIPHENYLPHOSPHANOMETHYL)-3-(DIPHENYLPHOSPHANO)-
PROPYL-TRIMETHYLSILYLETHER-TRIS(BORAN) (
20
).103
5.2.33 ESSIGSAEURE-2,2-BIS(DIPHENYLPHOSPHANOMETHYL)-3-(DIPHENYL-
PHOSPHANO)-L-PROPYL-ESTER-TRIS(BORAN) (
21
).104
5.2.34 XANTHOGENSAEURE-0-(2,2-BIS(DIPHENYLPHOSPHANOMETHYL)-
3-(DIPHENYLPHOSPHANO
)-1
-PROPYL-S-METHYL-ESTER-TRIS(BORAN) (
22
). 105
5.2.35 METHANSULFONSAEURE-2,2-BIS(DIPHENYLPHOSPHANOMETHYL)-
3-(DIPHENYLPHOSPHANOPROPYL)-ESTER-TRIS(BORAN)
(23)
.107
5.2.26 TETRAKIS(DIPHENYLPHOSPHANOMETHYL)-METHAN
24)
.108
5.2.37 RAC. 2-(5-DIBENZOPHOSPHOLYLMETHYL)-2-(DIPHENYLPHOSPHANO-
METHYL)-3-(DI-M-XYLYLPHOSPHANO)-L-PROPANOL-TRIS(BORAN)
(25)
.109
5.2.38 MOSHER-ESTER VON RAC.
5C
UND RAC.
14C
.110
5.2.38A MOSHERSAEUREESTER VON RAC.2-(5-DIBENZOPHOSPHOLYL-
METHYL)-(DIPHENYLPHOSPHANOMETHYL)-L-PROPANOL
(26A/B).111
5.2.38B MOSHERSAEUREESTER VON RAC. 2-(5-DIBENZOPHOSPHOLYL-
METHYL)-2-(DIPHENYLPHOSPHANOMETHYL)-3-(DI-M-XYLYLPHOS-
PHANO)-L-PROPANOL
(27A/B).111
5.2.39 DIASTEREOMERENGEMISCH AUS (-)-CAMPHANSAEURE-
(R)-2-(5-DIBENZOPHOSPHOLYLMETHYL)-2-(DI
-1
-NAPHTHYLPHOS-
PHANOMETHYL)-3-(DIPHENYLPHOSPHANO)-1
-PROPYL-ESTER
(28A)
UND
(-)-CAMPHANSAEURE-(S)-2-(5-DIBENZOPHOSPHOLYLMETHYL)-2-(DI-1
-
NAPHTHYLPHOSPHANOMETHYL)-3-(DIPHENYLPHOSPHANO)-1
-PROPYL-
ESTER
(28B)
.
112
5.2.40 RAC. PHTHALSAEURE-2-(5-DIBENZOPHOSPHOLYLMETHYL)-2-(DI
-1
-NAPHTYL-
PHOSPHANOMETHYL)-3-(DIPHENYLPHOSPHANO
)-1
-PROPYL-MONOESTER
(29)
.114
IV
5.2.41 [RAC. PHTHALSAEURE-2-(5-DIBENZOPHOSPHOLYLMETHYL)-2-(DI-1
-NAPHTHYL-
PHOSPHANOMETHYL)-3-(DIPHENYLPHOSPHANO)-1 -PROPYL-MONOESTER]-
EISEN(II)-TRIS(ACETONITRUE)-BIS(TETRAFLUOROBORAT)
(30)
.115
5.2.42 (-)-SPARTEIN-KATALYSIERTE OXETANSPALTUNGEN.117
5.2.42A DARSTELLUNG VON (R)- UND (S)-5C.118
5.2.42B DARSTELLUNG VON (R)- UND (S)-14C.118
5.3 ANGABEN ZUR HPLC.119
5.4 ROENTGENSTRUKTURANALYSEN.122
6 ZUSAMMENFASSUNG. .126
7 LITERATURVERZEICHNIS.133
ANHANG A:
1H-NMR-SPEKTREN.139
ANHANG B: DANK.
.152
ANHANG C: LEBENSLAUF.153
ANHANG D: FORMELUEBERSICHT.154 |
| any_adam_object | 1 |
| author | Seitz, Thomas |
| author_facet | Seitz, Thomas |
| author_role | aut |
| author_sort | Seitz, Thomas |
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| bvnumber | BV010433603 |
| ctrlnum | (OCoLC)258566323 (DE-599)BVBBV010433603 |
| edition | [Mikrofiche-Ausg.] |
| format | Microfilm Book |
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| genre | (DE-588)4113937-9 Hochschulschrift gnd-content |
| genre_facet | Hochschulschrift |
| id | DE-604.BV010433603 |
| illustrated | Illustrated |
| indexdate | 2024-10-09T16:19:17Z |
| institution | BVB |
| language | German |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-006952566 |
| oclc_num | 258566323 |
| open_access_boolean | |
| owner | DE-355 DE-BY-UBR DE-29T |
| owner_facet | DE-355 DE-BY-UBR DE-29T |
| physical | IV, 153 Bl. graph. Darst. |
| publishDate | 1994 |
| publishDateSearch | 1994 |
| publishDateSort | 1994 |
| record_format | marc |
| spelling | Seitz, Thomas Verfasser aut Chirale, tripodale Neopentyl-Tris(phosphan)-Liganden Synthese und Koordinationschemie von Thomas Seitz [Mikrofiche-Ausg.] 1994 IV, 153 Bl. graph. Darst. txt rdacontent h rdamedia he rdacarrier Heidelberg, Univ., Diss., 1994. - Mikrofiche-Ausg.: 3 Mikrofiches : 24x Neopentylgruppe (DE-588)4336495-0 gnd rswk-swf Phosphine (DE-588)4174379-9 gnd rswk-swf Tripodmetallkomplexe (DE-588)4283671-2 gnd rswk-swf (DE-588)4113937-9 Hochschulschrift gnd-content Phosphine (DE-588)4174379-9 s Neopentylgruppe (DE-588)4336495-0 s Tripodmetallkomplexe (DE-588)4283671-2 s DE-604 DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=006952566&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Seitz, Thomas Chirale, tripodale Neopentyl-Tris(phosphan)-Liganden Synthese und Koordinationschemie Neopentylgruppe (DE-588)4336495-0 gnd Phosphine (DE-588)4174379-9 gnd Tripodmetallkomplexe (DE-588)4283671-2 gnd |
| subject_GND | (DE-588)4336495-0 (DE-588)4174379-9 (DE-588)4283671-2 (DE-588)4113937-9 |
| title | Chirale, tripodale Neopentyl-Tris(phosphan)-Liganden Synthese und Koordinationschemie |
| title_auth | Chirale, tripodale Neopentyl-Tris(phosphan)-Liganden Synthese und Koordinationschemie |
| title_exact_search | Chirale, tripodale Neopentyl-Tris(phosphan)-Liganden Synthese und Koordinationschemie |
| title_full | Chirale, tripodale Neopentyl-Tris(phosphan)-Liganden Synthese und Koordinationschemie von Thomas Seitz |
| title_fullStr | Chirale, tripodale Neopentyl-Tris(phosphan)-Liganden Synthese und Koordinationschemie von Thomas Seitz |
| title_full_unstemmed | Chirale, tripodale Neopentyl-Tris(phosphan)-Liganden Synthese und Koordinationschemie von Thomas Seitz |
| title_short | Chirale, tripodale Neopentyl-Tris(phosphan)-Liganden |
| title_sort | chirale tripodale neopentyl tris phosphan liganden synthese und koordinationschemie |
| title_sub | Synthese und Koordinationschemie |
| topic | Neopentylgruppe (DE-588)4336495-0 gnd Phosphine (DE-588)4174379-9 gnd Tripodmetallkomplexe (DE-588)4283671-2 gnd |
| topic_facet | Neopentylgruppe Phosphine Tripodmetallkomplexe Hochschulschrift |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=006952566&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT seitzthomas chiraletripodaleneopentyltrisphosphanligandensyntheseundkoordinationschemie |