Functional analysis of lignins and their derivatives:
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| Main Author: | |
|---|---|
| Format: | Book |
| Language: | English Russian |
| Published: |
Atlanta, Ga.
Tappi Press
1994
|
| Edition: | 1. printing |
| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Physical Description: | VIII, 94 S. graph. Darst. |
| ISBN: | 0898522587 |
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MARC
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| 245 | 1 | 0 | |a Functional analysis of lignins and their derivatives |c G. F. Zakis |
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Record in the Search Index
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|---|---|
| adam_text | Functional Analysis of Lignins
and Their Derivatives
G F Zakis
Latvian Academy of Sciences
Institute of Wood Chemistry
Riga, Latvia
Translated by
Robert Porozny, Slovak Technical University, Bratislava, Slovakia
and
Thomas W Joyce, North Carolina State University, Raleigh, NC
TARPI
Atlanta, GA
TAPPI PRESS
©1994
Fachbibliothek Zellstoff und Papier
TU Darmstadt
lllll II III I 111
FAC !■? n ? ■ ■
ZSUsr:
tcJ - S
Contents
Preface v
List of abbreviations vi
Introduction vii
Chapter 1
Some physico-chemical properties of lignins
and their importance in sample preparation 1
Chapter 2
Methoxy groups 3
2 1 Method of Zeisel-Vieböck-Schwappach 3
2 2 Modification of Zeisel’s method using GLC 7
2 3 Method of Kirpal and Bühn 10
2 4 Methods based on methanol elimination 11
Chapter 3
Hydroxyl groups 13
3 1 Determination of hydroxyl groups by methylation 14
311 Methylation by diazomethane and alkaline
hydrolysis of methyl esters 14
312 Methylation by dimethyl sulfate 16
313 Methylation by methanol 18
314 Calculation of hydroxyl group content
from methylation results 18
3 2 Determination of hydroxyl groups by acylation 19
321 Acetylation 20
322 Phthalation 25
323 Specific character of analysis by
acylation methods of preparations
containing carboxyl groups : 26
324 Acetylation with subsequent aminolysis 29
3 3 Determination of hydroxyl groups
by Tserevitinov’s method 29
3 4 Determination of acidic hydroxyl groups
by chemisorption method 31
341 Total acidic groups 31
342 Highly acidic (carboxyl) groups 32
3 5 Acid-base titration 33
351 Potentiometrie titration 33
352 Conductometric titration 36
3 6 Spectrophotometric determination of phenol hydroxyl
groups (Ae method) 43
3 7 Determination of guaiacyl phenol groups
by oxidation with periodate 50
3 8 Determination of catechol structures 51
3 9 Determination of /7-hydroxy and /7-alkoxy benzyl
alcohol structures 54
3 10 Determination of carboxyl groups by
decarboxylation 57
3 11 Other methods of determination 58
Chapter 4
Carbonyl groups 61
4 1 Determination by oximation 61
4 2 Gasometric borohydride method 65
4 3 Spectrophotometric method and differentiation
of carbonyl groups 67
4 4 Determination of quinone carbonyl groups 71
4 5 Reduction of lignin preparations by complex
hydrides 74
Chapter 5
Determination of acidic groups in lignosulfonic acids 77
Chapter 6
Analysis of nitrogen-containing lignin derivatives 83
Appendices 87
Appendix A: Units of measurement for lignin
functional groups 87
Appendix B: Design of expanded empirical formulae
for the lignin phenylpropane structural unit 89
Literature cited 91
|
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| illustrated | Illustrated |
| indexdate | 2024-07-09T17:49:41Z |
| institution | BVB |
| isbn | 0898522587 |
| language | English Russian |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-006836553 |
| oclc_num | 30437267 |
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| owner | DE-M347 |
| owner_facet | DE-M347 |
| physical | VIII, 94 S. graph. Darst. |
| publishDate | 1994 |
| publishDateSearch | 1994 |
| publishDateSort | 1994 |
| publisher | Tappi Press |
| record_format | marc |
| spelling | Zakis, Girt F. Verfasser aut Funkcionalńyj analiz ligninov 1 1 ch proizvodnych Functional analysis of lignins and their derivatives G. F. Zakis 1. printing Atlanta, Ga. Tappi Press 1994 VIII, 94 S. graph. Darst. txt rdacontent n rdamedia nc rdacarrier Produtos naturais (quimica organica) larpcal Lignin Funktionelle Gruppe (DE-588)4155684-7 gnd rswk-swf Lignin (DE-588)4167660-9 gnd rswk-swf Lignin (DE-588)4167660-9 s Funktionelle Gruppe (DE-588)4155684-7 s DE-604 HEBIS Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=006836553&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Zakis, Girt F. Functional analysis of lignins and their derivatives Produtos naturais (quimica organica) larpcal Lignin Funktionelle Gruppe (DE-588)4155684-7 gnd Lignin (DE-588)4167660-9 gnd |
| subject_GND | (DE-588)4155684-7 (DE-588)4167660-9 |
| title | Functional analysis of lignins and their derivatives |
| title_alt | Funkcionalńyj analiz ligninov 1 1 ch proizvodnych |
| title_auth | Functional analysis of lignins and their derivatives |
| title_exact_search | Functional analysis of lignins and their derivatives |
| title_full | Functional analysis of lignins and their derivatives G. F. Zakis |
| title_fullStr | Functional analysis of lignins and their derivatives G. F. Zakis |
| title_full_unstemmed | Functional analysis of lignins and their derivatives G. F. Zakis |
| title_short | Functional analysis of lignins and their derivatives |
| title_sort | functional analysis of lignins and their derivatives |
| topic | Produtos naturais (quimica organica) larpcal Lignin Funktionelle Gruppe (DE-588)4155684-7 gnd Lignin (DE-588)4167660-9 gnd |
| topic_facet | Produtos naturais (quimica organica) Lignin Funktionelle Gruppe |
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