Particle size analysis in pharmaceutics and other industries: theory and practice
Saved in:
| Main Author: | |
|---|---|
| Format: | Book |
| Language: | English |
| Published: |
New York u.a.
Horwood
1992
|
| Series: | Ellis Horwood series in pharmaceutical technology
|
| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Physical Description: | 243 S. Ill., graph. Darst. |
| ISBN: | 0136516130 |
Staff View
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Record in the Search Index
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| adam_text | A PARTICLE SIZE ANALYSIS IN PHARMACEUTICS AND OTHER INDUSTRIES THEORY
AND PRACTICE CLIVE WASHINGTON, P H D DEPARTMENT OF PHARMACEUTICAL
SCIENCES, SCHOOL OF PHARMACY UNIVERSITY OF NOTTINGHAM ELLIS HORWOOD NEW
YORK LONDON TORONTO SYDNEY TOKYO SINGAPORE TABLE OF CONTENTS PREFACE 7
1. BASIC PRINCIPLES 9 RANGE OF PARTICLE SIZES AND UNITS 10 MEASURES OF
PARTICLE SIZE 10 DISTRIBUTIONS OF PARTICLE SIZES 12 INCREMENTAL AND
CUMULATIVE DISTRIBUTIONS 17 NUMBER, AREA AND MASS DISTRIBUTIONS 18
CHARACTERIZATION OF DISTRIBUTIONS 21 MEASURES OF CENTRAL TENDENCY 21
MOMENTS OF A DISTRIBUTION AND MOMENT NOTATION 23 MEASURES OF DISPERSION
25 MEASURES OF DISTRIBUTION SHAPE 26 MODEL DISTRIBUTIONS 26 THE NORMAL
DISTRIBUTION 27 THELOGNORMAL DISTRIBUTION 29 THE ROSIN-RAMMLER
DISTRIBUTION 30 IDENTIFICATION OF SPECIFIC DISTRIBUTIONS 31 PARTICLE
SHAPE 33 DESCRIPTIVE 34 DESCRIPTORS BASED ON DIRECT MEASUREMENT OF
DIMENSIONS 34 SHAPE FACTORS 35 FOURIER TRANSFORM METHODS 36 FRACTAL
CHARACTERIZATION OF PARTICLES 37 REFERENCES 39 2. SAMPLE SELECTION AND
PREPARATION 41 SAMPLE SELECTION 41 SELECTION OF PRIMARY SAMPLE 43
SAMPLING FROM FLOWING POWDERS 44 SAMPLING FROM STORED POWDERS 45
SAMPLING FROM LIQUIDS 47 SPLITTING THE PRIMARY SAMPLE 47 MANUAL METHODS
OF SAMPLE SPLITTING 47 MECHANICAL METHODS OF SAMPLE SPLITTING 48
DISPERSION OF MATERIALS 50 WETTING 51 DISINTEGRATION 54 STABILIZATION
AND FLOCCULATION 55 TABLE OF CONTENTS PRACTICAL TECHNIQUES FOR SAMPLE
DISPERSION 56 CALIBRATION AND REFERENCE STANDARDS 58 REFERENCES 59 3.
SIEVING 61 SIEVE SIZES AND RANGES 61 WHAT DOES SIEVING MEASURE? 62
METHODS OF SIEVE CONSTRUCTION 63 WOVEN SIEVES 63 ETCHED SIEVES 64
PUNCHED SIEVES 65 TECHNIQUES FOR USING SIEVES 65 WET SIEVING 65 HAND
SIEVING 67 MACHINE SIEVING 68 SONIC AND ULTRASONIC SIEVING 69 AIRJET
SIEVING 70 CLEANING OF SIEVES 72 CALIBRATION AND TESTING OF SIEVES 73
ERRORS AND PROBLEMS IN SIEVING 75 ERRORS IN THE SIEVE 75 SIEVE LOAD 75
SIEVING TIME 75 PROPERTIES OF THE FEEDSTOCK 76 WHEN TO USE SIEVING 77
REFERENCES 78 4. ELECTRICAL ZONE SENSING 79 PRINCIPLE OF OPERATION 79
SAMPLING HEAD OPERATION 81 APERTURE CONSTRUCTION AND MAINTENANCE 83
CALIBRATION 84 TECHNIQUES FOR THE USE OF THE COULTER COUNTER 86
OVERLAPPING RANGES 89 MASS BALANCE CHECKS 90 ELECTROLYTE SELECTION AND
PREPARATION 91 ERRORS IN ELECTRICAL ZONE SENSING 93 INTERFERENCE AND
VIBRATION 93 COINCIDENCE CORRECTION 95 PARTICLE PATH AND SHAPE 96
FLOCCULATION IN THE ELECTROLYTE 98 PARTICLE SEDIMENTATION 99
APPLICATIONS 99 PARTICLE COUNTING IN PARENTERALS 100 TABLE OF CONTENTS
PARENTERAL FAT EMULSIONS 101 REFERENCES 102 5. INTRODUCTION TO LIGHT
SCATTERING 105 LIGHT DIFFRACTION 106 SINGLE PARTICLE SCATTERING 107
PHOTON CORRELATION 107 6. THE ANGULAR DISTRIBUTION OF SCATTERED LIGHT
109 INTRODUCTION 109 THEORY OF LIGHT DIFFRACTION 110 OPTICAL PROPERTIES
OF MATERIALS 110 MIE THEORY ILL SCATTERING OF POLARIZED LIGHT 113
RAYLEIGH SCATTERING 114 RAYLEIGH-GANS-DEBYE (RGD) SCATTERING 116
FRAUNHOFER SCATTERING 116 ANOMALOUS SCATTERING 116 LASER DIFFRACTION
PARTICLE SIZERS 117 DATA PROCESSING 120 SAMPLE PREPARATION 122 DRY
POWDER FEEDERS 123 AEROSOL SIZING ACCESSORIES 123 CALIBRATION 125 ERRORS
AND DISADVANTAGES OF DIFFRACTION SIZE ANALYSIS 126 SUBMICROMETRE
RESOLUTION 127 MULTIPLE SCATTERING 128 FLOW AND REFRACTIVE INDEX
FLUCTUATIONS 129 COMPUTING ARTEFACTS 129 PARTICLE SHAPE 130 LASER SAFETY
131 OPTICS CLEANING 132 REFERENCES 133 7. PHOTON CORRELATION
SPECTROSCOPY 135 PRINCIPLE OF PHOTON CORRELATION 136 PARTICLE SIZE
DISTRIBUTIONS FROM PCS 140 CUMULANT ANALYSIS 143 HISTOGRAM METHOD 145
EXPONENTIAL SAMPLING METHOD 146 CONSTRAINED REGULARIZATION 147 MULTIPLE
ANGLE MEASUREMENT 147 EQUIPMENT FOR PHOTON CORRELATION 147 TABLE OF
CONTENTS THE LASER 148 THE SAMPLE OPTICS 149 THE DETECTOR 150 THE
CORRELATOR 151 SAMPLE PREPARATION 153 ERRORS IN PCS SIZE MEASUREMENT 154
ZETA POTENTIAL MEASUREMENT 155 OVERVIEW OF ZETA POTENTIAL 155 ZETA
POTENTIAL MEASUREMENT 156 EXPERIMENTAL ASPECTS 158 ELECTROACOUSTIC
ANALYSIS 163 APPLICATIONS 164 REFERENCES 165 8. PARTICLE SIZE ANALYSIS
OF AEROSOLS 169 INERTIALIMPACTION 170 SAMPLING AEROSOL GASES 173
GENERATION OF CALIBRATION AEROSOLS 175 IMPACTION PARTICLE SIZERS 176 THE
TWO-STAGE IMPINGER 176 THE ANDERSEN SAMPLER 178 SETTING UP AND
CALIBRATION 181 ERRORS OF ANDERSEN SAMPLER ANALYSIS 182 OPTICAL COUNTING
METHODS 184 LIGHT SCATTERING INTENSITY MEASUREMENTS 184 AERODYNAMIC
PARTICLE SIZERS 186 THE MALVERN AEROSIZER 186 PHASE DOPPLER ANEMOMETRY
188 MISCELLANEOUS TECHNIQUES 190 FILTRATION 190 NUCLEATION COUNTERS 191
REFERENCES 192 9. SEDIMENTATION 193 THEORY 194 LIMITATIONS OF STOKES
LAW 195 THE ANDREASEN PIPETTE 198 DATA ANALYSIS 200 SEDIMENTATION
BALANCES .!.. ... .L. .2O1 DATA ANALYSIS 202 PHOTOSEDIMENTATION
. . .. .!...! .2O4 X-RAY SEDIMENTATION !. . . . ! . . ! . !. !!. 207
CENTRIFUGAL SEDIMENTATION 209 TABLE OF CONTENTS DETERMINATION OF DENSITY
212 REFERENCES 214 10. MICROSCOPY AND IMAGE ANALYSIS 215 RESOLUTION 216
STATISTICAL CONSIDERATIONS 216 SAMPLE SELECTION AND PREPARATION 217
INSTRUMENTATION 219 ELECTRON MICROSCOPY 220 MANUAL METHODS 220
SEMIAUTOMATIC METHODS 222 AUTOMATIC IMAGE ANALYSIS 224 IMAGE PROCESSING
INSTRUMENTATION 224 IMAGE DISPLAY 228 IMAGE ENHANCEMENT 229 IMAGE
MEASUREMENT 231 FRACTAL MEASUREMENT 231 REFERENCES 234 INDEX 237
|
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| discipline | Chemie / Pharmazie |
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| illustrated | Illustrated |
| indexdate | 2024-07-09T17:44:59Z |
| institution | BVB |
| isbn | 0136516130 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-006641066 |
| oclc_num | 28510558 |
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| owner_facet | DE-355 DE-BY-UBR |
| physical | 243 S. Ill., graph. Darst. |
| publishDate | 1992 |
| publishDateSearch | 1992 |
| publishDateSort | 1992 |
| publisher | Horwood |
| record_format | marc |
| series2 | Ellis Horwood series in pharmaceutical technology |
| spelling | Washington, Clive Verfasser aut Particle size analysis in pharmaceutics and other industries theory and practice Clive Washington New York u.a. Horwood 1992 243 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Ellis Horwood series in pharmaceutical technology Chemistry Techniques, Analytical methods Particle Size Particle size determination Korngrößenanalyse (DE-588)4165322-1 gnd rswk-swf Pharmazie (DE-588)4045705-9 gnd rswk-swf Korngrößenanalyse (DE-588)4165322-1 s Pharmazie (DE-588)4045705-9 s DE-604 GBV Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=006641066&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Washington, Clive Particle size analysis in pharmaceutics and other industries theory and practice Chemistry Techniques, Analytical methods Particle Size Particle size determination Korngrößenanalyse (DE-588)4165322-1 gnd Pharmazie (DE-588)4045705-9 gnd |
| subject_GND | (DE-588)4165322-1 (DE-588)4045705-9 |
| title | Particle size analysis in pharmaceutics and other industries theory and practice |
| title_auth | Particle size analysis in pharmaceutics and other industries theory and practice |
| title_exact_search | Particle size analysis in pharmaceutics and other industries theory and practice |
| title_full | Particle size analysis in pharmaceutics and other industries theory and practice Clive Washington |
| title_fullStr | Particle size analysis in pharmaceutics and other industries theory and practice Clive Washington |
| title_full_unstemmed | Particle size analysis in pharmaceutics and other industries theory and practice Clive Washington |
| title_short | Particle size analysis in pharmaceutics and other industries |
| title_sort | particle size analysis in pharmaceutics and other industries theory and practice |
| title_sub | theory and practice |
| topic | Chemistry Techniques, Analytical methods Particle Size Particle size determination Korngrößenanalyse (DE-588)4165322-1 gnd Pharmazie (DE-588)4045705-9 gnd |
| topic_facet | Chemistry Techniques, Analytical methods Particle Size Particle size determination Korngrößenanalyse Pharmazie |
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