Quantitative x-ray fluorescence analysis: theory and application
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| Main Authors: | , |
|---|---|
| Format: | Book |
| Language: | English |
| Published: |
Chichester u.a.
Wiley
1995
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| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Physical Description: | XXII, 402 S. graph. Darst. |
| ISBN: | 0471951676 |
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Record in the Search Index
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| adam_text | QUANTITATIVE X-RAY FLUORESCENCE ANALYSIS THEORY AND APPLICATION GERALD
R. LACHANCE FORMERLY, GEOLOGICAL SURVEY OF CANADA FERNAND CLAISSE
CORPORDTION SCIENTIFIQUE CLAISSE, INC., QUEBEC, CANADA FORMERLY
PROFESSOR, DEPARTMENT OF MINING AND METALLURGY, UNIVERSITE LAVAL, CANADA
JOHN WILEY & SONS CHICHESTER * NEW YORK * BRISBANE * TORONTO * SINGAPORE
CONTENTS PREFACE XV SYMBOLS, DEFINITIONS AND TERMINOLOGY XIX PART I:
THEORY 1 CHAPTER 1. X-RAY PHYSICS 3 1.1 GENERAL CONSIDERATIONS 3 1.2
ATOMIC STRUCTURE 4 1.3 BINDING ENERGIES OF ORBITAL ELECTRONS 6 1.4*
CRITICAL EXCITATION ENERGY 8 1.5* CRITICAL EXCITATION WAVELENGTH 9 1.6*
CHARACTERISTIC X-RADIATIONS 9 1.7* EXCITATION SOURCES 11 1.7.1
EMANATIONS FROM X-RAY TUBES 12 1.7.2 THE CONTINUOUS SPECTRUM 12 1.7.3
CHARACTERISTIC X-RADIATIONS FROM THE TARGET ELEMENT 15 1.8* ATTENUATION
OF X-RAYS 18 1.8.1 EXPERIMENTAL DETERMINATION OF ^ 20 1.9* RELATION
BETWEEN X., Z AND X; ABSORPTION EDGES 21 1.10 SCATTERING OF X-RAYS 24
1.10.1 COHERENT SCATTER * * 24 1.10.2 INCOHERENT SCATTER 25 1.11* LINE
INTENSITIES; PROBABILITY OF EXCITATION 26 1.11.1 ABSORPTION JUMP RATIOS
27 1.11.2 RELATIVE LINE INTENSITIES WITHIN THE K, L AND M SERIES 28
1.11.3 FLUORESCENCE YIELD 30 1.12 DISCUSSION 31 1.13 SUMMARY 32 VIII
CONTENTS CHAPTER 2. X-RAY FLUORESCENCE EMISSIONS 33 2.1 GENERAL
CONSIDERATIONS 33 2.2 SPECTROMETER CONFIGURATIONS 34 2.3* PRIMARY
FLUORESCENCE 37 2.3.1 DESCRIPTION OF PRIMARY FLUORESCENCE 37 2.3.2
INTENSITY EXPRESSION FOR PRIMARY FLUORESCENCE 39 2.3.3 EXPERIMENTAL
VERIFICATION 44 2.3.4 PRIMARY FLUORESCENCE, POLYCHROMATIC EXCITATION
SOURCE 45 2.4* SECONDARY FLUORESCENCE 45 2.4.1 DESCRIPTION OF SECONDARY
FLUORESCENCE 45 2.4.2 INTENSITY EXPRESSION FOR SECONDARY FLUORESCENCE 47
2.4.3 EXPERIMENTAL VERIFICATION 49 2.4.4 SECONDARY FLUORESCENCE,
POLYCHROMATIC EXCITATION SOURCE 53 2.5 TERTIARY FLUORESCENCE 54 2.5.1
DESCRIPTION OF TERTIARY FLUORESCENCE 54 2.5.2 INTENSITY EXPRESSION FOR
TERTIARY FLUORESCENCE 55 2.6 RELATIVE CONTRIBUTION FROM PRIMARY,
SECONDARY AND TERTIARY EMISSIONS 58 2.7 DISCUSSION 59 2.8 SUMMARY 60
CHAPTER 3. THE FUNDAMENTAL PARAMETERS APPROACH 63 3.1 GENERAL
CONSIDERATIONS 63 3.2* CONCEPT OF THE FUNDAMENTAL PARAMETERS APPROACH 64
3.2.1 REPLACING INTEGRALS BY FINITE SUMMATIONS 64 3.2.2 SPECTRAL
DISTRIBUTIONS 65 3.2.3 ITERATION PROCEDURE 66 3.3 CLASSICAL FORMALISM 67
3.3.1 PRIMARY EMISSION 67 3.3.1.1 NUMERICAL EXAMPLE OF THE CALCULATION
OF P (I ) AND PI 68 3.3.2 SECONDARY EMISSION 70 3.3.2.1 NUMERICAL
EXAMPLE OF THE CALCULATION OF (PI + SIJ)X 70 3.3.2.2 EXPERIMENTAL
CONFIRMATION 74 3.4* ALTERNATE FORMALISM 76 3.4.1 PRIMARY FLUORESCENCE
EMISSION 77 3.4.1.1 NUMERICAL EXAMPLE 79 3.4.2 SECONDARY FLUORESCENCE
EMISSION 80 3.4.2.1 NUMERICAL EXAMPLE 82 CONTENTS IX 3.4.3 GENERAL
EXPRESSION 83 3.4.3.1 NUMERICAL EXAMPLE 83 3.5 DISCUSSION 86 3.5.1 MONTE
CARLO MODEL 86 3.5.2 GENERAL EXPRESSION FOR QUANTITATIVE X-RAY
FLUORESCENCE ANALYSIS 87 3.5.2.1 NUMERICAL EXAMPLES 89 3.6* SUMMARY 90
CHAPTER 4. FUNDAMENTAL INFLUENCE COEFFICIENTS 93 4.1 GENERAL
CONSIDERATIONS 93 4.2 THE CONCEPT OF INFLUENCE COEFFICIENTS 94 4.3 THE
DOMAIN OF FUNDAMENTAL INFLUENCE COEFFICIENTS 95 4.4 INITIAL DEVELOPMENTS
95 4.4.1 VON HAMOS 95 4.4.2 BEATTIE AND BRISSEY 96 4.4.3 LACHANCE AND
TRAILL 97 4.5 INTRODUCING POLYCHROMATIC EXCITATION 97 4.5.1 CLAISSE AND
QUINTIN 97 4.5.2 LACHANCE 98 4.6* FUNDAMENTAL INFLUENCE COEFFICIENT
ALGORITHMS 99 4.6.1 TERTIAN AND BROIL-TERTIAN FORMALISMS 100 4.6.2
ROUSSEAU FORMALISM 102 4.6.3 LACHANCE FORMALISM 104 4.6.4 DE JONGH
FORMALISM 105 4.7 NUMERICAL EXAMPLES 107 4.7.1 EFFECT OF TARGET MATERIAL
109 4.7.2 EFFECT OF INSTRUMENTAL GEOMETRY 111 4.7.3 EFFECT OF SPECIMEN
COMPOSITION 112 4.7.4 EFFECT OF CHARACTERISTIC TUBE TARGET LINES 112
4.7.5 BINARY AWJJ ARRAYS 115 4.7.6 FUNDAMENTAL INFLUENCE COEFFICIENTS,
MULTIELEMENT SPECIMENS 116 4.8 DISCUSSION 120 4.9 SUMMARY 121 CHAPTER 5.
ALPHA COEFFICIENT CONCEPT 125 5.1 GENERAL CONSIDERATIONS 125 5.2 CONCEPT
AND DOMAIN OF ALPHA COEFFICIENTS 126 5.3 CONCEPT OF THEORETICAL
INFLUENCE COEFFICIENTS 129 5.4* EXTENSION TO POLYCHROMATIC EXCITATION
130 5.4.1 BINARY WIJ INFLUENCE COEFFICIENT ARRAYS 132 X CONTENTS 5.5*
LINEAR APPROXIMATION OF BINARY MY ARRAYS 134 5.5.1 NUMERICAL EXAMPLE 138
5.6* HYPERBOLIC APPROXIMATIONS OF BINARY MY ARRAYS 139 5.6.1 NUMERICAL
EXAMPLE 140 5.7* THIRD ELEMENT EFFECT 143 5.7.1 CROSS-COEFFICIENT
FORMALISMS 144 5.7.2 TERTIAN FORMALISM 146 5.7.3 NUMERICAL EXAMPLES 147
5.8 DISCUSSION 152 5.8.1 THE EQUIVALENT WAVELENGTH CONCEPT 152 5.8.2
VARIATION OF AY WITH SPECIMEN COMPOSITION 153 5.8.3 LIMITED THEORETICAL
JUSTIFICATION OF ALPHA COEFFICIENT MODELS 154 5.9 SUMMARY 156 CHAPTER 6.
EMPIRICAL INFLUENCE COEFFICIENTS 159 6.1 GENERAL CONSIDERATIONS 159 6.2
CONCEPT AND DOMAIN OF EMPIRICAL INFLUENCE COEFFICIENTS 160 6.3*
CRISS-BIRKS AND LACHANCE-TRAILL FORMALISMS 161 6.4* METHOD OF RASBERRY
AND HEINRICH 163 6.5* METHOD OF LUCAS-TOOTH AND PRICE 166 6.6* METHOD OF
LUCAS-TOOTH AND PYNE 168 6.7 THE JAPANESE INDUSTRIAL STANDARD METHOD 170
6.8* DISCUSSION 171 6.9 SUMMARY 173 CHAPTER 7. GLOBAL MATRIX EFFECT
CORRECTION APPROACHES 175 7.1 GENERAL CONSIDERATIONS 175 7.1.1
ANALYTICAL CONTEXT 176 7.2* THE DOUBLE DILUTION METHOD 177 7.2.1
PRINCIPLE OF THE METHOD 177 7.2.1.1 NUMERICAL EXAMPLE 179 7.2.2 EFFECT
OF ENHANCEMENT 181 7.2.3 PRACTICAL CONSIDERATIONS 183 7.3* COMPTON
(INCOHERENT) SCATTER METHODS 183 7.3.1 THEORETICAL CONSIDERATIONS 184
7.3.1.1 NUMERICAL EXAMPLE 187 7.4 THE INTERNAL STANDARD METHOD 190 7.4.1
NUMERICAL EXAMPLE 191 7.5* THE STANDARD ADDITION METHOD 193 7.5.1
NUMERICAL EXAMPLE 194 CONTENTS 7.6* 7.7* 7.8 7.9 THE HIGH DILUTION-HEAVY
ABSORBER METHOD 7.6.1 NUMERICAL MATRIX MATCHING 7.7.1 NUMERICAL
DISCUSSION SUMMARY EXAMPLE METHODS EXAMPLE XI 195 196 199 200 201 202
CHAPTER 8. SPECIAL ANALYTICAL CONTEXTS 203 8.1 GENERAL CONSIDERATIONS
203 8.2* LOW Z ANALYTES AND MATRICES 204 8.2.1 LOW Z ANALYTES 204 8.2.2
LOW Z MATRICES 205 8.3 LIMITED SAMPLE QUANTITY 208 8.4* THIN SPECIMENS
209 8.5* THIN FILMS 211 8.5.1 DETERMINATION OF FILM THICKNESS 211
8.5.1.1 NUMERICAL EXAMPLES 212 8.5.2 MULTI-LAYER THIN FILMS 215 86
PARTICULATES 216 8.7 OXIDE SYSTEMS 216 8.7.1 NUMERICAL EXAMPLE 217 8.8*
FUSED DISC SPECIMENS 219 8.8.1 INFLUENCE COEFFICIENTS MODIFIED FOR FLUX
219 8.8.1.1 NUMERICAL EXAMPLE 221 8.8.2 CORRECTION FOR LOSS ON FUSION
(LOF) 224 8.8.2.1 NUMERICAL EXAMPLE 225 8.8.3 CORRECTION FOR GAIN ON
FUSION (GOF) 227 8.8.3.1 NUMERICAL EXAMPLE 229 8.8.4 GENERAL THEORY OF
LOF AND GOF 231 8.8.4.1 NUMERICAL EXAMPLE 233 8.9 LIQUIDS 236 8.10
CONCLUSIONS 237 CHAPTER 9. ANALYTICAL STRATEGIES 239 9.1 GENERAL
CONSIDERATIONS 239 9.2 ANALYTICAL CONTEXT 241 9.2.1 NATURE OF SAMPLES
SUBMITTED 242 9.2.2 INSTRUMENTAL RESOURCES 242 9.2.3 SAMPLE COMPOSITION
243 9.2.4 PRECISION AND ACCURACY 243 9.3* SPECIMEN PREPARATION 245 9.3.1
BULK SOLIDS*ALLOYS, GLASSES, PLASTICS, CERAMICS 245 XLL 9.4* 9.5* 9.6*
9.7 9.3.2 PRESSED POWDER PELLETS 9.3.3 FUSED DISCS 9.3.4 LIQUIDS
INTENSITY MEASUREMENTS 9.4.1 PRECISION, COUNTING STATISTICS 9.4.2
EXCITATION SOURCE SELECTION 9.4.3 LINE SELECTION 9.4.4 COLLIMATION 9.4.5
CRYSTAL SELECTION 9.4.6 DETECTOR SELECTION 9.4.7 CORRECTION FOR
BACKGROUND 9.4.8 CORRECTION FOR SPECTRAL INTERFERENCE 9.4.9 CORRECTION
FOR DEAD TIME CALIBRATION 9.5.1 DEFINITION 9.5.2 MATHEMATICAL MODELS THE
ANALYTICAL PROCESS 9.6.1 CONFIRMATION OF THE VALIDITY OF A CALIBRATION
9.6.2 COUNTING MONITORS 9.6.2.1 NUMERICAL EXAMPLE 9.6.3 QUALITY CONTROL
9.6.4 ANALYTICAL PRECISION AND THE DETECTION LIMIT 9.6.5 SOFTWARE
SUMMARY CONTENTS 246 247 250 251 251 252 253 253 254 254 255 256 258 259
260 261 266 266 267 268 270 271 273 275 PART II: APPLICATION 279 II. 1
X-RAY PHYSICS 281 II. 1.4 CRITICAL EXCITATION (BINDING) ENERGIES 281 II.
1.5 CRITICAL EXCITATION (ABSORPTION EDGE) WAVELENGTHS 282 II. 1.6
ENERGIES AND WAVELENGTHS OF CHARACTERISTIC X-RADIATIONS 283 II. 1.7.1
EXPERIMENTALLY MEASURED SPECTRAL DISTRIBUTIONS 284 II. 1.8.1
EXPERIMENTAL DETERMINATION OF //. 285 II. 1.8.2 ALGORITHMS FOR
GENERATING L VALUES 286 II. 1.9 GENERATING /* AS A FUNCTION OF Z AND X
290 II. 1.11.1 ABSORPTION JUMP RATIOS; ABSORPTION JUMP FACTORS 294 II.
1.11.2 RELATIVE LINE INTENSITIES WITHIN SERIES 295 11.1.11.3
FLUORESCENCE YIELDS 296 1.1.12 SUMMARY AND CONCLUSIONS 297 II.2 X-RAY
FLUORESCENCE EMISSIONS 299 II.2.1 TWO-THETA VALUES FOR CHARACTERISTIC
LINES 299 CONTENTS XLLL 11.2.2 EXCITATION PROBABILITY FACTOR 299 11.2.3
EXPERIMENTAL VERIFICATION OF PRIMARY EMISSION 301 11.2.4 EXPERIMENTAL
VERIFICATION OF SECONDARY EMISSION 302 11.2.5 SUMMARY 305 11.3 THE
FUNDAMENTAL PARAMETERS APPROACH 307 II.3.2 CONCEPT OF THE FUNDAMENTAL
PARAMETERS APPROACH 307 II.3.2.3 THE ITERATIVE PROCESS 311 II.3.4
COMPREHENSIVE TABULATION OF PI + SI, A VI AND E V] DATA 313 11.3.6
SUMMARY AND CONCLUSIONS 322 11.4 FUNDAMENTAL INFLUENCE COEFFICIENTS 323
11.4.6.1 BROIL-TERTIAN FORMALISM 323 11.4.6.2 ROUSSEAU FORMALISM 324
11.4.6.3 LACHANCE FORMALISM 325 11.4.6.4 THE DE JONGH FORMALISM 327
11.4.6.5 TYPICAL ANALYTICAL PROCEDURE 330 11.4.6.6 INTERRELATION BETWEEN
FUNDAMENTAL INFLUENCE COEFFICIENTS 333 II.4. 6.1 SUMMARY AND CONCLUSIONS
336 11.5 ALPHA INFLUENCE COEFFICIENTS 337 11.5.4 THE LACHANCE-TRAILL
ALGORITHM 338 11.5.5 THE MODIFIED CLAISSE-QUINTIN ALGORITHM 340 II 5 7
1 THE C O L A A1 8 ORITHM 344 LL L T , THE TERTIAN ALGORITHM 348 11.6
EMPIRICAL INFLUENCE COEFFICIENTS 351 11.6.3 THE LACHANCE-TRAILL MODEL:
EQN (6.7) 351 II.6.3.1 NUMERICAL EXAMPLE 354 11.6.4 THE
RASBERRY-HEINRICH MODEL: EQN (6.11) 355 11.6.5 THE LUCAS-TOOTH AND PRICE
MODEL: EQN (6.14) 357 11.6.6 LUCAS-TOOTH AND PYNE MODEL: EQN (6.17) 358
II.6.8 DISCUSSION 358 11.7 GLOBAL MATRIX EFFECT CORRECTION METHODS 361
11.7.2 DOUBLE DILUTION METHOD: EQN (7.20) 361 11.7.3 COMPTON
(INCOHERENT) SCATTER METHODS: EQN (7.30) 362 II.7.5 STANDARD ADDITION
METHOD 364 XIV CONTENTS 11.7.6 HIGH DILUTION-HEAVY ABSORBER METHOD 365
11.7.7 MATRIX MATCHING METHODS 365 11.8 SPECIAL ANALYTICAL CONTEXTS 367
II.8.2 LOW Z ANALYTES AND MATRICES 367 11.8.4 THIN SPECIMENS 368 11.8.5
THIN FILMS, FILM THICKNESS 369 11.8.8 FUSED DISC SPECIMENS 370 11.9
ANALYTICAL STRATEGIES 371 11.9.1 STEELS, NICKEL-BASE, COPPER-BASE, BROAD
MIXTURES 372 11.9.2 CEMENTS AND RAW MATERIALS IN THE CEMENT INDUSTRY 374
11.9.3 GEOLOGICAL CONTEXTS 378 11.9.4 DISCUSSION AND SUMMARY 383
REFERENCES AND BIBLIOGRAPHY 387 AUTHOR INDEX 395 SUBJECT INDEX 398
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| id | DE-604.BV009973550 |
| illustrated | Illustrated |
| indexdate | 2024-07-09T17:44:11Z |
| institution | BVB |
| isbn | 0471951676 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-006609049 |
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| physical | XXII, 402 S. graph. Darst. |
| publishDate | 1995 |
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| publisher | Wiley |
| record_format | marc |
| spelling | Lachance, Gerald R. Verfasser aut Quantitative x-ray fluorescence analysis theory and application Gerald R. Lachance ; Fernand Claisse Chichester u.a. Wiley 1995 XXII, 402 S. graph. Darst. txt rdacontent n rdamedia nc rdacarrier X-ray spectroscopy X-ray spectroscopy Industrial applications Röntgenfluoreszenzspektroskopie (DE-588)4135992-6 gnd rswk-swf Röntgenfluoreszenzspektroskopie (DE-588)4135992-6 s DE-604 Claisse, Fernand Verfasser aut GBV Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=006609049&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Lachance, Gerald R. Claisse, Fernand Quantitative x-ray fluorescence analysis theory and application X-ray spectroscopy X-ray spectroscopy Industrial applications Röntgenfluoreszenzspektroskopie (DE-588)4135992-6 gnd |
| subject_GND | (DE-588)4135992-6 |
| title | Quantitative x-ray fluorescence analysis theory and application |
| title_auth | Quantitative x-ray fluorescence analysis theory and application |
| title_exact_search | Quantitative x-ray fluorescence analysis theory and application |
| title_full | Quantitative x-ray fluorescence analysis theory and application Gerald R. Lachance ; Fernand Claisse |
| title_fullStr | Quantitative x-ray fluorescence analysis theory and application Gerald R. Lachance ; Fernand Claisse |
| title_full_unstemmed | Quantitative x-ray fluorescence analysis theory and application Gerald R. Lachance ; Fernand Claisse |
| title_short | Quantitative x-ray fluorescence analysis |
| title_sort | quantitative x ray fluorescence analysis theory and application |
| title_sub | theory and application |
| topic | X-ray spectroscopy X-ray spectroscopy Industrial applications Röntgenfluoreszenzspektroskopie (DE-588)4135992-6 gnd |
| topic_facet | X-ray spectroscopy X-ray spectroscopy Industrial applications Röntgenfluoreszenzspektroskopie |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=006609049&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT lachancegeraldr quantitativexrayfluorescenceanalysistheoryandapplication AT claissefernand quantitativexrayfluorescenceanalysistheoryandapplication |