Experimental mass spectrometry:
Saved in:
| Format: | Book |
|---|---|
| Language: | English |
| Published: |
New York u.a.
Plenum Press
1994
|
| Series: | Topics in mass spectrometry
1 |
| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Physical Description: | XIII, 311 S. graph. Darst. |
| ISBN: | 0306444577 |
Staff View
MARC
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| 245 | 1 | 0 | |a Experimental mass spectrometry |c ed. by David H. Russell |
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Record in the Search Index
| _version_ | 1804124135685619712 |
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| adam_text | EXPERIMENTAL MASS SPECTROMETRY EDITED BY DAVID H. RUSSELL DEPARTMENT OF
CHEMISTRY TEXAS A&M UNIVERSITY COLLEGE STATION, TEXAS PLENUM PRESS * NEW
YORK AND LONDON CONTENTS 1. THE FRAGMENTATIONS OF (M-H) IONS DERIVED
FROM ORGANIC COMPOUNDS: AN AID TO STRUCTURE DETERMINATION JOHN H. BOWIE
1. INTRODUCTION 1 2. FRAGMENTATION OF ORGANIC FUNCTIONAL GROUPS 4 2.1.
HYDROCARBONS AND HALOCARBONS 4 2.2. ALCOHOLS AND PHENOLS 7 2.3. ETHERS 9
2.4. ALDEHYDES AND KETONES 13 2.5. CARBOXYLIC ACIDS 16 2.6. ESTERS 18
2.7. ORGANONITROGEN COMPOUNDS 20 3. CLASSIFICATION OF FRAGMENTATIONS OF
EVEN-ELECTRON ORGANIC NEGATIVE IONS 32 3.1. FRAGMENTATIONS INVOLVING
RADICAL LOSS 33 3.2. FRAGMENTATIONS PROCEEDING DIRECTLY THROUGH AN ION
COMPLEX 33 3.3. FRAGMENTATIONS FOLLOWING PROTON TRANSFER TO THE INITIAL
ANION 33 3.4. FRAGMENTATIONS OCCURRING FOLLOWING SKELETAL REARRANGEMENT
34 3.5. UNCLASSIFIED FRAGMENTATIONS 34 REFERENCES 34 IX X CONTENTS 2.
GAS-PHAS E CHEMISTRY OF ALKALI ADDUCTS OF SIMPLE AND COMPLEX MOLECULES
LYNN M. TEESCH AND JEANETTE ADAMS 1. INTRODUCTION 39 2. SIMPLE MOLECULES
40 3. MULTIFUNCTIONAL MOLECULES 43 3.1. FATTY ACIDS AND RELATED
COMPOUNDS 44 3.2. MONOSACCHARIDES AND OLIGOSACCHARIDES 48 3.3. PEPTIDES
58 4. CONCLUSIONS 67 REFERENCES 68 3. FUNDAMENTAL STUDIES OF
COLLISION-INDUCED DISSOCIATION OF IONS ANIL K. SHUKLA AND JEAN H.
FUTRELL 1. INTRODUCTION 71 2. COLLISION-INDUCED DISSOCIATION: A TWO-STEP
PROCESS 76 3. REACTION KINEMATICS 77 4. DATA PRESENTATION 80 5. SELECTED
RESULTS 84 5.1. THE HYDROGEN MOLECULAR ION: A COMPARISON OF THEORY AND
EXPERIMENTS 84 5.2. PROPANE CATION CID 87 5.3. NON-RRKM CID PROCESSES 97
6. CONCLUSIONS AND PROSPECTS 109 REFERENCES 110 4. MULTIPLE PULSES AND
DIMENSIONS IN FTICR TINO GAEUMANN 1. INTRODUCTION 113 2. EXCITATION 118
CONTENTS XI 3. COLLISIONAL ACTIVATION 121 4. EJECTION 123 5. PULSING THE
PRESSURE 124 6. PHOTOFRAGMENTATION 127 7. MULTIPLE DIMENSIONS 129 8.
HADAMARD TRANSFORM 130 9. TWO-DIMENSIONAL SPECTROSCOPY 139 10.
CONCLUSIONS 147 REFERENCES 14 8 5. EXPERIMENTAL FOURIER TRANSFORM ION
CYCLOTRON RESONANCE MASS SPECTROSCOPY DAVID A. LAUDE, JR. AND STEVEN C.
BEU 1. INTRODUCTION 153 2. SINGLE-SECTION CELL FTICR EXPERIMENT 154 2.1.
SIMPLE ION MOTION IN THE TRAPPED ION CELL 154 2.2. ION EXCITATION AND
DETECTION 157 2.3. FTICR LINE-SHAPE SIGNAL PROCESSING 158 3. THE MODERN
FTICR EXPERIMENT 160 3.1. MAGNET AND VACUUM CHAMBER CONSIDERATIONS 160
3.2. THE TRAPPED-ION CELL 162 3.3. DIFFERENTIAL-PUMPING CONFIGURATIONS
164 3.4. SAMPLE INTRODUCTION 168 3.5. FTICR IONIZATION 170 3.6. ION
EXCITATION 174 3.7. ION DISSOCIATION 178 3.8. FTICR PULSE SEQUENCES 182
4. FTICR PERFORMANCE 184 4.1. ION TRAPPING 184 4.2. MASS RESOLUTION 185
4.3. MASS MEASUREMENT ACCURACY 186 4.4. MASS RANGE 188 5. EXPERIMENTAL
LIMITATIONS TO THE FTICR MEASUREMENT 189 5.1. PRESSURE BROADENING 189
5.2. SPACE-CHARGE 190 5.3. RADIAL-TRAPPING FIELDS 190 XII CONTENTS 6.
CONCLUSION 191 REFERENCES 192 6. ELUCIDATION OF PROTEIN STRUCTURE AND
PROCESSING USING TIME-OF-FLIGHT MASS SPECTROMETRY AMINA WOODS, RONG
WANG, MARC CHEVRIER, TIM CORNISH, CATHY WOLKOW, AND ROBERT J. COTTER 1.
INTRODUCTION 199 1.1. PLASMA DESORPTION MASS SPECTROMETRY 201 1.2.
MATRIX-ASSISTED LASER DESORPTION 203 2. INSTRUMENTATION AND STRATEGIES
204 2.1. THE BIO-ION PLASMA DESORPTION MASS SPECTROMETER 205 2.2.
MATRIX-ASSISTED LASER DESORPTION USING A 600-PSEC N 2 LASER 206 2.3.
BASIC STRATEGIES FOR PROTEIN/PEPTIDE ANALYSIS 207 3. STRUCTURE OF
PORPOISE RELAXIN 209 3.1. MOLECULAR WEIGHT MEASUREMENTS 210 3.2.
ENZYMATIC DIGESTION AND PEPTIDE MAPPING 211 3.3. CARBOXYPEPTIDASE AND
AMINOPEPTIDASE DIGESTION 214 4. REACTIONS OF BRCCL 3 WITH HEMOGLOBIN 216
4.1. DIGESTION WITH ELASTASE 217 4.2. ON-FOIL DIGESTION WITH
AMINOPEPTIDASE 217 5. CLEAVAGE OF THE AMYLOID PRECURSOR PROTEIN 220 5.1.
DETERMINING THE CLEAVAGE SITE OF APP DURING NORMAL PROCESSING 221 5.2.
CARBOXYPEPTIDASE DIGESTION 222 5.3. SYNTHETIC C-TERMINAL FRAGMENT 223 6.
PROCESSING THE ASSEMBLY PROTEIN FROM CYTOMEGALOVIRUS 224 6.1.
DETERMINING THE CLEAVAGE SITE 224 7. INSERTION PEPTIDES USED IN X-RAY
CRYSTALLOGRAPHIC STUDIES 227 8. DEVELOPING A TANDEM TIME-OF-FLIGHT MASS
SPECTROMETER 231 8.1. MASS RESOLUTION 233 8.2. THE DESKTOP TANDEM
TIME-OF-FLIGHT MASS SPECTROMETER 234 8.3. RESULTS OF THE LINEAR PORTION
OF MSI 236 8.4. RESULTS FOR REFLECTED IONS IN MSI 236 9. CONCLUSIONS 238
REFERENCES 239 CONTENTS XIII 7. ELECTROSPRAY LONIZATION MASS
SPECTROMETRY AND TANDEM MASS SPECTROMETRY OF LARGE BIOMOLECULES JOSEPH
A. LOO, CHARLES G. EDMONDS, RACHEL R. OGORZAIEK LOO, HAMID R. UDSETH,
AND RICHARD D. SMITH 1. INTRODUCTION 243 2. PRINCIPLES AND PRACTICE OF
ELECTROSPRAY LONIZATION 245 2.1. ELECTROSPRAY LONIZATION PROCESS 245
2.2. ATMOSPHERIC PRESSURE ESI SOURCE 247 2.3. ATMOSPHERE/VACUUM
INTERFACE 249 2.4. ESI MASS SPECTROMETERS 251 3. ESI-MASS SPECTROMETRY
252 3.1. POSITIVE-ION ESI-MS OF PROTEINS AND M R DETERMINATION ... 252
3.2. EFFECTS OF HIGHER ORDER STRUCTURE ON ESI CHARGE STATE DISTRIBUTION
261 3.3. NEGATIVE ION ESI MS 264 4. DISSOCIATION OF ESI-GENERATED
MULTIPLY CHARGED IONS 268 5. INTERFACE WITH CAPILLARY SEPARATION SCHEMES
278 6. CONCLUSIONS 281 REFERENCES 282 8. LIQUID CHROMATOGRAPHY/FAST ATOM
BOMBARDMENT MASS SPECTROMETRY JUSTIN G. STROH AND KENNETH L. RINEHART 1.
INTRODUCTION 287 2. MOVING BELT INTERFACE 288 2.1. DESIGN AND OPERATION
OF THE MOVING BELT INTERFACE 288 2.2. APPLICATIONS OF THE MOVING BELT
INTERFACE 292 3. CONTINUOUS FLOW FAB 298 3.1. DESIGN OF THE CONTINUOUS
FLOW FAB INTERFACE 298 3.2. APPLICATIONS OF THE CONTINUOUS FLOW FAB
INTERFACE 301 4. PARTICLE BEAM/FAB 303 5. CONCLUSION 304 REFERENCES 304
INDEX 307
|
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| illustrated | Illustrated |
| indexdate | 2024-07-09T17:40:51Z |
| institution | BVB |
| isbn | 0306444577 |
| language | English |
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| physical | XIII, 311 S. graph. Darst. |
| publishDate | 1994 |
| publishDateSearch | 1994 |
| publishDateSort | 1994 |
| publisher | Plenum Press |
| record_format | marc |
| series | Topics in mass spectrometry |
| series2 | Topics in mass spectrometry |
| spelling | Experimental mass spectrometry ed. by David H. Russell New York u.a. Plenum Press 1994 XIII, 311 S. graph. Darst. txt rdacontent n rdamedia nc rdacarrier Topics in mass spectrometry 1 Massaspectrometrie gtt Mass Spectrometry Mass spectrometry Massenspektrometrie (DE-588)4037882-2 gnd rswk-swf Massenspektrometrie (DE-588)4037882-2 s DE-604 Russell, David H. Sonstige oth Topics in mass spectrometry 1 (DE-604)BV009787414 1 GBV Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=006475100&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Experimental mass spectrometry Topics in mass spectrometry Massaspectrometrie gtt Mass Spectrometry Mass spectrometry Massenspektrometrie (DE-588)4037882-2 gnd |
| subject_GND | (DE-588)4037882-2 |
| title | Experimental mass spectrometry |
| title_auth | Experimental mass spectrometry |
| title_exact_search | Experimental mass spectrometry |
| title_full | Experimental mass spectrometry ed. by David H. Russell |
| title_fullStr | Experimental mass spectrometry ed. by David H. Russell |
| title_full_unstemmed | Experimental mass spectrometry ed. by David H. Russell |
| title_short | Experimental mass spectrometry |
| title_sort | experimental mass spectrometry |
| topic | Massaspectrometrie gtt Mass Spectrometry Mass spectrometry Massenspektrometrie (DE-588)4037882-2 gnd |
| topic_facet | Massaspectrometrie Mass Spectrometry Mass spectrometry Massenspektrometrie |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=006475100&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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