Nuclear magnetic resonance in solid polymers:
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| Main Authors: | , |
|---|---|
| Format: | Book |
| Language: | English |
| Published: |
Cambridge
Cambridge Univ. Press
1993
|
| Edition: | 1. publ. |
| Series: | Cambridge solid state science series
|
| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Physical Description: | XXII, 347 S. Ill., graph. Darst. |
| ISBN: | 0521301408 9780521031721 9780521301404 0521031729 |
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Record in the Search Index
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| adam_text | NUCLEAR MAGNETIC RESONANCE IN SOLID POLYMERS VINCENT J. MCBRIERTY
PROFESSOR OF POLYMER PHYSICS, TRINITY COLLEGE, DUBLIN AND KENNETH J.
PACKER CHIEF SCIENTIST, BRITISH PETROLEUM CO. P.L.C. * CAMBRIDGE **
UNIVERSITY PRESS CONTENTS PREFACE PAGE XV ACKNOWLEDGEMENTS XVIII
GLOSSARY OF TERMS XIX 1 THE NMR OF SOLID POLYMERS: AN OVERVIEW 1 1.1 THE
NATURE OF POLYMERS 1 1.2 THE ROLE OF NMR 2 1.3 STRUCTURAL
CONSIDERATIONS: A MODEL FOR THE POLYMER 5 1.4 MOLECULAR MOTION: AN
OVERVIEW 8 1.5 COMPARISON WITH OTHER RELAXATION EXPERIMENTS: TRANSITION
MAPS 11 2 BASIC CONCEPTS IN NMR 16 2.1 NUCLEAR MAGNETISATION 16 2.2 THE
RADIOFREQUENCY (RF) FIELD 19 2.3 RF PULSES AND NUCLEAR MAGNETIC
RELAXATION 22 2.4 NMR SIGNALS: THE FREE INDUCTION DECAY (FID) 23 2.5
SPIN TEMPERATURE 26 2.6 SPIN COUPLINGS, LINESHAPES AND MOTIONAL
AVERAGING 29 2.6.1 SPIN COUPLINGS 30 2.6.1.1 MAGNETIC DIPOLE-DIPOLE
COUPLING 30 2.6.1.2 MAGNETIC SHIELDING 33 2.6.1.3 NUCLEAR ELECTRIC
QUADRUPOLE COUPLING 35 2.6.2 MOTIONAL AVERAGING 36 2.7 SPIN-LATTICE
RELAXATION AND MOTION 38 2.7.1 DIPOLAR RELAXATION BETWEEN LIKE SPINS 39
2.7.2 DIPOLAR RELAXATION BETWEEN UNLIKE SPINS 44 2.7.3 RELAXATION DUE TO
ELECTRIC QUADRUPOLE INTERACTIONS 48 2.8 SUMMARY 49 3 NUCLEAR SPIN
INTERACTIONS 51 3.1 GENERAL CONSIDERATIONS 51 IX X CONTENTS 3.2
COORDINATE SYSTEMS 52 3.3 GENERAL EXPRESSION FOR THE INTERNAL
HAMILTONIANS 54 3.3.1 THE CHEMICAL SHIFT 54 3.3.2 NUCLEAR QUADRUPOLE
INTERACTIONS 55 3.3.3 DIPOLAR INTERACTIONS 56 3.4 SPECTRAL LINESHAPES 57
3.5 MOMENTS OF RIGID SPECTRAL LINESHAPES 59 3.5.1 MOMENTS EXPANSION OF
THE FID 62 3.6 EFFECTS OF MOTION ON SPECTRA 63 3.6.1 ROTATION ABOUT AN
AXIS AND MAGIC-ANGLE SPINNING 64 3.6.2 ROTATIONAL SPIN ECHOES IN SOLIDS
65 3.6.3 RAPID ROTATION ABOUT AN ARBITRARY MOLECULAR AXIS 66 3.6.4 SOME
IDEALISED MOTIONS ENCOUNTERED IN POLYMERS 67 3.7 NMR RELAXATION IN
SOLIDS 69 3.7.1 DIPOLAR RELAXATION IN SOLIDS 69 3.7.2 DISTRIBUTION OF
CORRELATION TIMES 71 3.8 SPIN DIFFUSION 73 3.8.1 OFF-RESONANCE
EXPERIMENTS 76 3.8.2 DILUTE SPIN SYSTEMS 76 3.8.3 DIFFUSION-LIMITED
RELAXATION 77 3.8.4 GEOMETRICAL CONSIDERATIONS 78 3.8.5 RELAXATION TO
PARAMAGNETIC CENTRES 78 3.9 OVERVIEW AND SUMMARY 81 4 EXPERIMENTAL
METHODS 8 2 4.1 SPECTROMETER CHARACTERISTICS 83 4.2 NMR PROBES FOR
SOLIDS 86 4.3 SAMPLE-SPINNING DEVICES 88 4.4 PULSE SEQUENCES 90 4.4.1
SINGLE-RESONANCE EXPERIMENTS 90 4.4.1.1 SINGLE-PULSE DETERMINATION OF
SPECTRA 90 4.4.1.2 SPECTRAL MOMENTS 93 4.4.1.3 SPIN-ECHO EXPERIMENTS 93
4.4.1.4 SPIN-LATTICE RELAXATION EXPERIMENTS 95 4.4.2 DOUBLE-RESONANCE
EXPERIMENTS 102 4.4.2.1 SINGLE-PULSE EXCITATION (SPE) 102 4.4.2.2 CROSS
POLARISATION (CP) 103 4.4.2.3 DIPOLAR DEPHASING/NON-QUATERNARY
SUPPRESSION (NQS) 106 4.4.2.4 DELAYED CONTACT AND RELATED EXPERIMENTS
108 4.4.2.5 DILUTE-SPIN SPIN-LATTICE RELAXATION 109 4.4.2.6 FACTORS
AFFECTING RESOLUTION 110 CONTENTS XI 4.4.2.7 FACTORS AFFECTING
QUANTITATIVE MEASUREMENTS 115 4.5 MULTIDIMENSIONAL NMR IN SOLIDS 118
4.5.1 TWO-DIMENSIONAL NMR IN SOLIDS 118 4.5.2 THREE-DIMENSIONAL NMR IN
SOLIDS 122 5 STRUCTURE AND MOTION IN SOLID POLYMERS 124 5.1 INTRODUCTION
124 5.2 HIGH-RESOLUTION 13 C NMR SPECTROSCOPY OF SOLID POLYMERS 126
5.2.1 13 C CHEMICAL SHIFTS IN SOLID POLYMERS 127 5.2.1.1 CONFORMATIONAL
EFFECTS 127 5.2.1.2 CRYSTALLOGRAPHIC EFFECTS 131 5.3 NMR STRUCTURAL
INVESTIGATIONS OF SOLID POLYMERS 133 5.3.1 CELLULOSE AND ITS DERIVATIVES
133 5.3.2 TACTICITY OF SOLID POLY(VINYL ALCOHOL) 135 5.3.3 THE STRUCTURE
OF INSOLUBLE POLYMERIC RESINS 137 5.3.4 STRUCTURAL HETEROGENEITY 145
5.3.5 SPECIALIST METHODS FOR STRUCTURE DETERMINATION 150 5.4 MOLECULAR
MOTIONS IN SOLID POLYMERS 153 5.4.1 POLYETHYLENE TEREPHTHALATE) AND
RELATED POLYMERS 156 5.4.2 POLYSTYRENES 165 5.4.3 POLYCARBONATES 174
5.4.4 POLYETHYLENE 179 5.4.5 POLY(VINYLIDENE FLUORIDE) 187 5.4.6 EPOXY
POLYMERS 188 6 STRUCTURAL HETEROGENEITY IN POLYMERS 191 6.1 EXPERIMENTAL
PROBES OF HETEROGENEITY: AN OVERVIEW 191 6.2 NMR AS A STRUCTURAL PROBE
194 6.2.1 SPIN DIFFUSION AND STRUCTURAL HETEROGENEITY 195 6.3 NATURE OF
THE INTERFACE 202 6.4 HETEROGENEITY IN HOMOPOLYMERS 206 6.4.1
POLYETHYLENE 207 6.4.2 POLYETHYLENE TEREPHTHALATE) 211 6.5
AMORPHOUS-AMORPHOUS POLYMER BLENDS 213 6.5.1 MODIFIED
POLYSTYRENE-METHACRYLATE SYSTEMS 214 6.5.2 POLY(VINYL
CHLORIDE)-POLY(METHYL METHACRYLATE) 216 6.5.3 POLYSTYRENE-POLY(VINYL
METHYL ETHER) 218 6.5.4 POLYETHYLENE TEREPHTHALATE)-BISPHENOL A
POLYCARBONATE 223 6.6 AMORPHOUS-CRYSTALLINE POLYMER BLENDS 223 6.6.1
POLYVINYL CHLORIDE)-POLY(E-CAPROLACTONE) 223 6.6.2 POLY(VINYLIDENE
FLUORIDE)-POLY(METHYL METHACRYLATE) 226 XLL CONTENTS 6.7
CRYSTALLINE-CRYSTALLINE POLYMER BLENDS 227 6.7.1
POLYETHYLENE-POLYPROPENE 228 6.8 BLOCK COPOLYMERS 228 6.8.1
POLYSTYRENE-POLYBUTADIENE-POLYSTYRENE 229 6.8.2 POLYURETHANES 231 6.9
POLYMER-DILUENT SYSTEMS 233 6.9.1 PLASTICISED POLYVINYL CHLORIDE) 234
6.9.2 PLASTICISED D 8 -POLY(METHYL METHACRYLATE) 235 7 ORIENTED POLYMERS
238 7.1 INTRODUCTORY REMARKS 238 7.2 NATURE OF THE DISTRIBUTION 240
7.2.1 SYMMETRY CONSIDERATIONS 240 7.2.2 THEORETICAL DISTRIBUTION
FUNCTIONS 243 7.3 NMR OF ORIENTED POLYMERS 244 7.3.1 DIPOLAR LINEWIDTH
STUDIES 245 7.3.2 CHEMICAL SHIFT ANISOTROPY 247 7.3.3 QUADRUPOLE
LINESHAPE ANALYSIS 249 7.3.4 ANALYSIS OF TWO-DIMENSIONAL MAS SPECTRA 251
7.4 ORIENTATION IN POLYETHYLENE 251 7.5 ORIENTATION IN
POLYTETRAFLUOROETHYLENE 258 7.6 ORIENTATION IN POLY(ETHYLENE
TEREPHTHALATE) 262 7.7 POLYMER LIQUID CRYSTALS 265 7.8 SECONDARY LOCAL
PROBES OF ORIENTATION 267 8 SELECTED TOPICS 269 8.1 NETWORK SYSTEMS 269
8.1.1 FILLED ELASTOMERS 270 8.1.1.1 SILOXANE-SILICA SYSTEMS 270 8.1.1.2
CARBON BLACK-ELASTOMER SYSTEMS 272 8.2 WATER IN POLYMERS 277 8.3
IONOMERS 284 8.4 ELECTRICALLY ACTIVE POLYMERS 288 8.4.1 CONDUCTING
POLYMERS 288 8.4.1.1 DOPED AND UNDOPED POLYACETYLENE 290 8.4.2
PIEZOELECTRIC POLYMERS 291 8.4.3 FERROELECTRIC POLYMERS 295 APPENDIX 1
DATA ON COMMON POLYMERS 297 APPENDIX 2 TH E ROTATION OPERATOR 303
APPENDIX 3 ROTATION OF TENSORS BETWEEN COORDINATE FRAMES 307 CONTENTS **
APPENDIX 4 SPATIAL DISTRIBUTION OF STRUCTURAL UNITS IN A POLYMER 308
APPENDIX 5 THE INTERNAL HAMILTONIAN 309 APPENDIX 6 SPECTRAL LINESHAPES
312 APPENDIX! ANALYSIS OF SPINNING SIDEBANDS 314 BIBLIOGRAPHY 316
REFERENCES 320 AUTHOR INDEX 337 SUBJECT INDEX 342
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| illustrated | Illustrated |
| indexdate | 2024-07-09T17:26:44Z |
| institution | BVB |
| isbn | 0521301408 9780521031721 9780521301404 0521031729 |
| language | English |
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| physical | XXII, 347 S. Ill., graph. Darst. |
| publishDate | 1993 |
| publishDateSearch | 1993 |
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| publisher | Cambridge Univ. Press |
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| series2 | Cambridge solid state science series |
| spelling | McBrierty, Vincent J. Verfasser (DE-588)137978898 aut Nuclear magnetic resonance in solid polymers Vincent J. McBrierty and Kenneth J. Packer 1. publ. Cambridge Cambridge Univ. Press 1993 XXII, 347 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Cambridge solid state science series Polymères - Analyse Spectroscopie de la résonance magnétique nucléaire Nuclear magnetic resonance spectroscopy Polymers Analysis Festkörper-NMR-Spektroskopie (DE-588)4713583-9 gnd rswk-swf Polymere (DE-588)4046699-1 gnd rswk-swf Polymere (DE-588)4046699-1 s Festkörper-NMR-Spektroskopie (DE-588)4713583-9 s DE-604 Packer, Kenneth J. Verfasser aut GBV Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=005881227&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | McBrierty, Vincent J. Packer, Kenneth J. Nuclear magnetic resonance in solid polymers Polymères - Analyse Spectroscopie de la résonance magnétique nucléaire Nuclear magnetic resonance spectroscopy Polymers Analysis Festkörper-NMR-Spektroskopie (DE-588)4713583-9 gnd Polymere (DE-588)4046699-1 gnd |
| subject_GND | (DE-588)4713583-9 (DE-588)4046699-1 |
| title | Nuclear magnetic resonance in solid polymers |
| title_auth | Nuclear magnetic resonance in solid polymers |
| title_exact_search | Nuclear magnetic resonance in solid polymers |
| title_full | Nuclear magnetic resonance in solid polymers Vincent J. McBrierty and Kenneth J. Packer |
| title_fullStr | Nuclear magnetic resonance in solid polymers Vincent J. McBrierty and Kenneth J. Packer |
| title_full_unstemmed | Nuclear magnetic resonance in solid polymers Vincent J. McBrierty and Kenneth J. Packer |
| title_short | Nuclear magnetic resonance in solid polymers |
| title_sort | nuclear magnetic resonance in solid polymers |
| topic | Polymères - Analyse Spectroscopie de la résonance magnétique nucléaire Nuclear magnetic resonance spectroscopy Polymers Analysis Festkörper-NMR-Spektroskopie (DE-588)4713583-9 gnd Polymere (DE-588)4046699-1 gnd |
| topic_facet | Polymères - Analyse Spectroscopie de la résonance magnétique nucléaire Nuclear magnetic resonance spectroscopy Polymers Analysis Festkörper-NMR-Spektroskopie Polymere |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=005881227&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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