Chemical analysis for the arson investigator and attorney:
Saved in:
| Main Authors: | , , |
|---|---|
| Format: | Book |
| Language: | German |
| Published: |
Heidelberg
Hüthig
1993
|
| Series: | Chromatographic methods
|
| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Physical Description: | ca. 440 S. |
| ISBN: | 3778518909 |
Staff View
MARC
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Record in the Search Index
| _version_ | 1804122471135182848 |
|---|---|
| adam_text | CHEMICAL ANALYSIS FOR THE ARSON INVESTIGATOR AND ATTORNEY BY WOLFGANG
BERTSCH GUNTHER HOLZER CLARA SUZANNE SELLERS HIITHIG BUCH VERLAG
HEIDELBERG CONTENTS PREFACE V 1 FIRE INVESTIGATION, ACCELERANTS AND 1
CHEMICAL ANALYSIS. HOW DO THE PIECES OF THE PUZZLE FIT TOGETHER? 1.1
INTRODUCTORY REMARKS 1 1.2 FIRE AND ARSON. ASSESSING THE MAGNITUDE OF
THE PROBLEM ....2 1.3 THE CRIME OF ARSON. WHY, WHO, AND HOW? 7 1.4 THE
FIRE INVESTIGATION 11 1.4.1 ON-SITE DETECTION OF ACCELERANTS 16 1.4.2
MANIPULATION OF FIRE DEBRIS SAMPLES 18 PACKAGING AND PRESERVATION 1.4.3
REPORTING 19 1.5 A LAYMAN S PERSPECTIVE OF FIRE AND OF 19 CHEMICAL
LABORATORY ANALYSIS METHODS. WHY DO FIRES OCCUR? WHERE DOES THE CHEMIST
FIT IN? 1.5.1 A PRIMER ON FIRE. WHAT CHEMICAL AND 20 PHYSICAL PROCESSES
ARE RESPONSIBLE FOR FIRES? 1.5.2 THE SCOPE OF CHEMICAL ANALYSIS FOR
ACCELERANTS 24 WHAT IS AN ACCELERANT AND HOW CAN THE CHEMIST FIND IT?
1.5.3 TECHNICAL ASPECTS OF ANALYSIS. ARE THERE 28 INSTRUMENTS FOR THE
DETECTION OF ACCELERANTS DIRECTLY AT THE FIRE SCENE? WHY IS IT NECESSARY
TO CARRY OUT CHEMICAL ANALYSIS IN THE LABORATORY RATHER THAN IN THE
FIELD? 1.5.3.1 SAMPLE PREPARATION. WHAT IS DONE TO A FIRE 28 DEBRIS
SAMPLE BEFORE IT IS ANALYZED? WHAT METHODS ARE AVAILABLE? 1.5.3.2
INSTRUMENTAL ANALYSIS. HOW DOES ANALYTICAL 30 INSTRUMENTATION WORK? WHAT
SORT OF RESULTS DOES IT PRODUCE? ARE THESE MACHINES RELIABLE? 1.5.3.3
DATA INTERPRETATION. HOW DOES THE CHEMIST DECIDE 33 WHETHER A FIRE
DEBRIS SAMPLE CONTAINS AN ACCELERANT? 1.6 ETHICAL AND PROFESSIONAL
ISSUES 39 CONTENTS 1.6.1 PROFESSIONAL ETHICS 39 1.6.2 THE CHEMIST AS
FORENSIC EXPERT 42 1.6.3 THE ATTORNEY AS EXAMINER OF SCIENTIFIC DATA 46
REFERENCES 51 2 FIRE, MATTER, AND ACCELERANTS. AN INTRODUCTION 55 TO
PHYSICAL AND CHEMICAL PRINCIPLES 2.1 INTRODUCTION 55 2.2 THE CHEMISTRY
OF FIRE AND ACCELERANTS 56 2.2.1 MATTER AND MEASUREMENT. AN INTRODUCTION
56 TO SCIENTIFIC PRINCIPLES 2.2.2 ATOMS AND ELEMENTS 59 2.2.3 MOLECULES
AND IONS. THE NATURE OF CHEMICAL BONDS 64 2.2.4 PRINCIPLES OF CHEMICAL
REACTIONS 68 2.2.5 GAS LAWS. OXIDIZERS AND EXPLOSIVE REACTIONS 77 2.2.6
THE CHEMISTRY OF FIRE FIGHTING 86 2.3 THE FATE OF RESIDUAL ACCELERANT
AFTER A FIRE 89 2.4 AN INTRODUCTION TO ORGANIC CHEMISTRY 91 2 4.1
ALIPHATIC HYDROCARBONS 92 2.4.1.1 NORMAL AND BRANCHED ALKANES 92 2.4.1.2
CYCLOALKANES 96 2.4.2 UNSATURATED HYDROCARBONS. ALKENES 96 2.4.3
AROMATIC HYDROCARBONS 99 2.4.4 ALCOHOLS 102 2 4 5 ETHERS 105 2.4.6
ALDEHYDES, KETONES, AND ESTERS 106 2.4.7 TERPENES 108 2.4.8 SUBSTANCES
CONTAINING HETEROATOMS AND MIXED 108 FUNCTIONAL GROUPS 2.5 POLYMERS 111
2.5.1 POLYMERS DERIVED FROM PLANTS AND ANIMALS ILL 2.5.2 SYNTHETIC
POLYMERS 114 2.6 PETROLEUM BASED CHEMICALS 121 2.6.1 THE ORIGIN OF
PETROLEUM 121 2.6.2 REFINERY PROCESSES 22 2.6.3 CHEMICAL REACTIONS IN
PETROLEUM REFINING 129 2.6.4 PROPERTIES AND USES OF PETROLEUM
DISTILLATES 136 A DESCRIPTION OF PHYSICAL, CHEMICAL, AND CHROMATOGRAPHIC
CHARACTERISTICS 2.6.5 COMBUSTION PROPERTIES OF FUELS 155 2.7
CLASSIFICATION OF ACCELERANTS 157 2.7.1 LIQUID ACCELERANTS 157 2.7.2
SOLID ACCELERANTS, OXIDIZERS AND MISCELLANEOUS SOLIDS ..162 CONTENTS XI
2.8 PHYSICAL PHENOMENA IN THE COMBUSTION OF SOLIDS 166 2.8.1 FUNDAMENTAL
PROCESSES 166 2.8.2 THERMAL DEGRADATION OF SOLIDS 166 2.8.3 FLAMING AND
GLOWING COMBUSTION 168 2.8.4 SPONTANEOUS COMBUSTION 169 2.8.5 SOURCES OF
HEAT 170 2.8.6 HEAT TRANSFER 171 REFERENCES 173 3 LABORATORY METHODS 177
3.1 THE ANALYTICAL PROBLEM 177 3.2 SAMPLE PREPARATION AND ACCELERANT
RECOVERY 178 TECHNIQUES 3.2.1 PERSPECTIVE 178 3.2.2 PHYSICAL PRINCIPLES
OF ACCELERANT RECOVERY 182 3.2.2.1 SOLVENT EXTRACTION 186 3.2.2.2
DISTILLATION 188 3.2.2.3 HEADSPACE METHODS 191 3.2.2.3.1 DIRECT
HEADSPACE METHODS 191 3.2.2.3.2 STATIC HEADSPACE METHODS BASED ON
ADSORBENTS 195 3.2.2.3.3 DYNAMIC HEADSPACE METHODS BASED ON ADSORBENTS
196 3.2.2.3.4 AUTOMATED EQUIPMENT. ON-LINE CONCENTRATORS 208 3.2.3
COMPARISON OF TECHNIQUES. ENRICHMENT FACTORS 212 3.2.4 PRECOLUMN
TREATMENT AND CLEANUP PROCEDURES 215 3.3 INSTRUMENTAL METHODS OF
ANALYSIS 217 3.3.1 PERSPECTIVE 217 3.3.2 FUNDAMENTALS OF GAS
CHROMATOGRAPHY 221 3.3.2.1 BASIC CONCEPTS 223 3.3.2.1.1 COLUMN
TECHNOLOGY 234 3.3.2.1.2 COLUMN SELECTION CRITERIA 240 3.3.2.2 THE
PRACTICE OF GAS CHROMATOGRAPHY 246 3.3.2.3 SAMPLE INTRODUCTION 253
3.3.2.4 DETECTORS 260 3.3.2.4.1 FLAME IONIZATION DETECTOR (FID) 264
3.3.2.4.2 THERMAL CONDUCTIVITY DETECTOR (TCD) 265 3.3.2.4.3
PHOTOIONIZATION DETECTOR (PID) 267 3.3.2.4.4 FLAME PHOTOMETRIC DETECTOR
(FPD) 268 3.3.2.4.5 ELECTRON CAPTURE DETECTOR (ECD) 270 3.3.2.4.6
NITROGEN PHOSPHORUS DETECTOR (NPD) 271 3.3.2.4.7 OXYGEN SPECIFIC FLAME
IONIZATION DETECTOR (OFID) 272 3.3.2.4.8 OTHER DETECTORS 273 3.3.2.5
RECORDERS AND DATA SYSTEMS 274 3.3.2.5.1 POTENTIOMETRIC RECORDERS 275
XII CONTENTS 3.3.2.5.2 MICROPROCESSOR BASED INTEGRATORS 276 3.3.2.5.3
PERSONAL COMPUTER BASED SYSTEMS AND WORKSTATIONS 277 3.3.3 GAS
CHROMATOGRAPHY AND HYPHENATED TECHNIQUES 278 3.3.3.1 FUNDAMENTALS OF
MASS SPECTROMETRY 282 3.3.3.2 INSTRUMENTATION IN MASS SPECTROMETRY 284
3.3.3.3 GAS CHROMATOGRAPHY/MASS SPECTROMETRY 293 3.3.3.4 OPERATIONAL
ASPECTS OF GAS CHROMATOGRAPHY/MASS 297 SPECTROMETRY 3.3.3.4.1 TUNING AND
CALIBRATION 297 3.3.3.4.2 DATA ACQUISITION 297 3.3.3.4.3 DATA PROCESSING
299 3.3 3.4.4 OPERATION AND OPTIMIZATION IN GAS 301 CHROMATOGRAPHY/MASS
SPECTROMETRY 3.3.4 THE MASS SPECTROMETER AS ACCELERANT SPECIFIC DETECTOR
..302 3.3.5 GAS CHROMATOGRAPHY AND OTHER SPECTROMETERS 308 GC/FTIR AND
GC/AED 3.3.6 GENERAL SPECTROSCOPIC METHODS 316 3.3.7 INSTRUMENTAL
METHODS FOR OXIDIZERS, SOLID 319 ACCELERANTS, AND OTHER SOLIDS
INCENDIARIES 3.3.8 FUTURE DEVELOPMENTS IN INSTRUMENTATION 321 REFERENCES
323 4 METHODS DEVELOPMENT, QUALITY ASSURANCE ..................333 AND
LABORATORY PROTOCOL 4.1 PRELIMINARY REMARKS 333 4.2 A SUMMARY OF CURRENT
METHODS IN THE INDUSTRY 333 4.3 SELECTION AND IMPLEMENTATION OF
LABORATORY METHODS ....345 4.3.1 CRITERIA FOR ESTABLISHMENT OF A
LABORATORY METHOD 345 4.3.2 SOURCES OF INTERFERENCES IN THE FIELD AND
LABORATORY 347 4.3.2.1 PYROLYSIS 347 4.3.2.2 ACCELERANT TYPE COMPOUNDS
IN MATRIXES AND 356 IN THE ENVIRONMENT 4.3.2.3 BURN EXPERIMENTS AND
ACCELERANT RECOVERY STUDIES 364 4.4 METHOD VERIFICATION AND LABORATORY
PROTOCOL 369 4.4.1 IMPLEMENTATION AND OPTIMIZATION OF GENERAL 369
LABORATORY METHODS 4.4.2 ADVANCED CONCEPTS 372 4.4.2.1 THE USE OF
PRECISION INDEXES 372 4.4.2.2 MULTICOLUMN CHROMATOGRAPHY 374 REFERENCES
376 5 EVALUATION AND INTERPRETATION OF DATA ........................379
5.1 PRELIMINARY REMARKS 379 CONTENTS XIII 5.2 AN INTRODUCTION TO PATTERN
RECOGNITION 379 5.2.1 PATTERN RECOGNITION BY VISUAL INSPECTION OF 380
CHROMATOGRAMS 5.2.2 COMPUTER ASSISTED PATTERN RECOGNITION 383 5.3 A
GC/MS BASED EXPERT SYSTEM 385 5.3.1 ASPECTS OF AUTOMATION 388 5.3.2 PEAK
IDENTIFICATION ROUTINE 392 5.3.3 MASS SPECTRAL CRITERIA OR ACCELERANT
COMPONENTS 397 5.4 EVALUATION OF CHROMATOGRAPHIC PROFILES FROM 406 FIRE
DEBRIS SAMPLES AND SIMULATED ARSON SAMPLES 5.4.1 PETROLEUM BASED
ACCELERANTS 406 5.4.1.1 LIGHT PETROLEUM DISTILLATES (LPD) 406 5.4.1.2
GASOLINE 406 5.4.1.3 MEDIUM PETROLEUM DISTILLATES (MPD) 417 5.4.1.4
KEROSENE 421 5.4.1.5 HEAVY PETROLEUM DISTILLATES (HPD) 427 5.4.1.6 LAMP
OILS 431 5.4.1.7 NAPHTHENIC CHARCOAL LIGHTER FLUIDS 432 5.4.1.8
PETROLEUM BASED INDUSTRIAL SOLVENTS AND 433 LACQUER THINNERS 5.4.1.9
LIQUID ACCELERANTS OTHER THAN PETROLEUM DISTILLATES 436 5 4.1.10
TURPENTINE 437 REFERENCES 439 6 P APPENDIX 441 6.1 GLOSSARY OF TERMS IN
PHYSICAL/CHEMICAL 441 CHARACTERIZATION OF FIRES, MATERIALS, ACCELERANTS,
SAMPLE PREPARATION, CHROMATOGRAPHY, AND MASS SPECTROMETRY 6.2 CONVERSION
FACTORS 474 6.3 ACCELERANT LIBRARY 475 INDEX 517
|
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| id | DE-604.BV008097477 |
| illustrated | Not Illustrated |
| indexdate | 2024-07-09T17:14:24Z |
| institution | BVB |
| isbn | 3778518909 |
| language | German |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-005334868 |
| oclc_num | 634276114 |
| open_access_boolean | |
| owner | DE-355 DE-BY-UBR |
| owner_facet | DE-355 DE-BY-UBR |
| physical | ca. 440 S. |
| publishDate | 1993 |
| publishDateSearch | 1993 |
| publishDateSort | 1993 |
| publisher | Hüthig |
| record_format | marc |
| series2 | Chromatographic methods |
| spelling | Bertsch, Wolfgang Verfasser aut Chemical analysis for the arson investigator and attorney by Wolfgang Bertsch ; Günther Holzer ; Clara Suzanne Sellers Heidelberg Hüthig 1993 ca. 440 S. txt rdacontent n rdamedia nc rdacarrier Chromatographic methods Chemische Analyse (DE-588)4009840-0 gnd rswk-swf Brandstiftung (DE-588)4007981-8 gnd rswk-swf Brandstiftung (DE-588)4007981-8 s Chemische Analyse (DE-588)4009840-0 s DE-604 Holzer, Günther Verfasser aut Sellers, Clara Suzanne Verfasser aut GBV Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=005334868&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Bertsch, Wolfgang Holzer, Günther Sellers, Clara Suzanne Chemical analysis for the arson investigator and attorney Chemische Analyse (DE-588)4009840-0 gnd Brandstiftung (DE-588)4007981-8 gnd |
| subject_GND | (DE-588)4009840-0 (DE-588)4007981-8 |
| title | Chemical analysis for the arson investigator and attorney |
| title_auth | Chemical analysis for the arson investigator and attorney |
| title_exact_search | Chemical analysis for the arson investigator and attorney |
| title_full | Chemical analysis for the arson investigator and attorney by Wolfgang Bertsch ; Günther Holzer ; Clara Suzanne Sellers |
| title_fullStr | Chemical analysis for the arson investigator and attorney by Wolfgang Bertsch ; Günther Holzer ; Clara Suzanne Sellers |
| title_full_unstemmed | Chemical analysis for the arson investigator and attorney by Wolfgang Bertsch ; Günther Holzer ; Clara Suzanne Sellers |
| title_short | Chemical analysis for the arson investigator and attorney |
| title_sort | chemical analysis for the arson investigator and attorney |
| topic | Chemische Analyse (DE-588)4009840-0 gnd Brandstiftung (DE-588)4007981-8 gnd |
| topic_facet | Chemische Analyse Brandstiftung |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=005334868&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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