Chemical methods of rock analysis:
Saved in:
| Main Author: | |
|---|---|
| Format: | Book |
| Language: | English |
| Published: |
Oxford [u.a.]
Pergamon Press
1970
|
| Edition: | 1. ed. |
| Series: | International series of monographs on analytical chemistry
36 |
| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Physical Description: | XV, 509 S. Ill., graph. Darst. |
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| _version_ | 1804121415342882816 |
|---|---|
| adam_text | Titel: Chemical methods of rock analysis
Autor: Jeffery, Paul G
Jahr: 1970
CONTENTS
Acknowledgements xv
Chapter 1. The Composition of Sock Material 1
Introduction 1
International standards 4
Elements determined 8
Reporting an analysis 10
Chapter 2. Sample Preparation 13
Selection of material 13
Crushing and grinding 15
Contamination 16
Fine grinding of micas 18
Sample material for trace-element determinations 19
Chapter 3. Sample Decomposition 20
Extraction procedures 21
Extraction with water 21
Extraction with organic solvents 21
Decomposition with mineral acids 21
Decomposition with hydrochloric acid 21
Decomposition with nitric acid 22
Decomposition with hydrofluoric acid 22
Fusion procedures 24
Fusion with alkali fluoride 24
Fusion with potassium pyrosulphate 24
Fusion with sodium carbonate 25
Fusion with alkali hydroxide 27
Sinter or fusion with sodium peroxide 29
Fusion with boric oxide and alkali borates 30
Miscellaneous decomposition procedures 32
Fire assay for gold and silver 32
Miscellaneous fluxes 32
Chapter 4. Classical Scheme for tibe Analysis of Silicate Rocks 34
Introduction 34
Decomposition of the sample 35
The determination of silica 37
Separation and collection of silica 37
Ignition and volatilisation of silica 38
The determination of mixed oxides 40
Precipitation of the mixed oxides 40
Recovery of the aluminium traces 41
Ignition of the mixed oxides 42
Recovery of silica traces 42
Determination of aluminium by difference 43
The determination of calcium 43
The determination of magnesium 44
Determination of manganese in the magnesium residue 46
Chapter 5. The Rapid Analysis of Silicate Rocks 48
Introduction 48
Individual schemes of rapid rock analysis 54
Schemes of Shapiro and Brannock 54
Scheme of Riley 54
Scheme of Langmyhr and Graff 55
Scheme of Ingamells 56
Chapter 6. Some Statistical Considerations 59
Classification of errors 59
Precision and accuracy 60
Confidence limits 64
The significance of results 65
The z» test 68
Chapter 7. The Alkali Metals 72
Occurrence 72
Determination in silicate rocks and minerals 73
Gravimetric methods 73
Flame photometry 74
Atomic absorption spectroscopy 76
Chromatographic separation of the alkali metals 78
The determination of sodium and potassium in silicate rocks 79
The determination of lithium 82
Small amounts of alkali metals in ultrabasic rocks 82
The determination of potassium in micas 84
The decomposition of silicate rocks and minerals by the
method of J. Lawrence Smith 85
The determination of rubidium and caesium 89
Chapter 8. Aluminium 93
Occurrence 93
The determination of aluminium in silicate rocks 93
Gravimetric methods 93
Titrimetric determination 95
Photometric determination 96
Atomic absorption spectroscopy 98
98
98
100
100
100
100
102
104
105
108
108
108
109
112
112
113
113
114
115
118
119
122
122
127
127
128
128
128
129
133
133
134
134
135
137
140
141
147
148
148
149
149
The separation of aluminium
Extraction procedures
Precipitation with sodium hydroxide
Ion-exchange separation
Electrolysis with a mercury cathode
The gravimetric determination with 8-hydroxyquinoline
The titrimetric determination with CyDTA
The photometric determination with 8-hydroxyquinoline
Hie photometric determination with pyrocatechol violet
Antimony
Occurrence
The determination of antimony in silicate rocks
Polarographic determination
Arsenic
Occurrence
The determination of arsenic in silicate rocks
The separation of arsenic
Photometric determination
A molybdenum blue method using acid digestion
A molybdenum blue method using a fusion
An arsine-molybdenum blue method
Method using silver diethyldithiocarbamate
Method using co-crystallisation with thionalide
Barium
Occurrence
The determination of barium in silicate rocks
Gravimetric method
Determination by flame photometry
Gravimetric determination as sulphate
Beryllium
Occurrence
Warning
The determination of beryllium
Gravimetric determination as phosphate
Photometric determination with berylion II
Precipitation as phosphate with titanium as collector
Fluorimetrie determination of beryllium with morin
Bismuth
Boron
Occurrence
The determination of boron
The separation of boron
The determination of boron in tourmaline 150
The determination of boron in silicate rocks 151
Chapter 15. Cadmium 155
Occurrence 155
The determination in silicate rocks 155
Chapter 16. Calcium 158
Occurrence 158
The determination of calcium as oxalate 158
Classical gravimetric procedure 158
Direct gravimetric determination 159
The separation of strontium 161
Titrimetric determination with permanganate 161
Titrimetric determination with EDTA 162
The determination of calcium in carbonate rocks 163
Photometric determination of calcium in silicate rocks 164
The determination of calcium by flame photometry 165
The determination of calcium by atomic absorption
spectroscopy 166
Chapter 17. Carbon 167
Occurrence 167
Carbon dioxide 167
The determination of carbon dioxide 169
Method of Shapiro and Brannock 169
Method using Schrotter s apparatus 170
Gravimetric method using absorption tubes and acid
decomposition 172
Gravimetric method using absorption tubes and
thermal decomposition 175
The determination of carbon dioxide by gas chroma-
tography 177
The titrimetric determination of carbon dioxide 178
Loss on ignition 178
The determination of carbon ( non-carbonate carbon ) 179
Gravimetric method using oxidation with chromic acid 180
Combustion tube methods 182
The determination of organic matter 182
Chapter 18. Chlorine, Bromine and Iodine 184
Occurrence 184
Water-soluble chlorine 185
A cid-soluble chlorine 185
Total chlorine 186
The photometric determination of chlorine 187
The determination of bromine 188
The determination of iodine 189
191
191
193
194
197
201
206
206
206
207
208
211
213
216
216
217
217
218
218
222
223
225
227
227
228
229
231
234
234
238
238
238
243
243
244
249
249
249
250
251
254
258
Chromium
Occurrence
The determination of chromium
Determination of chromium with EDTA
Determination of chromium as alkali Chromate
Determination of chromium using sym-diphenylcarbazide
Cobalt
Occurrence
The determination of cobalt
Photometric methods for the determination of cobalt
Determination of cobalt with nitroso-R-salt
Determination of cobalt with thiocyanate and
tri-n-butylamine
Ion-exchange separation and determination with CyDTA
Copper
Occurrence
The determination of copper
Photometric methods
Determination by atomic absorption spectroscopy
Determination of copper with 2, 2 -diqwnolyl
Extraction and determination of copper with dithizone
Extraction of copper, lead and zinc
Determination of copper with dithizone
Fluorine
Occurrence
The determination of fluorine
The lead chlorofluoride method
The photometric determination of fluorine
Photometric determination without distillation
Pyrohydrolytic determination of fluorine
Gallium
Occurrence
The determination of gallium
Germanium
Occurrence
The determination of germanium
Hydrogen
Occurrence
Free hydrogen
Organic hydrogen
Water evolved at 105°
Total water
Loss on ignition
Chapter 26.
Indium
Occurrence
260
260
Chapter 27. Iron 262
Occurrence 262
Metallic iron 263
Sulphate iron 265
Carbonate iron 265
Sulphide iron 266
Ferrous iron 267
The Pratt method 269
The Wilson method 270
Photometric determination offerrous iron 271
The determination of ferrous iron in carbonaceous shales 273
Ferric iron 274
Total iron 275
Photometric reagents for iron 276
Photometric determination of iron in silicate rocks 278
The titrimetric determination of total iron 281
Method based upon stannous chloride reduction 282
Methods based upon metallic reducing agents 284
The titration of ferric iron 286
Chapter 28. Lead 288
Occurrence 288
The determination of lead in silicate rocks 289
Separation procedures 289
Methods of determination 290
A solvent extraction—spectrophotometric method 291
A sublimation procedure 293
Chapter 29. Magnesium 296
Occurrence 296
Gravimetric determination in silicate rocks 297
Pyrophosphate method 297
8-Hydroxyquinoline method 297
Titrimetric determination in silicate rocks 299
Determination with 8-hydroxyquinoline 299
Determination with EDTA 299
The separation and determination of calcium and
magnesium 302
Photometric determination in silicate rocks 303
Determination of calcium and magnesium by atomic
absorption spectroscopy 308
Determination of magnesium in carbonate rocks 310
Chapter 30. Manganese 314
Occurrence 314
The determination of manganese in silicate rocks 315
Photometric determination 315
Determination with potassium periodate 318
Determination with ammonium persulphate 319
Photometric determination of manganese in carbonatite
rocks 320
The determination of manganese by atomic absorption
spectroscopy 321
Chapter 31. Mercury 323
Occurrence 323
The determination of mercury in silicate rocks 323
Chapter 32. Molybdenum and Tungsten 325
Occurrence 325
The determination of molybdenum and tungsten 326
Photometric methods 327
The determination of molybdenum and tungsten in
silicate rocks 330
Chapter 33. Nickel 334
Occurrence 334
The determination of nickel in silicate rocks 335
Gravimetric determination with dimethylglyoxime 336
Photometric determination following a preliminary
separation by chloroform extraction 338
Photometric determination after ion-exchange
separation 340
Chapter 34. Niobium and Tantalum 344
Occurrence 344
The determination of niobium 345
The determination of niobium in carbonatites with hydrogen
peroxide 345
The determination of niobium in silicate rocks with
thiocyanate 349
The determination of niobium with 4-(2-pyridylazo )-
resorcinol 353
The determination of tantalum 357
Chapter 35. Nitrogen 359
Occurrence 359
The determination of nitrogen 360
Chapter 36. Phosphorus 361
Occurrence 361
The determination of phosphorus 362
The determination of phosphorus using a vanadomolybdate
reagent 362
Acid-soluble phosphate in phosphate rock 363
Total phosphorus in silicate rocks 364
Determination of phosphorus in carbonate rocks 366
The determination of phosphorus as a molybdenum blue 367
Determination in silicate rocks 369
Chapter 37. Scandium, Yttrium and the Lanthanide Rare Earths 372
Occurrence 372
The determination of scandium in silicate rocks 373
The determination of yttrium 374
The determination of the lanthanide rare earths 375
Gravimetric determination in silicate rocks 375
Gravimetric determination in carbonatite rocks 379
Photometric determination of rare earths in silicate rocks 380
Chapter 38. Selenium and Tellurium 384
Occurrence 384
The determination of selenium 384
The determination of tellurium 388
Chapter 39. Silicon 389
Occurrence 389
The gravimetric determination of silica in quartzites and
sandstones 390
Gravimetric determination in silicate and carbonate rocks 392
Determination in carbonate rocks 393
Gravimetric determination without dehydration 393
A titrimetric method for silicate rocks 395
Photometric determination of silica 396
A combined gravimetric and photometric determination
of silica 400
Chapter 40. Silver, Gold and the Platinum Metals 403
Occurrence 403
The determination of silver, gold and the platinum
metals 406
Chapter 41. Strontium 408
Occurrence 408
The determination of strontium 409
Determination by flame photometry 410
Determination by atomic absorption spectroscopy 412
414
414
414
415
417
417
418
421
421
422
426
426
427
427
427
429
430
435
435
436
436
438
439
441
441
443
445
445
446
447
451
454
458
458
459
459
461
461
467
467
468
468
471
474
Sulphur
Occurrence
Free sulphur
Sulphide-sulphur
Water-soluble sulphur
Acid-soluble sulphur
Total sulphur
Thallium
Occurrence
The determination of thallium in silicate rocks
Thorium
Occurrence
The determination of thorium
Gravimetric determination
Photometric methods
Separation methods
The determination in silicate rocks
Tin
Occurrence
The determination of tin
Sample decomposition
Separation of tin
Photometric determination
The determination of tin in silicate rocks
Determination with catechol violet
Determination using salicylideneamino-2-thiophenol
Titanium
Occurrence
The determination of titanium in silicate rocks
Method using hydrogen peroxide
Method using diantipyrylmethane
Method using tiron
Uranium
Occurrence
The determination of uranium
Photometric methods
Separation of uranium
The determination in silicate rocks
Vanadium
Occurrence
The determination of vanadium in silicate rocks
Phosphotungstate method
Method using N-benzoyl-o-tolylhydroxylamine
Diaminobenzidine method
Chapter 49. Zinc 477
Occurrence 477
The determination of zinc in silicate rocks 478
Ion-exchange—zincon method 478
Determination of zinc by atomic absorption spectroscopy 482
Chapter 50. Zirconium and Hafnium 483
Occurrence 483
Gravimetric determination in silicate rocks 484
Phosphate method 484
Other gravimetric methods 486
Photometric methods for the determination of zirconium
and hafnium 486
The determination of hafnium 488
Index of Rock and Mineral Species 491
Author Index 495
Subject Index 505
Other titles in the series 509
|
| any_adam_object | 1 |
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| discipline | Chemie / Pharmazie |
| edition | 1. ed. |
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| oclc_num | 62484 |
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| owner | DE-355 DE-BY-UBR DE-20 DE-91 DE-BY-TUM DE-29 DE-188 |
| owner_facet | DE-355 DE-BY-UBR DE-20 DE-91 DE-BY-TUM DE-29 DE-188 |
| physical | XV, 509 S. Ill., graph. Darst. |
| publishDate | 1970 |
| publishDateSearch | 1970 |
| publishDateSort | 1970 |
| publisher | Pergamon Press |
| record_format | marc |
| series | International series of monographs on analytical chemistry |
| series2 | International series of monographs on analytical chemistry |
| spelling | Jeffery, Paul G. Verfasser aut Chemical methods of rock analysis by P. G. Jeffery 1. ed. Oxford [u.a.] Pergamon Press 1970 XV, 509 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier International series of monographs on analytical chemistry 36 Rocks Analysis Nachweis (DE-588)4115334-0 gnd rswk-swf Gestein (DE-588)4020734-1 gnd rswk-swf Chemisches Verfahren (DE-588)4454573-3 gnd rswk-swf Analytische Chemie (DE-588)4129906-1 gnd rswk-swf Geochemische Analyse (DE-588)4290341-5 gnd rswk-swf 1\p (DE-588)4144950-2 Bestimmungsbuch gnd-content Gestein (DE-588)4020734-1 s Geochemische Analyse (DE-588)4290341-5 s DE-604 Nachweis (DE-588)4115334-0 s Chemisches Verfahren (DE-588)4454573-3 s 2\p DE-604 Analytische Chemie (DE-588)4129906-1 s 3\p DE-604 International series of monographs on analytical chemistry 36 (DE-604)BV001889010 36 HBZ Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=004611938&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis 1\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk 2\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk 3\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk |
| spellingShingle | Jeffery, Paul G. Chemical methods of rock analysis International series of monographs on analytical chemistry Rocks Analysis Nachweis (DE-588)4115334-0 gnd Gestein (DE-588)4020734-1 gnd Chemisches Verfahren (DE-588)4454573-3 gnd Analytische Chemie (DE-588)4129906-1 gnd Geochemische Analyse (DE-588)4290341-5 gnd |
| subject_GND | (DE-588)4115334-0 (DE-588)4020734-1 (DE-588)4454573-3 (DE-588)4129906-1 (DE-588)4290341-5 (DE-588)4144950-2 |
| title | Chemical methods of rock analysis |
| title_auth | Chemical methods of rock analysis |
| title_exact_search | Chemical methods of rock analysis |
| title_full | Chemical methods of rock analysis by P. G. Jeffery |
| title_fullStr | Chemical methods of rock analysis by P. G. Jeffery |
| title_full_unstemmed | Chemical methods of rock analysis by P. G. Jeffery |
| title_short | Chemical methods of rock analysis |
| title_sort | chemical methods of rock analysis |
| topic | Rocks Analysis Nachweis (DE-588)4115334-0 gnd Gestein (DE-588)4020734-1 gnd Chemisches Verfahren (DE-588)4454573-3 gnd Analytische Chemie (DE-588)4129906-1 gnd Geochemische Analyse (DE-588)4290341-5 gnd |
| topic_facet | Rocks Analysis Nachweis Gestein Chemisches Verfahren Analytische Chemie Geochemische Analyse Bestimmungsbuch |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=004611938&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| volume_link | (DE-604)BV001889010 |
| work_keys_str_mv | AT jefferypaulg chemicalmethodsofrockanalysis |