X-ray scattering of synthetic polymers:
Saved in:
| Main Authors: | , |
|---|---|
| Format: | Book |
| Language: | English |
| Published: |
Amsterdam u.a.
Elsevier
1989
|
| Series: | Polymer science library
8 |
| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Physical Description: | XI, 317 S. Ill., graph. Darst. |
| ISBN: | 0444873856 |
Staff View
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Record in the Search Index
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| adam_text | POLYMER SCIENCE LIBRARY 8 X-RAY SCATTERING OF SYNTHETIC POLYMERS FJ.
BALTAE-CALLEJA INSTITUTO DE ESTRUCTURA DE LA MATERIA (CSIC), SERRANO 119,
E-28006 MADRID, SPAIN CG. VONK FORMERLY DSM CENTRAL LABORATORY, GELEEN,
THE NETHERLANDS ELSEVIER AMSTERDAM * OXFORD * NEW YORK * TOKYO 1989 VM
CONTENTS PREFACE V CHAPTER 1 THE THEORY OF COHERENT X-RAY SCATTERING
1.1. INTRODUCTION 1 1.2. THE SCATTERING FROM ONE ELECTRON 2 1.3. THE
SCATTERING FROM MANY ELECTRONS 3 1.4. FOURIER TRANSFORMATION AND
RECIPROCAL SPACE 6 1.5. THE EWALD SPHERE CONSTRUCTION 7 1.6. THE
CONVOLUTION OPERATION 8 1.7. THE FOURIER TRANSFORMS OF CONVOLUTIONS AND
PRODUCTS OF FUNCTIONS 12 1.8. GENERAL RELATIONS INVOLVING FOURIER
TRANSFORMS 14 1.9. DIFFRACTION BY CRYSTALS 16 1.10. POWDER PATTERNS 23
1.11. DIFFRACTION FROM NON-CRYSTALLINE SUBSTANCES 25 REF ERENCES 31
CHAPTER 2 EXPERIMENTAL TECHNIQUES 2.1. PROPERTIES OF X-RAY RADIATION 33
2.2. X-RAY EXCITATION 34 2.2.1. WHITE RADIATION 3 4 2.2.2.
CHARACTERISTIC RADIATION 35 2.2.3. SEALEDTUBES 37 2.2.4. ROTATING ANODE
TUBES 39 2.2.5. SYNCHROTRON RADIATION. 40 2.2.5.1. SYNCHROTRONS AND
STORAGE RINGS 41 2.2.5.2. INTENSITY, POLARIZATION, TIME STRUCTURE 42
2.2.5.3. ENERGY SPECTRUM 44 2.2.5.4. APPLICATIONS IN SYNTHETIC POLYMERS
46 2.3. ABSORPTION OF X-RAY RADIATION 47 2.3.1. ABSORPTION 47 2.3.2.
PHOTELECTRIC EFFECT 48 2.3.3. SCATTERING OF X-RAYS 48 2.3.4. ABSORPTION
EDGES 49 2.3.5. SINGLE AND BALANCED FILTERS 50 2.4. X-RAY DETECTION 51
2.4.1. PHOTOGRAPHIC FILMS 51 2.4.2. COUNTERS FOR X-RAY DETECTION 55
2.4.2.1. GAS COUNTERS 56 2.4.2.2. SCINTILLATION COUNTERS 57 2.4.2.3.
SOLID STATE DETECTORS 58 CONTENTS IX 2.4.2.4. PULSE HEIGHT
DISCRIMINATION 58 2.4.2.5. USE OF CRYSTAL MONOCHROMATORS 60 2.4.2.6.
POSITION SENSITIVE COUNTERS (PSC) 61 2.5. APPARATUS 66 2.5.1. WIDE-ANGLE
TECHNIQUES 66 2.5.1.1. CAMERAS 66 2.5.1.2. DIFFRACTOMETER 11 2.5.1.3.
ADVANCED TECHNIQUE FOR RAPID RECORDING OF X-RAY DIFFRACTOGRAMS 75
2.5.1.4. ENERGY DISPERSIVE DIFFRACTOMETER 76 2.5.2. SMALL-ANGLE
SCATTERING TECHNIQUES 78 2.5.2.1. PINHOLE COLLIMATION 78 2.5.2.2.
FOCUSING BY REFLECTION 82 2.5.2.3. SLIT COLLIMATION 82 REFERENCES 86
CHAPTER 3 LATTICE CONSTANTS 3.1. INTRODUCTION 89 3.2. MEASUREMENT OF
LATTICE CONSTANTS BY PHOTOGRAPHIE METHODS 89 3.2.1. DEBYE-SCHERRER
CAMERA 91 3.3. MEASUREMENT OF LATTICE CONSTANTS FROM DIFFRACTOMETER LINE
PROFILES 92 3.3.1. USE OF A FLAT SPEEIMEN 94 3.3.2. TRANSPARENCY ERROR
95 3.3.3. DIVERGENCE OF THE PRIMARY BEAM 96 3.3.4. SPEEIMEN DISPLACEMENT
97 3.3.5. CALIBRATION 98 3.4. UNIT CELL MEASUREMENTS IN POLYMERS 99
3.4.1. VARIATIONS WITH TEMPERATURE (THERMAL EXPANSION) 99 3.4.2. EFFECT
OF CRYSTALLIZATION TEMPERATURE 103 3.4.3. EFFECT OF LATERAL CHAIN
DEFECTS 106 3.4.4. EFFECT OF DRAWING 114 3.4.5. EFFECT OF HIGH PRESSURE
118 3.5. INTERPRETATION OF UNIT CELL VARIATIONS 119 3.5.1. THE
INCORPORATION OF CHAIN DEFECTS IN POLYMER CRYSTALS 121 3.5.2. EFFECT OF
LAMELLAR THICKNESS ON LATTICE CONSTANTS 124 REFERENCES 127 CHAPTER 4
LINE BREADTH MEASUREMENTS: PARACRYSTALLINITY 4.1. INTRODUCTION 129 4.2.
LATTICE DISTORTIONS 130 4.3. DISTORTIONS OF THE FIRST KIND 132 4.4. THE
CONEEPT OF PARACRYSTAL: DISTORTIONS OF THE SECOND KIND 134 4.4.1. THE
PARACRYSTALLINE LATTICE FACTOR 138 4.4.2. INTEGRAL BREADTH 139 4.4.3.
INTENSITY FUNETION 140 X CONTENTS 4.5. LINE BROADENING ANALYSIS 141
4.5.1. CRYSTALLITE SIZE 143 4.5.2. LATTICE DISORDER 143 4.5.3.
SEPARATION OF CRYSTAL SIZE AND LATTICE DISORDER BROADENING 145 4.5.4.
APPLICATIONS TO SYNTHETIC POLYMERS 148 4.5.4.1. 8/3-VERSUS-H PLOTS 148
4.5.4.2. SHAPE ELLIPSOID 151 4.6. A*-RELATION: NATURAL PARACRYSTALS 155
4.6.1. BEARING LATTICE PLANES 158 4.6.2. ORIGIN OF DISTORTIONS OF THE
2ND KIND IN POLYMERS 158 4.7. FOURIER TRANSFORM METHODS 161 4.7.1. THE
WARREN-AVERBACH METHOD 161 4.7.2. ALTERNATIVE FOURIER TECHNIQUES 162
4.7.3. TRUNCATION EFFECT 164 4.7.4. EXAMPLES 165 4.8. INSTRUMENTAL
CORRECTIONS 169 4.8.1. FOURIER METHOD 169 4.8.2. REFERENCE METHODS 170
REFERENCES 172 CHAPTER 5 THE X-RAY DETERMINATION OF THE CRYSTALLINITY IN
POLYMERS 5.1. INTRODUCTION 175 5.2. METHODS BASED ON EXTERNAL COMPARISON
176 5.2.1. THE METHOD OF GOPPEL AND ARLMAN 176 5.2.2. THE METHOD OF
WAKELIN, VIRGIN AND CRYSTAL 177 5.2.3 THE METHOD OF HERMANS AND
WEIDINGER 179 5.2.4. THE METHOD OF HENDUS AND SCHNELL 180 5.3. METHODS
BASED ON INTERNAL COMPARISON 182 5.3.1. THEORETICAL 182 5.3.2. SOME
OLDER METHODS 183 5.3.3. RULAND S METHOD 184 5.3.3.1. PRINCIPLES 184
5.3.3.2 COMPUTERIZATION 187 5.3.3.3. PRACTICALASPECTS 192 5.3.3.4.
ANISOTROPIE SAMPLES 195 5.3.3.5. INCONGRUENT PHASES 198 5.3.3.6. GENERAL
CONSIDERATIONS 201 REFERENCES 203 CHAPTER 6 THE X-RAY DETERMINATION OF
THE ORIENTATION IN POLYMERS 6.1. INTRODUCTION 205 6.2. CLASSIFICATION
206 6.3. THE X-RAY REGISTRATION OF THE ORIENTATION OF CRYSTALLITES 207
6.4. POLEFIGURES 211 6.5. SPECIFICATION OF ORIENTATION 213 6.5J. TYPES
OF ORIENTATION 214 CONTENTS . M 6.5.2. THE DEGREE OF ORIENTATION 215
6.5.2.1. UNIAXIAL ORIENTATION 218 6.5.2.2. BIAXIAL ORIENTATION 223
6.5.2.3. APPLICATION TO BLOWN FILMS OF POLYETHYLENE 226 6.6. THE
INTERPRETATION OF ORIENTATION PHENOMENA 228 6.6.1. THE PSEUDO-AFFINE
TRANSFORMATION APPROXIMATION 228 6.6.2. STUDIES ON THE DEFORMATION OF
POLYETHYLENE 229 6.6.2.1. TWINNING 230 6.6.2.2. SLIP 233 6.6.3. ROW
ORIENTATION 236 REFERENCES 239 CHAPTER 7 THE SMALL-ANGLE X-RAY
SCATTERING OF POLYMERS 7.1. INTRODUCTION 241 7.2. PRIMARY DATA TREATMENT
242 7.2.1. RAW DATA CORRECTION 242 7.2.2. BACKGROUND SUBTRACTION 242
7.2.3. DESMEARING 244 7.2.4. CALCULATION OF THE CORRELATION FUNCTION 247
7.2.5. CALCULATION OF ABSOLUTE INTENSITIES 251 7.2.6. CALCULATION OF THE
INVARIANT 254 7.3. TWO-PHASE STRUCTURES 255 7.3.1. GENERAL 255 7.3.2.
DETERMINATION OF THE SPECIFIC SURFACE 257 7.3.3. DETERMINATION OF THE
WIDTH OF THE PHASE BOUNDARY 261 7.4. PARTICLE SCATTERING 266 7.5.
LAMELLAR SYSTEMS 270 7.5.1. THE IDEAL LAMELLAR MODEL: SIMPLE ANALYSIS
271 7.5.2. THE DIRECT METHOD 273 7.5.2.1. PROPERTIES OF THE INTENSITY
FUNCTION AT THE LOWEST ANGLES 278 7.5.2.2. VARIATIONS IN LAMELLAR
THICKNESS 280 7.5.2.3. FURTHER IMPROVEMENTS OF THE MODEL 281 7.5.3. THE
CORRELATION FUNCTION APPROACH 282 7.5.4. DEVIATIONS FROM THE IDEAL
LAMELLAR MODEL 288 7.6. THE SMALL-ANGLE SCATTERING OF ORIENTED POLYMERS
294 7.6.1. REGISTRATION OF TWO-DIMENSIONAL X-RAY PATTERNS 294 7.6.2.
GENERAL DESCRIPTION OF SAXS FIBRE PATTERNS 296 7.6.3. INTERPRETATION OF
FIBRE PATTERNS IN TERMS OF MODEIS 298 7.6.3.1. MODELS BASED ON
CONTINUOUS LAMELLAR STRUCTURES 299 7.6.3.2. MODELS BASED ON MICROFIBRILS
300 REFERENCES 304 AUTHOR INDEX 307 SUBJECT INDEX 312
|
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| id | DE-604.BV005550483 |
| illustrated | Illustrated |
| indexdate | 2024-07-09T16:31:30Z |
| institution | BVB |
| isbn | 0444873856 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-003480568 |
| oclc_num | 19457975 |
| open_access_boolean | |
| owner | DE-92 DE-703 DE-83 DE-11 DE-188 |
| owner_facet | DE-92 DE-703 DE-83 DE-11 DE-188 |
| physical | XI, 317 S. Ill., graph. Darst. |
| psigel | TUB-nveb |
| publishDate | 1989 |
| publishDateSearch | 1989 |
| publishDateSort | 1989 |
| publisher | Elsevier |
| record_format | marc |
| series | Polymer science library |
| series2 | Polymer science library |
| spelling | Baltá Calleja, Francisco J. 1936- Verfasser (DE-588)171964616 aut X-ray scattering of synthetic polymers F. J. Baltá-Calleja ; C. G. Vonk Amsterdam u.a. Elsevier 1989 XI, 317 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Polymer science library 8 Polymères - Analyse Radiocristallographie Rayons X - Diffraction Polymers Analysis X-ray crystallography X-rays Diffraction Röntgenstrukturanalyse (DE-588)4137203-7 gnd rswk-swf Röntgenstreuung (DE-588)4178324-4 gnd rswk-swf Polymere (DE-588)4046699-1 gnd rswk-swf Röntgenstrukturanalyse (DE-588)4137203-7 s Polymere (DE-588)4046699-1 s DE-604 Röntgenstreuung (DE-588)4178324-4 s Vonk, C. G. Verfasser (DE-588)127213856 aut Polymer science library 8 (DE-604)BV000899569 8 GBV Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=003480568&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Baltá Calleja, Francisco J. 1936- Vonk, C. G. X-ray scattering of synthetic polymers Polymer science library Polymères - Analyse Radiocristallographie Rayons X - Diffraction Polymers Analysis X-ray crystallography X-rays Diffraction Röntgenstrukturanalyse (DE-588)4137203-7 gnd Röntgenstreuung (DE-588)4178324-4 gnd Polymere (DE-588)4046699-1 gnd |
| subject_GND | (DE-588)4137203-7 (DE-588)4178324-4 (DE-588)4046699-1 |
| title | X-ray scattering of synthetic polymers |
| title_auth | X-ray scattering of synthetic polymers |
| title_exact_search | X-ray scattering of synthetic polymers |
| title_full | X-ray scattering of synthetic polymers F. J. Baltá-Calleja ; C. G. Vonk |
| title_fullStr | X-ray scattering of synthetic polymers F. J. Baltá-Calleja ; C. G. Vonk |
| title_full_unstemmed | X-ray scattering of synthetic polymers F. J. Baltá-Calleja ; C. G. Vonk |
| title_short | X-ray scattering of synthetic polymers |
| title_sort | x ray scattering of synthetic polymers |
| topic | Polymères - Analyse Radiocristallographie Rayons X - Diffraction Polymers Analysis X-ray crystallography X-rays Diffraction Röntgenstrukturanalyse (DE-588)4137203-7 gnd Röntgenstreuung (DE-588)4178324-4 gnd Polymere (DE-588)4046699-1 gnd |
| topic_facet | Polymères - Analyse Radiocristallographie Rayons X - Diffraction Polymers Analysis X-ray crystallography X-rays Diffraction Röntgenstrukturanalyse Röntgenstreuung Polymere |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=003480568&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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