Holdings: Fundamentals of analytical chemistry

Fundamentals of analytical chemistry:

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Bibliographic Details
Main Authors:	Skoog, Douglas A. 1918-2008 (Author), West, Donald M. (Author)
Format:	Book
Language:	English
Published:	Fort Worth u.a. Saunders 1988
Edition:	5. ed.
Series:	Saunders golden sunburst series
Subjects:	Chemistry, Analytic Analytische Chemie Lehrbuch
Online Access:	Inhaltsverzeichnis
Physical Description:	XVI, 894 S.
ISBN:	0030148286

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MARC


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adam_text	FUNDAMENTALSOF Analytical Chemistry FIFTHEDITION DOUGLASASKOOG Stanford University DONALDMWEST San Jose State University FJAMESHOLLER University of Kentucky H Saunders Golden Sunburst Series Saunders College Publishing New York Chicago San Francisco Philadelphia Montreal Toronto London Sydney Tokyo Contents Overview Introduction i Evaluation of Analytical Data 6 Gravimetric Methods of Analysis 57 Titrimetric Methods of Analysis 84 A Review of Aqueous-Solution Chemistry 103 The Application of Equilibrium Calculations to Complex Systems 135 Precipitation Titrations 164 Titration Curves for Simple Acid/Base Systems 182 Titration Curves for Complex Acid/Base Systems 211 Applications of Neutralization Titrations 233 Complex-Formation Titrations 257 An Introduction to Oxidation!Reduction Equilibria and Electrochemical Theory 282 Theory of Oxidation/Reduction Titrations 315 Applications of Oxidation!Reduction Titrations 331 Potentiometric Methods 357 Electrogravimetric and Coulometric Methods 393 Voltammetry and Polarography 424 An Introduction to Spectroscopic Methods of Analysis 457 Instruments for Optical Spectroscopy 481 Molecular Spectroscopy 505 Atomic Spectroscopy Based on Ultraviolet and Visible Radiation 554 Kinetic Methods of Analysis 578 An Introduction to Chromatographic Methods 598 Gas-Liquid Chromatography 626 High-Performance Liquid Chromatography 644 The Analysis of Real Samples 667 Preparing Samples for Analysis 678 Decomposing and Dissolving the Sample 692 Eliminating Interferences 702 Chemicals, Apparatus, and Unit Operations of Analytical Chemistry 719 Selected Methods of Analysis 757 ix X/l CONTENTS 7 Precipitation Titrations 164 7A Titration Curves in Titrimetric Methods 164 7B Titration Curves for Precipitation Reactions 165 7C Applications of Precipitation Titrations 177 8 Titration Curves for Simple Acid/Base Systems 182 8A Solutions and Indicators for Neutralization Titrations 182 8B Titration Curves for Strong Acids and Strong Bases 185 8C Properties of Weak Acid and Weak Base Systems 188 8D Properties of Buffer Solutions 193 8E Titration Curves for Weak Acids 197 8F Titration Curves for Weak Bases 202 8G Common Types of Acid/Base Indicators 204 9 Titration Curves for Complex Acid/Base Systems 2 1 1 9A Mixtures of Strong and Weak Acids or Strong and Weak Bases 211 9B Equilibrium Calculations for Compounds with Multiple Acidic or Basic Functional Groups 214 9C Titration Curves for Polyprotic Acids and Their Conjugate Bases 221 9D The Composition of a Solution of a Polyprotic Acid as a Function of pH 227 10 Applications of Neutralization Titrations 233 1QA Reagents for Neutralization Reactions 233 JOB Typical Applications of Neutralization Titrations 238 IOC Application of Neutralization Titrations in Nonaqueous Media 245 11 Complex-Formation Titrations 257 11A Complex-Formation Reactions 257 11B Titrations with Aminopolycarboxylic Acids 259 11C Titrations with Inorganic Complexing Agents 277 12 An Introduction to Oxidation/Reduction Equilibria and Electrochemical Theory 282 12A Oxidation/Reduction Processes 282 12B Electrochemical Cells 284 12C Electrode Potentials 288 12D Applications of Electrode Potentials 299 13 Theory of Oxidation/Reduction Titrations 315 13A Electrode Potentials for Redox Titration Systems 315 13B Oxidation/Reduction Indicators 325 13C Potentiometric End Points 329 14 Applications of Oxidation/Reduction Titrations 331 14A Auxiliary Oxidizing and Reducing Reagents 331 14B Applications of Standard Oxidants 334 14C Volumetric Applications of Reductants 341 14D Some Specialized Oxidants 344 CONTENTS xiii 15 Potentiometric Methods 357 15A Reference Electrodes 357 15B Indicator Electrodes 359 15C Instruments for the Measurement of Cell Potentials 374 15D Direct Potentiometric Measurements 376 15E Potentiometric Titrations 384 16 Electrogravimetric and Couiometric Methods 393 16A The Effect of Current on Cell Potentials 393 16B The Potential Selectivity of Electrolytic Methods 398 16C Electrogravimetric Methods of Analysis 399 16D Couiometric Methods of Analysis 407 17 Voitammetry and Polarography 424 17A Polarographic Measurements 424 17B Polarographic Currents 428 17C Half-Wave Potentials 431 17D Instrumentation 435 17E Applications of Polarography 438 17F Modified Voltammetric Methods 442 18 An Introduction to Spectroscopic Methods of Analysis 457 18A Properties of Electromagnetic Radiation 457 18B The Electromagnetic Spectrum 460 18C Absorption of Radiation 460 18D Emission of Electromagnetic Radiation 473 19 Instruments for Optical Spectroscopy 48i 19A Instrument Components 481 19B Spectroscopic Instruments 498 20~ Molecular Spectroscopy 505 20A Ultraviolet and Visible Absorption Spectroscopy 505 20B Infrared Absorption Spectroscopy 528 20C Molecular Fluorescence Methods 534 20D Automation of Photometric and Spectrophotometry Methods 538 21 Atomic Spectroscopy Based on Ultraviolet and Visible Radiation 554 21A A Comparison of Atomic and Molecular Spectroscopic Methods 554 21B Atomic Spectroscopy Based on Flame Atomization 555 21C Atomic Absorption Methods with Electrothermal Atomizers 570 21D Atomic Emission Methods Based on Atomization in Plasmas 571 22 Kinetic Methods of Analysis 578 22A Rates of Chemical Reactions; Rate Laws 578 22B The Determination of Reaction Rates 588 22C Applications of Kinetic Methods 593 xiv CONTENTS 23 An Introduction to Chromatographic Methods 598 23A A General Description of Chromatography 598 23B Migration Rates of Solutes 602 23C Band Shapes and Band Broadening 605 23D Optimization of Column Performance 614 23E A Summary of Important Relationships for Chromatography 620 23F Applications of Chromatography 620 24 Gas-Liquid Chromatography 626 24A Principles of Gas-Liquid Chromatography 627 24B Instruments for Gas-Liquid Chromatography 627 24C Liquid Phases for Gas-Liquid Chromatography 637 24D Applications of Gas-Liquid Chromatography 638 24E Typical Applications of Gas Chromatography 639 25 High-Performance Liquid Chromatography 644 25A Instruments for High-Performance Liquid Chromatography 645 25B High-Performance Partition Chromatography 648 25C High-Performance Adsorption Chromatography 650 25D High-Performance Ion-Exchange Chromatography 652 25E High-Performance Size-Exclusion Chromatography 655 25F A Comparison of High-Performance Liquid Chromatography and Gas-Liquid Chromatography 657 25G Supercritical-Fluid Chromatography 658 25H Planar Chromatography 662 26 The Analysis of Real Samples 667 26A Choice of Method for the Analysis of Real Samples 669 26B The Accuracy Obtainable in the Analysis of Complex Materials 674 27 Preparing Samples for Analysis 678 27A Sampling 678 27B Moisture in Samples 685 27C Determination of Water in Samples 689 28 Decomposing and Dissolving the Sample 692 28A Some General Considerations 692 28B Aqueous Reagents for Dissolving or Decomposing Samples 693 28C Decomposition of Samples by Fluxes 694 28D Decomposition of Organic Compounds for Elemental Analysis 697 29 Eliminating Interferences 702 29A The Nature of the Separation Process 702 29B Separation by Precipitation 703 29C Extraction Methods 706 29D Applications of Extraction Procedures 710 29E Ion-Exchange Separations 715 29F The Separation of Inorganic Species by Distillation 716 CONTENTS XV 30 The Chemicals, Apparatus, and Unit Operations ofAnalyticalChemistry7i9 30A The Selection and Handling of Reagents and Other Chemicals 719 30B The Cleaning and Marking of Laboratory Ware 721 30C The Evaporation of Liquids 721 30D The Measurement of Mass 722 30E The Equipment and Manipulations Associated with Weighing 731 30F Weight Titrations 734 30G The Equipment and Manipulations for Filtration and Ignition 735 30H The Measurement of Volume 742 301 The Calibration of Volumetric Ware 750 30J The Laboratory Notebook 753 30K Safety in the Laboratory 754 31 Selected Methods of Analysis 757 31A Gravimetric Methods of Analysis 758 31B Precipitation Titrations 762 31C Neutralization Titrations 765 31D Complex-Formation Titrations with EDTA 771 31E Oxidation/Reduction Titrations with Potassium Permanganate 773 31F lodimetric Titrations 779 31G lodometric Methods of Analysis 781 31H Titrations with Potassium Bromate 784 311 Potentiometric Methods 786 31J Electrogravimetric Methods 791 31K Couiometric Titrations 792 31L Voltammetry 794 31M Methods Based on the Absorption of Radiation 796 31N Molecular Fluorescence 800 310 Atomic Spectroscopy 801 31P Separation of Cations by Ion Exchange 803 31Q Gas-Liquid Chromatography 805 Appendix 1 Selected References to the Literature of Analytical Chemistry 807 Appendix 2 Some Standard and Formal Electrode Potentials 81 / Appendix 3 Solubility-Product Constants 815 Appendix 4 Dissociation Constants for Acids 817 Appendix 5 Dissociation Constants for Bases 818 Appendix 6 Stepwise Formation Constants 819 Appendix 7 Designations and Porosities for Filtering Crucibles 821 Appendix 8 Designations Carried by Ashless Filter Papers 822 XVI CONTENTS Appendix 9 Volumetric Calculations Using Normality and Equivalent Weight 823 Appendix 10 The Potentiometer 831 Appendix 11 The Method of Successive Approximations 833 Appendix 12 Compounds Recommended for the Preparation of Standard Solutions of Some Common Elements 835 Answers to Questions and Problems 837 Index 873
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author	Skoog, Douglas A. 1918-2008 West, Donald M.
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title	Fundamentals of analytical chemistry
title_auth	Fundamentals of analytical chemistry
title_exact_search	Fundamentals of analytical chemistry
title_full	Fundamentals of analytical chemistry Douglas A. Skoog ; Donald M. West*
title_fullStr	Fundamentals of analytical chemistry Douglas A. Skoog ; Donald M. West*
title_full_unstemmed	Fundamentals of analytical chemistry Douglas A. Skoog ; Donald M. West*
title_short	Fundamentals of analytical chemistry
title_sort	fundamentals of analytical chemistry
topic	Chemistry, Analytic Analytische Chemie (DE-588)4129906-1 gnd
topic_facet	Chemistry, Analytic Analytische Chemie Lehrbuch
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