Principles of adsorption chromatography: the separation of nonionic organic compounds
Saved in:
| Main Author: | |
|---|---|
| Format: | Book |
| Language: | English |
| Published: |
New York
Dekker
1968
|
| Series: | Chromatographic science
3 |
| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Physical Description: | XVI, 413 S. graph. Darst. |
Staff View
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Record in the Search Index
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|---|---|
| adam_text | CONTENTS
Foreword vii
Preface ix
chapter 1 Introduction 1
1-1. Intended Coverage 1
1-2. Historical Perspective 3
1-3. A Comment on the Following Pages 6
References 7
chapter 2 The Chromatographic Process and Techniques
of Separation 9
2-1. Sample Migration in the Adsorbent Bed 10
2-2. Elution from the Bed 16
2-3. Resolution and Separation. The General Elution Problem 17
2-4. Nonlinear Isotherm Separations. Variations in K with Sample
Concentration 22
2-5. Chromatographic Techniques 24
Symbols Used in Chapter 2 36
References 37
chapter 3 General Aspects of Adsorption 39
3-1. Fundamental Contributions to Adsorption 42
3-2. Adsorption Isotherm 52
3-3. Adsorption of Polyatomic Molecules and Spatial Arrangement of
Surface Sites 60
3-4. Useful Physical Concepts in the Adsorption of Organic Molecules 63
Symbols Used in Chapter 3 70
References 71
xiv CONTENTS
chapter 4 The Importance of Sample Size in Adsorption
Chromatography. Isotherm Linearity 75
4-1. Linear Isotherms in Adsorption Chromatography 77
4-2. Dependence of Linear Capacity on Relative Sample Adsorption 83
4-3. Dependence of Linear Capacity on Other Separation Variables 87
4-4. //-Type Isotherms and Chemisorption 92
4-5. Preparative Scale Separations 94
Symbols Used in Chapter 4 95
References 96
chapter 5 Bed Efficiency. Bandwidth versus Separation
Conditions 99
5-1. Genera Theory 100
5-2. Bed Efficiency in Liquid Column Chromatography 111
5-3. Bed Efficiency in Thin-Layer Chromatography 118
Symbols Used in Chapter 5 122
References 123
chapter 6 The General Role of Adsorbent Type
and Activity 125
6-1. Significant Adsorbent Properties 127
6-2. Dependence of Sample Adsorption on Adsorbent Activity 130
6-3. Adsorbent Standardization 143
Symbols Used in Chapter 6 152
References 153
chapter 7 Individual Adsorbents 155
7-1. Silica 156
7-2. Alumina 163
7-3. Other General Purpose Adsorbents 168
7-4. Group-Selective Adsorbents 172
7-5. Specific Adsorbents 177
References 181
chapter 8 The Role of the Solvent 185
8-1. Primary Effect of the Solvent on Sample Adsorption. Pure Solvents 186
8-2. Solvent Mixtures 205
CONTENTS XV
8-3. Secondary Solvent Effects 216
8-4. Predicting Solvent Strength 229
8-5.- Other Aspects of the Solvent 234
Symbols Used in Chapter 8 237
References 239
chapter 9 Gas-Solid Chromatography 241
9-1. Theory 241
9-2. Practical Aspects 249
Symbols Used in Chapter 9 253
References 254
chapter 10 The Role of Sample Structure. Primary Effects 257
10-1. Contribution of Group Adsorption Energies to Sample Adsorption.
The Martin Relationship 258
10-2. Localized Adsorption of the Sample 266
10-3. Predicting Group Adsorption Energies 282
10-4. Configuration of Adsorbed Sample Molecules 288
Symbols Used in Chapter 10 291
References 292
chapter 11 The Role of Sample Structure. Secondary
Effects 295
11-1. Variations in Group Adsorption Energy with Sample Structure 296
11-2. Contributions of Overall Sample Structure to K 320
Symbols Used in Chapter 11 331
References 333
chapter 12 Separation Temperature as a Variable 335
12-1. Sample Adsorption versus Temperature 335
12-2. Practical Importance of Temperature Effects 340
Symbols Used in Chapter 12 342
References 343
chapter 13 Some Related Topics 345
13-1. Equipment 346
13-2. Some Special Techniques 350
13-3. Problems 357
References 362
xvi CONTENTS
appendix i Calculation of R M Values from Experimental
RF Values 365
References 369
appendix ii Characterization of Silica Samples by
Silanization 371
References 374
appendix in A Rapid Procedure for Estimating the Solvent
Strengths of a Series of Binary Mixtures.
Tabulated e° Values for Several Binary
Solvent Systems 375
appendix iv Differing Adsorption Mechanisms on Alumina
and Silica 381
References 383
appendix v Examples of the Calculation of K° Values in
Adsorption Chromatography 385
References 396
Author Index 397
Subject Index 407
|
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| discipline | Chemie / Pharmazie |
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| illustrated | Illustrated |
| indexdate | 2024-07-09T15:43:13Z |
| institution | BVB |
| language | English |
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| physical | XVI, 413 S. graph. Darst. |
| publishDate | 1968 |
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| publisher | Dekker |
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| series2 | Chromatographic science |
| spelling | Snyder, Lloyd R. Verfasser aut Principles of adsorption chromatography the separation of nonionic organic compounds Lloyd R. Snyder New York Dekker 1968 XVI, 413 S. graph. Darst. txt rdacontent n rdamedia nc rdacarrier Chromatographic science 3 Adsorptie gtt Adsorption Chromatografie gtt Chromatographie Organische verbindingen gtt Chemistry, Organic Chromatographic analysis Chromatography, Thin Layer Adsorptionschromatographie (DE-588)4068422-2 gnd rswk-swf Adsorption (DE-588)4000536-7 gnd rswk-swf Chromatographie (DE-588)4010153-8 gnd rswk-swf Adsorptionschromatographie (DE-588)4068422-2 s DE-604 Adsorption (DE-588)4000536-7 s Chromatographie (DE-588)4010153-8 s Chromatographic science 3 (DE-604)BV000003251 3 HBZ Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=001495375&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Snyder, Lloyd R. Principles of adsorption chromatography the separation of nonionic organic compounds Chromatographic science Adsorptie gtt Adsorption Chromatografie gtt Chromatographie Organische verbindingen gtt Chemistry, Organic Chromatographic analysis Chromatography, Thin Layer Adsorptionschromatographie (DE-588)4068422-2 gnd Adsorption (DE-588)4000536-7 gnd Chromatographie (DE-588)4010153-8 gnd |
| subject_GND | (DE-588)4068422-2 (DE-588)4000536-7 (DE-588)4010153-8 |
| title | Principles of adsorption chromatography the separation of nonionic organic compounds |
| title_auth | Principles of adsorption chromatography the separation of nonionic organic compounds |
| title_exact_search | Principles of adsorption chromatography the separation of nonionic organic compounds |
| title_full | Principles of adsorption chromatography the separation of nonionic organic compounds Lloyd R. Snyder |
| title_fullStr | Principles of adsorption chromatography the separation of nonionic organic compounds Lloyd R. Snyder |
| title_full_unstemmed | Principles of adsorption chromatography the separation of nonionic organic compounds Lloyd R. Snyder |
| title_short | Principles of adsorption chromatography |
| title_sort | principles of adsorption chromatography the separation of nonionic organic compounds |
| title_sub | the separation of nonionic organic compounds |
| topic | Adsorptie gtt Adsorption Chromatografie gtt Chromatographie Organische verbindingen gtt Chemistry, Organic Chromatographic analysis Chromatography, Thin Layer Adsorptionschromatographie (DE-588)4068422-2 gnd Adsorption (DE-588)4000536-7 gnd Chromatographie (DE-588)4010153-8 gnd |
| topic_facet | Adsorptie Adsorption Chromatografie Chromatographie Organische verbindingen Chemistry, Organic Chromatographic analysis Chromatography, Thin Layer Adsorptionschromatographie |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=001495375&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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