Chemical methods of rock analysis:
Saved in:
| Main Author: | |
|---|---|
| Format: | Book |
| Language: | English |
| Published: |
Oxford (u.a.)
Pergamon Pr.
1975
|
| Edition: | 2. ed. |
| Series: | International series of monographs on analytical chemistry.
36 |
| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Physical Description: | XIX, 525 S. Ill., graph. Darst. 22 cm |
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| adam_text | Titel: Chemical methods of rock analysis
Autor: Jeffery, Paul G
Jahr: 1975
CONTENTS
Preface to the Second Edition
xvii
Acknowledgements xix
Chapter 1. The Composition of Rock Material 1
Introduction 1
International standards 4
Elements determined 6
Reporting an analysis 10
Chapter 2. Sample Preparation 13
Selection of material 13
Crushing and grinding 15
Contamination 16
Fine grinding of micas 19
Sample material for trace-element determinations 19
Chapter 3. Sample Decomposition 20
Extraction procedures 21
Extraction with water 21
Extraction with organic solvents 21
Decomposition with mineral acids 21
Decomposition with hydrochloric acid 21
Decomposition with nitric acid 22
Decomposition with hydrofluoric acid 22
Fusion procedures 24
Fusion with alkali fluoride 24
Fusion with potassium pyrosulphate 24
Fusion with sodium carbonate 25
Fusion with alkali hydroxide 27
Sinter or fusion with sodium peroxide 29
Fusion with boric oxide and alkali borates 30
Miscellaneous decomposition procedures 32
Fire assay for gold and silver 32
Miscellaneous fluxes 32
Chapter 4. Classical Scheme for the Analysis of Silicate Rocks 34
Introduction 34
Decomposition of the sample 35
V
The determination of silica
Separation and collection of silica
Ignition and volatilisation of silica
The determination of mixed oxides
Precipitation of the mixed oxides
Recovery of the aluminium traces
Ignition of the mixed oxides
Recovery of silica traces
Determination of aluminium by difference
The determination of calcium
The determination of magnesium
Determination of manganese in the magnesium residue
Chapter 5. The Rapid Analysis of Silicate Rocks
Introduction
Individual schemes of rapid rock analysis
Schemes of Shapiro and Brannock
Scheme of Riley
Scheme of Langmyhr and Graff
Scheme of Ingamells
Schemes based upon atomic absorption spectroscopy
Scheme of Belt
Scheme of Bernas
Scheme of Langmyhr and Paus
Schemes of Abbey
Chapter 6. Some Statistical Considerations
Classification of errors
Precision and accuracy
Confidence limits
The significance of results
The X* test
Chapter 7. The Alkali Metals
Occurrence
Determination in silicate rocks and minerals
Gravimetric methods
Flame photometry
Atomic absorption spectroscopy
Chromatographic separation of the alkali metals
Determination of sodium and potassium in silicate rocks
Small amounts of alkali metals in ultrabasic rocks
The determination of potassium in micas
The determination of lithium
Determination of lithium by atomic absorption
spectroscopy
The determination of rubidium and caesium
37
37
38
40
40
41
42
42
43
43
44
46
48
48
54
54
54
56
56
58
58
58
59
59
62
62
63
68
69
72
75
75
76
76
77
79
81
82
86
86
88
89
89
Chapter 8. Aluminium 94
Occurrence 94
The determination of aluminium in silicate rocks 94
Gravimetric methods 94
Titrimetric determination 96
Photometric determination 97
Atomic absorption spectroscopy 99
The separation of aluminium 99
Extraction procedures 99
Precipitation with sodium hydroxide 101
Ion-exchange separation 101
Electrolysis with a mercury cathode 101
The gravimetric determination with 8-hydroxyquinoline 101
The titrimetric determination with CyDTA 103
The photometric determination with 8-hydroxyquinoline 105
The photometric determination with pyrocatechol violet 106
Chapter 9. Antimony 109
Occurrence 109
The determination of antimony in silicate rocks 109
Photometric determination 110
Polarographic determination 112
Chapter 10. Arsenic 115
Occurrence 115
The determination of arsenic in silicate rocks 116
The separation of arsenic 116
Photometric determination 117
A molybdenum blue method using acid digestion 118
A molybdenum blue method using a fusion 121
An arsine-molybdenum blue method 122
Method using silver diethyldithiocarbamate 125
Method using co-crystallisation with thionalide 125
Chapter 11. Barium 130
Occurrence 130
The determination of barium in silicate rocks 131
Gravimetric method 131
Determination by flame photometry 134
Determination by atomic absorption spectroscopy 135
Chapter 12. Beryllium 137
Occurrence 137
Warning 138
The determination of beryllium 138
Gravimetric determination as phosphate 139
Photometric determination with berylion II 141
Precipitation as phosphate with titanium as collector 144
Fluorimetrie determination of beryllium with morin 145
The determination of beryllium by atomic absorption
spectroscopy 149
Chapter 13. Bismuth 151
Chapter 14. Boron 153
Occurrence 153
The determination of boron 154
The separation of boron 154
The determination of boron in tourmaline 155
The determination of boron in silicate rocks 156
Chapter 15. Cadmium 160 j
Occurrence 160 |
The determination in silicate rocks 160
Chapter 16. Calcium 163
Occurrence 163
The determination of calcium as oxalate 163
Classical gravimetric procedure 163 •
Direct gravimetric determination 164
The separation of strontium 166
Titrimetric determination with permanganate 166
Titrimetric determination with EDTA 167
The determination of calcium in carbonate rocks 168
Photometric determination of calcium in silicate rocks 169
The determination of calcium by flame photometry 170
The determination of calcium by atomic absorption
spectroscopy 171
Chapter 17. Carbon 172
Occurrence 172
Carbon dioxide 172
The determination of carbon dioxide 174
Method of Shapiro and Brannock 174
Method using Schrotter s apparatus 175
Gravimetric method using absorption tubes and acid
decomposition 177
Gravimetric method using absorption tubes and
thermal decomposition 180
The determination of carbon dioxide by non-aqueous i
titration 182
The determination of carbon dioxide by gas chroma-
tography 183
Loss on ignition 183
The determination of carbon ( non-carbonate carbon ) 184
Gravimetric method using oxidation with chromic acid 185
Combustion tube methods 187
The determination of organic matter 188
Chapter 18. Chlorine, Bromine and Iodine 190
Occurrence 190
Water-soluble chlorine 191
Acid-soluble chlorine 191
Total chlorine 192
The photometric determination of chlorine 193
The determination of chlorine using an ion-selective
electrode 194
The determination of bromine 195
The determination of iodine 196
Chapter 19. Chromium 198
Occurrence 198
The determination of chromium 200
Determination of chromium with EDTA 201
Determination of chromium as alkali Chromate 204
Determination of chromium using sym-diphenylcarbazide 208
Determination of chromium by atomic absorption
spectroscopy 212
Chapter 20. Cobalt 214
Occurrence 214
The determination of cobalt 214
Photometric methods for the determination of cobalt 215
Determination of cobalt with nitroso-R-salt 216
Determination of cobalt with thiocyanate and
tri-n-butylamine 219
Ion-exchange separation and determination with CyDTA 221
Chapter 21. Copper 224
Occurrence 224
The determination of copper 225
Photometric methods 225
Determination by atomic absorption spectroscopy 226
Determination of copper with 2, 2 -diquinolyl 226
Extraction and determination of copper with dithizone 230
Extraction of copper, lead and zinc 231
Determination of copper with dithizone 233
Chapter 22. Fluorine 235
Occurrence 235
The determination of fluorine 236
The lead chlorofluoride method 238
The photometric determination of fluorine 239
Photometric determination without distillation 242
Pyrohydrolytic determination of fluorine 243
The determination of fluorine using an ion-selective
electrode 245
Chapter 23. Gallium 248
Occurrence 248
The determination of gallium 248
Determination of gallium by atomic absorption 252
Chapter 24. Germanium 254
Occurrence 254
The determination of germanium 255
Chapter 25. Hydrogen 260
Occurrence 260
Free hydrogen 260
Organic hydrogen 261
Water evolved at 105° 262
Total water 265
Loss on ignition 270
Chapter 26. Indium 271
Occurrence 271
Chapter 27. Iron 273
Occurrence . 273
Metallic iron 274
Sulphate iron 276
Carbonate iron 276
Sulphide iron 277
Ferrous iron 278
The Pratt method 281
The Wilson method 282
Photometric determination offerrous iron 283
The determination of ferrous iron in carbonaceous shales 284
Ferric iron 285
Total iron 286
Photometric reagents for iron 287
Photometric determination of iron in silicate rocks 289
The titrimetric determination of total iron 292
Method based upon stannous chloride reduction 293
Methods based upon metallic reducing agents 295
The titration of ferric iron 297
Chapter 28. Lead 299
Occurrence 299
The determination of lead in silicate rocks 300
Separation procedures 300
Methods of determination 301
A solvent extraction—spectrophotometric method 302
A sublimation procedure 304
Chapter 29. Magnesium 307
Occurrence 307
Gravimetric determination in silicate rocks 308
Pyrophosphate method 308
8-Hydroxyquinoline method 308
Titrimetric determination in silicate rocks 310
Determination with 8-hydroxyquinoIine 310
Determination with EDTA 310
The separation and determination of calcium and
magnesium 313
Photometric determination in silicate rocks 314
Determination of calcium and magnesium by atomic
absorption spectroscopy 319
Determination of magnesium in carbonate rocks 321
Chapter 30. Manganese 325
Occurrence 325
The determination of manganese in silicate rocks 326
Photometric determination 326
Determination with potassium periodate 329
Determination with ammonium persulphate 330
Determination with formaldoxime 331
Photometric determination of manganese in carbonatite
rocks 332
The determination of manganese by atomic absorption
spectroscopy 332
Chapter 31. Mercury 334
Occurrence 334
The determination of mercury in silicate rocks 334
Vapour absorption for the determination of mercury 335
Chapter 32. Molybdenum and Tungsten 338
Occurrence 338
The determination of molybdenum and tungsten 339
Photometric methods 340
The determination of tungsten and molybdenum in
silicate rocks 343
Chapter 33. Nickel 347
Occurrence 347
The determination of nickel in silicate rocks 348
Gravimetric determination with dimethylglyoxime 349
Photometric determination following a preliminary
separation by chloroform extraction 351
Photometric determination after ion-exchange
separation 351
Determination of nickel by atomic absorption
spectroscopy 355
Chapter 34. Niobium and Tantalum 357
Occurrence 357
The determination of niobium 358
Determination of niobium in carbonatites with hydrogen
peroxide 358
Determination of niobium in silicate rocks with
thiocyanate 362
The determination of niobium with 442-pyridylazo)-
resorcinol 366
The determination of niobium by atomic absorption
spectroscopy 370
The determination of tantalum 370
Chapter 35. Nitrogen 372
Occurrence 372
The determination of nitrogen 372
Chapter 36. Phosphorus 375
Occurrence 375
The determination of phosphorus 376
The determination of phosphorus using a vanadomolybdate
reagent 376
Acid-soluble phosphate in phosphate rock 377
Total phosphorus in silicate rocks 378
Determination of phosphorus in carbonate rocks 380
The determination of phosphorus as a molybdenum blue 381
Determination in silicate rocks 383
Chapter 37. Scandium, Yttrium and the Lanthanide Rare Earths 386
Occurrence 386
The determination of scandium in silicate rocks 387
The determination of yttrium 389
The determination of the lanthanide rare earths 389
Gravimetric determination in silicate rocks 389
Gravimetric determination in carbonatite rocks 393
Photometric determination of rare earths in silicate rocks 394
Chapter 38. Selenium and Tellurium 398
Occurrence 398
The determination of selenium 398
The determination of tellurium 402
The determination of selenium and tellurium by atomic
absorption spectroscopy 402
Chapter 39. Silicon 404
Occurrence 404
Gravimetric determination of silica in quartzites and
sandstones 405
Gravimetric determination in silicate and carbonate rocks 407
Determination in carbonate rocks 408
Gravimetric determination without dehydration 408
A titrimetric method for silicate rocks 410
Photometric determination of silica 411
A combined gravimetric and photometric determination
of silica 415
The determination of silica by atomic absorption
spectroscopy 417
Chapter 40. Silver, Gold and the Platinum Metals 418
Occurrence 418
The determination of silver, gold and the platinum
metals 421
Chapter 41. Strontium 423
Occurrence 423
The determination of strontium 424
Determination by flame photometry 425
Determination by atomic absorption spectroscopy 427
Chapter 42. Sulphur 429
Occurrence 429
Free sulphur 429
Sulphide-sulphur 430
Water-soluble sulphur 432
Acid-soluble sulphur 432
Total sulphur 433
Chapter 43. Thallium 436
Occurrence 436
The photometric determination of thallium in silicate rocks 437
The fluorimetrie determination of thallium in silicate rocks 440
Chapter 44. Thorium 443
Occurrence 443
The determination of thorium 444
Gravimetric determination 444
Photometric methods 444
Separation methods 446
The determination in silicate rocks 447
xiv CONTENTS
Chapter 45. Tin 452
Occurrence 452
The determination of tin 453
Sample decomposition 453
Separation of tin 455
Photometric determination 456
The determination of tin in silicate rocks 458
Determination with catechol violet 458
Determination using salicylideneamino-2-thiophenol 460
The determination of tin by atomic absorption spectroscopy 461
Chapter 46. Titaniiim 462
Occurrence 462
The photometric determination of titanium in silicate rocks 463
Method using hydrogen peroxide 464
Method using diantipyrylmethane 468
Method using tiron 471
The determination of titanium by atomic absorption
spectroscopy 473
Chapter 47. Uranium 475
Occurrence 475
The determination of uranium 476
Photometric methods 476
Separation of uranium 478
The determination in silicate rocks 478
Chapter 48. Vanadium 484
Occurrence 484
The determination of vanadium in silicate rocks 485
Phosphotungstate method 485
Method using N-benzoyl-o-tolylhydroxylamine 488
Diaminobenzidine method 491
Chapter 49. Zinc 494
Occurrence 494
The determination of zinc in silicate rocks 495
Ion-exchange—zincon method 495
Determination of zinc by atomic absorption spectroscopy 499
Chapter 50. Zirconium and Hafnium 500
Occurrence 500
Gravimetric determination in silicate rocks 501
Phosphate method 501
Other gravimetric methods 503
Photometric methods for the determination of zirconium
and hafnium 503
The determination of hafnium 505
|
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| indexdate | 2024-07-09T15:39:05Z |
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| language | English |
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| series | International series of monographs on analytical chemistry. |
| series2 | International series of monographs on analytical chemistry. |
| spelling | Jeffery, Paul G. Verfasser aut Chemical methods of rock analysis by P. G. Jeffery 2. ed. Oxford (u.a.) Pergamon Pr. 1975 XIX, 525 S. Ill., graph. Darst. 22 cm txt rdacontent n rdamedia nc rdacarrier International series of monographs on analytical chemistry. 36 Roches - Analyse Rocks Analysis Analytische Chemie (DE-588)4129906-1 gnd rswk-swf Gestein (DE-588)4020734-1 gnd rswk-swf Geochemische Analyse (DE-588)4290341-5 gnd rswk-swf Chemisches Verfahren (DE-588)4454573-3 gnd rswk-swf Nachweis (DE-588)4115334-0 gnd rswk-swf (DE-588)4144950-2 Bestimmungsbuch gnd-content Gestein (DE-588)4020734-1 s Nachweis (DE-588)4115334-0 s Chemisches Verfahren (DE-588)4454573-3 s DE-604 Geochemische Analyse (DE-588)4290341-5 s Analytische Chemie (DE-588)4129906-1 s 1\p DE-604 International series of monographs on analytical chemistry. 36 (DE-604)BV001889010 36 HBZ Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=001323170&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis 1\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk |
| spellingShingle | Jeffery, Paul G. Chemical methods of rock analysis International series of monographs on analytical chemistry. Roches - Analyse Rocks Analysis Analytische Chemie (DE-588)4129906-1 gnd Gestein (DE-588)4020734-1 gnd Geochemische Analyse (DE-588)4290341-5 gnd Chemisches Verfahren (DE-588)4454573-3 gnd Nachweis (DE-588)4115334-0 gnd |
| subject_GND | (DE-588)4129906-1 (DE-588)4020734-1 (DE-588)4290341-5 (DE-588)4454573-3 (DE-588)4115334-0 (DE-588)4144950-2 |
| title | Chemical methods of rock analysis |
| title_auth | Chemical methods of rock analysis |
| title_exact_search | Chemical methods of rock analysis |
| title_full | Chemical methods of rock analysis by P. G. Jeffery |
| title_fullStr | Chemical methods of rock analysis by P. G. Jeffery |
| title_full_unstemmed | Chemical methods of rock analysis by P. G. Jeffery |
| title_short | Chemical methods of rock analysis |
| title_sort | chemical methods of rock analysis |
| topic | Roches - Analyse Rocks Analysis Analytische Chemie (DE-588)4129906-1 gnd Gestein (DE-588)4020734-1 gnd Geochemische Analyse (DE-588)4290341-5 gnd Chemisches Verfahren (DE-588)4454573-3 gnd Nachweis (DE-588)4115334-0 gnd |
| topic_facet | Roches - Analyse Rocks Analysis Analytische Chemie Gestein Geochemische Analyse Chemisches Verfahren Nachweis Bestimmungsbuch |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=001323170&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| volume_link | (DE-604)BV001889010 |
| work_keys_str_mv | AT jefferypaulg chemicalmethodsofrockanalysis |