Gas chromatographic detectors:
Saved in:
| Main Author: | |
|---|---|
| Format: | Book |
| Language: | English |
| Published: |
New York
Wiley
1974
|
| Series: | A Wiley-interscience publication.
|
| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Physical Description: | XII, 295 S., 2 Bl. Ill. u. graph. Darst. |
Staff View
MARC
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Record in the Search Index
| _version_ | 1804116409229246464 |
|---|---|
| adam_text | CONTENTS
One Introduction
I. Historical Background, 1
II. Classification of Detectors, 3
III. Definition of Terms, 7
A. Noise, 7
B. Sensitivity, 7
C. Detectability or Lower Limit
of Detection, 8
D. Specificity, 9
E. Linearity, 9
F. Response Time, 10
References, 10
Two Thermal Conductivity Detectors 14
I. Introduction, 14
A. Historical Background, 14
B. Definition, 15
II . Principles , 15
A. Basic Instrumentation, 15
B. Theory: Factors Affecting
Output Signal, 16
III. Developments Leading to Current
Designs, 29
vii
viii Contents
IV. Performance, 34
A. Factors Affecting Response, 34
B. Sensitivity and Response, 37
C. Linear Dynamic Range, 38
D. Noise and Drift, 38
References, 39
Three Flame Ionization Detection 42
I. Introduction, 42
II. Theory, Mechanisms, and Evolution of
Detector Designs, 42
III. Flame Mechanisms, 51
IV. Response Characteristics, 53
A. Influence of Geometry, 53
B. Group and Molecular Influence, 61
V. Performance, 70
A. Sensitivity and Noise, 70
B. Linear Range, 72
C. Maintenance, 72
References, 73
Four Electron Capture Detection 76
I. Introduction, 76
II. Background, Development and Current
Designs, 77
III. Electron Capture Mechanisms, 92
A. Introduction, 92
B. Kinetics, 92
C. Temperature Dependence, 95
IV. Response Characteristics, 96
A. Influence of Operating Vari-
ables, 96
B. Group and Molecular Response
Characteristics, 104
Contents ix
V. Performance, 106
A. Sensitivity and Noise, 106
B. Linear Range, 109
References, 112
Five The Thermionic Detector 114
I. Introduction, 114
II. Background, Principles, and
Development, 115
A. Basis, 115
B. Background and Development, 115
III. Principles and Mechanisms of
Detection, 122
A. Halogens, 122
B. Phosphorus, 125
C. Summary, 12 8
IV. Response Characteristics, 129
A. Effect of Gas Flow Rates, 129
B. Effect of Alkali Metal Salt
Used, 130
C. Effect of Applied Potential and
Polarity of the Electrodes, 132
D. Effect of Electrode Position,- 133
V. Performance, 133
A. Sensitivity, 133
B. Specificity, 135
C. Linear Dynamic Range and Noise
Level, 135
References, 140
Six The Ultrasonic Detector 144
I. Introduction, 144
Contents
II. Background, Theory, and Development
Leading to Current Designs, 144
A. Theory, 145
B. Development and Current Design,
148
III. Principles, 152
IV. Response Characteristics and Factors
Affecting Response, 154
A. Temperature, 154
B. Pressure, 155
C. Flow Rate, 156
D. Transducer Separation, 157
E. Cell Volume, 157
F. Predictability of Response, 158
G. Carrier Gases, 159
V. Performance, 161
A. Sensitivity, 161
B. Noise, 162
C. Linearity, 162
References, 164
Seven The Helium Ionization Detector 165
I. Introduction, 165
II. Background, Development, and
Principles, 165
A. Theory, 165
B. Background and Development, 166
III. Response Characteristics and Factors
Affecting Response, 168
IV. Performance, 173
A. Sensitivity. Linearity, and
Noise, 173
B. Precision, 175
References, 176
Contents xi
Eight Flame Photometric Detection 177
I. Introduction, 177
II. Theory, Background, and Current
Designs, 177
III. Response Characteristics and
Mechanisms, 181
IV. Performance, 187
A. Sensitivity and Specificity, 187
B. Noise, 192
C. Linear Range, 192
D. Additional Information, 192
References, 192
Nine Electrochemical Detectors 194
I. Introduction, 194
II. Background and Theory of the Various
Types, 194
A. The Microcoulometric Detector, 195
B. The Coulson Electrolytic Conduc-
tivity Detector, 199
C. The Reaction Coulometer, 203
III. Development and Principles of Current
Designs and Response Characteristics,
211
A. The Microcoulometric Detector, 211
B. The Coulson Electrolytic Conduc-
tivity Detector, 219
C. The Reaction Coulometer, 223
IV. Performance, 223
A. The Microcoulometric Detector, 223
B. The Coulson Electrolytic Conduc-
tivity Detector, 225
C. The Reaction Coulometer, 226
References, 229
xii Contents
Ten Miscellaneous Detectors 231
I. Introduction, 231
II. Detectors, 231
A. The Palladium Detector, 231
B. Molecular Weight Detector, 233
C. Catalytic Ionization Detector, 235
D. Discharge Detectors, 238
E. Selective Detector for Hydrogen-
atable Material, 252
F. Flame Emission Detectors, 255
G. Piezoelectric Sorption Detector, 260
H. Dielectric Constant Detectors, 261
I. Kr85 Clathrate Detector, 261
J. The Gas Density Detector, 261
K. Carbon, Hydrogen, and Nitrogen
Detectors, 267
L. The Cross Section Ionization
Detector, 268
M. Semiconductive Thin-Film Detector,
273
References, 274
Author Index 279
Subject Index 289
Appendix
Flame Ionization Fault Diagnosis
Chart (See Fold-out)
GC Nomenclature (See Fold-out)
|
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| id | DE-604.BV001965859 |
| illustrated | Illustrated |
| indexdate | 2024-07-09T15:38:03Z |
| institution | BVB |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-001282067 |
| oclc_num | 601226 |
| open_access_boolean | |
| owner | DE-355 DE-BY-UBR DE-188 |
| owner_facet | DE-355 DE-BY-UBR DE-188 |
| physical | XII, 295 S., 2 Bl. Ill. u. graph. Darst. |
| publishDate | 1974 |
| publishDateSearch | 1974 |
| publishDateSort | 1974 |
| publisher | Wiley |
| record_format | marc |
| series2 | A Wiley-interscience publication. |
| spelling | David, Donald J. Verfasser aut Gas chromatographic detectors New York Wiley 1974 XII, 295 S., 2 Bl. Ill. u. graph. Darst. txt rdacontent n rdamedia nc rdacarrier A Wiley-interscience publication. Chromatographie en phase gazeuse - Appareils et matériel Chromatographic detectors Gas chromatography Equipment and supplies Gaschromatographie (DE-588)4019330-5 gnd rswk-swf Detektor (DE-588)4123055-3 gnd rswk-swf Detektor (DE-588)4123055-3 s Gaschromatographie (DE-588)4019330-5 s DE-604 HBZ Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=001282067&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | David, Donald J. Gas chromatographic detectors Chromatographie en phase gazeuse - Appareils et matériel Chromatographic detectors Gas chromatography Equipment and supplies Gaschromatographie (DE-588)4019330-5 gnd Detektor (DE-588)4123055-3 gnd |
| subject_GND | (DE-588)4019330-5 (DE-588)4123055-3 |
| title | Gas chromatographic detectors |
| title_auth | Gas chromatographic detectors |
| title_exact_search | Gas chromatographic detectors |
| title_full | Gas chromatographic detectors |
| title_fullStr | Gas chromatographic detectors |
| title_full_unstemmed | Gas chromatographic detectors |
| title_short | Gas chromatographic detectors |
| title_sort | gas chromatographic detectors |
| topic | Chromatographie en phase gazeuse - Appareils et matériel Chromatographic detectors Gas chromatography Equipment and supplies Gaschromatographie (DE-588)4019330-5 gnd Detektor (DE-588)4123055-3 gnd |
| topic_facet | Chromatographie en phase gazeuse - Appareils et matériel Chromatographic detectors Gas chromatography Equipment and supplies Gaschromatographie Detektor |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=001282067&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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