The palladium hydrogen system:
Saved in:
| Main Author: | |
|---|---|
| Format: | Book |
| Language: | English |
| Published: |
London
Acad. Press
1967
|
| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Physical Description: | XII, 178 S. Ill., graph. Darst. |
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| 100 | 1 | |a Lewis, Frederick A. |e Verfasser |4 aut | |
| 245 | 1 | 0 | |a The palladium hydrogen system |c F. A. Lewis |
| 264 | 1 | |a London |b Acad. Press |c 1967 | |
| 300 | |a XII, 178 S. |b Ill., graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
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| 650 | 4 | |a Hydrure de palladium | |
| 650 | 7 | |a Metall-Wasserstoff-System |2 swd | |
| 650 | 7 | |a Palladium |2 gtt | |
| 650 | 7 | |a Palladium |2 swd | |
| 650 | 7 | |a Systemen |2 gtt | |
| 650 | 7 | |a Waterstof |2 gtt | |
| 650 | 4 | |a Palladium-hydrogen | |
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Record in the Search Index
| _version_ | 1804116382107828224 |
|---|---|
| adam_text | THE
PALLADIUM
HYDROGEN
SYSTEM
F. A. LEWIS
DEPARTMENT OF CHEMISTRY
THE QUEEN S UNIVERSITY OF BELFA ST
NORTHERN IRELAND
ACADEMIC PRESS * 1967
LONDON NEW YORK
CONTENTS
PREFACE
.......... V
CHAPTER
1. GENERAL INTRODUCTION
A. COMPARISON OF THE PROPERTIES OF PALLADIUM WITH THOSE OF
OTHER TRANSITION ELEMENTS ..... 1
B. PERMEATION OF HYDROGEN THROI IGH TRANSITION ELEMENTS*
OCCLUSION BY PALLADIUM ..... 3
C. PRESSURE-COMPOSITION-TEMPERATURE (P-C-T) RELATION
SHIPS: NON-STOICHIOMETRY ...... 4
D. INTRODUCTION OF HYDROGEN INTO PALLADIUM BY ELECTROLYSIS 5
E. GENERAL COMPARISON OF THE SOLUBILITY OF HYDROGEN IN
OTHER TRANSITION ELEMENTS ..... 6
F. SOLUBILITY OF HYDROGEN IN OTHER ELEMENTS OF GROUP 8 . 6
G. ABSORPTION OF HYDROGEN BY TRANSITION ELEMENTS OF
GROUPS 3, 4 AND 5 ...... 8
H. CHANGES OF THE ELECTRICAL RESISTANCE OF PALLADIUM AS A
FUNCTION OF HYDROGEN CONTENT: HYDROGENIUM . 10
I. THE INTRODUCTION OF HYDROGEN INTO PALLADIUM IN THE
COURSE OF CHEMICAL REACTIONS: PALLADIUM AS AN HYDRO-
GENATION
CATALYST
. . . . . . .11
CHAPTER
2. THERMODYNAMIC FACTORS
A. STAGES IN THE ACCUMULATION OF PRESSURE-COMPOSITION-
TEMPERATURE (P-C-T) RELATIONSHIPS BY DIRECT EQUILI
BRATION WITH HYDROGEN GAS: NON-STOICHIOMETRIC COM
POSITION
OF THE
HYDRIDED
SOLIDS . . . .13
B. THE CURRENT POSITION REGARDING PD
2
H ... 18
C. RELATIONSHIPS AT HIGHER TEMPERATURES THAN T
C
.20
D. THE PROBLEM OF OBTAINING EQUILIBRIUM BETWEEN SOLID
AND GASEOUS PHASES . . . . . .22
E. HYSTERESIS OF P-C RELATIONSHIPS BELOW T
R
. .23
F. P-C RELATIONSHIPS OVER PURELY A- OR /J-PHASE REGIONS . 30
VII
VIII
CONTENTS
G. RELATIONSHIPS AT VERY LOW TEMPERATURES ... 30
H. UNITS OF COMPOSITION . . . . . .31
I. RELATIONSHIPS BETWEEN ELECTRODE POTENTIAL AND HYDRO
GEN CONTENT AND CORRELATIONS WITH P-C-T RELATION
SHIPS
......... 31
J. CATALYTIC ACTIVITY OF ELECL RODES AND THE INTERCONVERSION
OF E AND P . . . . . . .36
K. INDEPENDENCE OF THE E AGAINST H/PD RELATIONSHIPS ON THE
METHODS OF INTRODUCING OR REMOVING HYDROGEN . 36
- L. THE
PALLADIUM
BIELECTRODE . . . . .37
M. OTHER MEASUREMENTS OF HYDROGEN OVERPOTENTIAL AT
PALLADIUM CATHODES ...... 38
N. CALORIMETRIC DETERMINATIONS OF HEATS OF ABSORPTION AND
DESORPTION OF HYDROGEN AND OF THE SPECIFIC HEAT OF
HYDROGEN
IN PALLADIUM
...... 39
0. DETERMINATIONS OF PARTIAL MOLAR HEATS AND ENTROPIES OF
ABSORPTION AND DESORPTION OF HYDROGEN FROM THE
TEMPERATURE DEPENDENCE OF P-C RELATIONSHIPS . . 41
CHAPTER 3. CHANGES OF THE SHAPE AND OF MECHANICAL
AND ELASTIC PROPERTIES OF PALLADIUM
RESULTING FROM ABSORPTION AND
DESORPTION OF HYDROGEN
A. CHANGES OF ELASTIC CONSTANTS AS A FUNCTION OF HYDROGEN
CONTENT
........ 43
B. CHANGES OF HARDNESS AND F
INTERNAL FRICTION . . 44
C. MICROSCOPIC EXAMINATION OF CHANGES OF THE TOPOLOGY OF
PALLADIUM SURFACES FOLL( WING ABSORPTION OF HYDROGEN 47
D. CHANGES OF SHAPE OF PALLADIUM SPECIMENS FOLLOWING
REPEATED CYCLES OF ABSORPTION AND DESORPTION OF
HYDROGEN
........ 48
CHAPTER 4. RELATIONSHIPS BETWEEN HYDROGEN CONTENT
AND ELECTRICAL RESISTANCE
A. GENERAL FORM OF THE RELATIONSHIPS BETWEEN H/PD AND
RJR
0
AND THE PROBLEM OF HYSTERESIS ... 50
B. HYSTERESIS OF RELATIONSHIPS BETWEEN H/PD AND RJR
0
. 54
CONTENTS
C. TEMPERATURE DEPENDENCE OF RELA TIONSHIPS BETWEEN H/PD
AND R/R
0
........
D. RELATIONSHIPS BETWEEN H/PD AND R/R
0
AT VERY LOW
TEMPERATURES
.......
E. THE USE OF RESISTANCE MEASUREMENTS AS AN ANALYTICAL
GUIDE TO HYDROGEN CONTENT 1 URING MEASUREMENTS OF
OTHER PARAMETERS .
P. APPLICATION OF RESISTANCE MEASUREMENTS TO STUDIES OF
RATES OF ABSORPTION AND DESORPTION OF HYDROGEN
G. ERRORS IN MEASUREMENTS OF THE ELECTRICAL RESISTANCE OF
* SPECIMENS IMMERSED IN SOLUTION DUE TO CO-CONDUCTION
OF THE MEASURING CURRENT THROUGH THE ELECTROLYTE
CHAPTER
5. CHEMICAL STABILITY OF HYDR.ID.ED
PALLADIUM
A. THE USE OF MEASUREMENTS OF PHYSICAL AND PHYSICO-
CHEMICAL PARAMETERS FOR ESTIMATIONS OF GAIN AND LOSS
OF HYDROGEN
........
B. CHEMICAL STABILITY OF SPECIMENS WITH HIGHLY-ACTIVE
SURFACES IN CONTACT WITH THE (RASEOUS PHASE
C. STABILITY OF SPECIMENS WITH HIGHIY-ACTIVE SURFACES IM
MERSED IN AQUEOUS SOLUTIONS .
D. STABILITY OF SPECIMENS WITH SURFACES WHICH ARE RELA
TIVELY INACTIVE FOR EQUILIBRATION WITH HYDROGEN
MOLECULES
........
CHAPTER
6. ABSORPTION OF HYDROGEN BY ALLOYS OF
PALLADIUM
A. SOME GENERAL COMMENTS ......
B. CRYSTAL STRUCTURES OF THE HYDROGEN-FREE ALLOYS
C. ABSORPTION OF HYDROGEN DURING, ELECTROLYTIC DISCHARGE
AND SUBSEQUENT COMPARISONS OF THE SOLUBILITY OF
HYDROGEN AS A FUNCTION OF A] LOY COMPOSITION .
D. DIRECT DERIVATION OF P-C-T RELATIONSHIPS FOR ALLOYS
E. DERIVATION OIP~C-T RELATIONSHI PS FROM MEASUREMENTS OF
ELECTRODE POTENTIAL ......
F. ACTIVATION OF ELECTRODES ......
G. METHODS OF ESTIMATING CHANGES OF HYDROGEN CONTENT .
H. ESTIMATIONS OF CHANGES OF HYDROGEN CONTENT DURING
DESORPTION
........
X
CONTKUTS
I.
COMPARISON OF P-C-T RELATIONSHIPS FOR THE VARIOUS
. ALLOY SYSTEMS .......
80
J.
HYSTERESIS OF P-C-T RELATIONSHIPS ....
86
K.
CRITICAL AND SUPERCRITICAL ISOTHERMS ....
86
L.
CHANGES OF PARTIAL MOLAR HEATS AND ENTROPIES OF ABSORP-
TION AND DESORPTION OF HYDROGEN AS A FUNCTION OF
ALLOY COMPOSITION AND BYDROGEN CONTENT . . 88
M. RELATIONSHIPS BETWEEN HYDROGEN CONTENT AND ELECTRICAL
RESISTANCE
........ 90
- N. CHANGES OF THE TEMPERATURE COEFFICIENT OF ELECTRICAL
RESISTANCE WITH CHANGES OF HYDROGEN CONTENT . . 93
CHAPTER 7. DIFFUSION OF HYDROGEN THROUGH PALLADIUM
AND PALLADIUM ALLOYS
A. GENERAL INTRODUCTION AND D ISCUSSION OF USES OF PALLADIUM
MEMBRANES ........
94
B. GENERAL FORMULATION OF DIFFUSION EQUATIONS BASED ON
FICK S FIRST LAW ....... 95
C. EXPRESSING FICK S EQUATION IN TERMS OF PRESSURE . . 95
D. SOME GENERAL COMMENTS ON THE INFLUENCE OF SURFACE
PROCESSES ON PERMEATION RATES .... 96
E. LIMITING LOWER TEMPERATURES FOR RAPID RATES OF
PERMEATION: VARIOUS METHODS OF PRE-ACTIVATION OF
SURFACES
........ 97
F. CHEMICAL POISONING OF THE 1 )IFFUSION PROCESS... 97
G. ADEQUATE GAS CIRCULATION: BLEED RATES . . 98
H. SOME METHODS OF MEASUREMENT OF PERMEATION RATES . 99
I. CALCULATION OF A-PHASE DIFFUSION COEFFICIENTS (D
A
) FROM
STUDIES INVOLVING ONLY GAS/SOLID INTERFACES . .101
J. MIGRATION OF HYDROGEN IN A-PHASE COMPOSITIONS IN AN
ELECTRIC FIELD GRADIENT . . . . . .103
K. GENERAL CONSIDERATIONS OF HE DIFFUSION OF HYDROGEN IN
ELECTRODES
. . . . . . . .104
L. PROBLEMS IN THE DETERMINA TION OF DIFFUSION COEFFICIENTS
FROM ELECTROCHEMICAL EXPERIMENTS . . . .106
M. DIFFUSION
OF HYDROGEN
IN TLI
E P-PHASE
. . .
.108
N. ELECTROCHEMICAL
STUDIES
OF D$ . . . .109
0. PRESENCE OF AN X-/(3-PHASE
BOUNDARY WITHIN THE MEM
BRANE
UNDER
STEADY-STATE
CONDITIONS . . .110
CONTENTS X
P. MOVEMENT OF THE BOUNDARY BET WEEN A- AND (3-PHASES . 112
Q. DIFFUSION PROCESSES, NUCLEAR MAGNETIC RESONANCE ABSORP
TION
AND
HEAT
LEAK
MEASUREMENTS
. . . .113
R. DIFFUSION OF HYDROGEN THROUGH ALLOYS OF PALLADIUM, AND
IMPROVED RESISTANCE TO DEFORMATION . . .114
S. POSSIBLE CORRELATIONS BETWEEN DEFORMATION AND
HYSTERESIS
. . . . . . . .115
T. DIFFUSION COEFFICIENTS FOR HYDROGEN IN PD ALLOYS . . 117
CHAPTER
8. ABSORPTION OF DEUTERIUM BY PALLADIUM
AND ALLOYS OF PALLADIUM: SEPARATION
OF HYDROGEN ISOTOPES
A. COMPARISON OF P-C-T RELATIONSHIPS FOR THE PD/H AND
PD/D SYSTEMS . . . . . . .118
B. P-C-T RELATIONSHIPS DERIVED FROM ELECTRODE POTENTIAL
MEASUREMENTS . . . . . .124
C. PARTIAL MOLAR HEATS AND ENTROPIES OF ABSORPTION AND
DESORPTION OF DEUTERIUM: HEAT CAPACITY MEASURE
MENTS ......... 125
D. VARIATION OF THE ELECTRICAL RESISTANCE OF PALLADIUM AS A
FUNCTION OF DEUTERIUM CONTENT . . .127
E. ISOTHERMAL RELATIONSHIPS OBTAINED WITH MIXTURES OF
HYDROGEN AND DEUTERIUM . . . .129
F. COMPARISON OF DIFFUSION COEFFICIENTS LOR HYDROGEN AND
DEUTERIUM
........ 130
G. SEPARATION OF HYDROGEN ISOTOPES BY GAS CHROMATO
GRAPHIC TECHNIQUES USING COLUMN PACKINGS COATED
WITH
PALLADIUM . . . . . . .130
H. FACTORS INVOLVED IN THE SEPARATION OF HYDROGEN ISOTOPES
DURING ELECTROLYSIS AT PALLADIUM ELECTRODES . . 133
CHAPTER
9. INVESTIGATIONS OF CHANGES OF LATTICE
STRUCTURE AND OF SOME OTHER PHYSICAL
AND ELECTRICAL PROPERTIES AS FUNCTIONS
OF HYDROGEN AND DEUTERIUM CONTENTS
A. GENERAL X-RAY CRYSTALLOGRAPHIC EVIDENCE OF LATTICE
EXPANSION AND OF THE CO-EXISTENCE OF TWO HYDRIDE
PHASES OVER REGIONS OF PRESSURE INVARIANCE . . 183
XLL CONTENTS
B. CORRELATION OF LATTICE PARAMETERS WITH P-C RELATION
SHIPS AND WITH HYSTERESIS . . . . 139
C. MEASUREMENTS OF CHANGES OF LATTICE PARAMETERS AT CLOSE
TO ROOM TEMPERATURE . . . . . .141
D. CHANGES OF LATTICE PARAMETERS IN THE PALLADIUM/
DEUTERIUM SYSTEM . . . . . .143
E. LINE-BROADENING OF X-RAY REFLECTIONS .... 143
F. X-RAY CRYSTALLOGRAPHIC STUDIES OF THE ABSORPTION OF
HYDROGEN BY ALLOYS OF PALLADIUM . . . 143
G. X-RAY EVIDENCE FOR ANALOGOUS P-PHASE HYDRIDES OF
NICKEL . . . . . . . .145
H. NEUTRON DIFFRACTION STUDIES AND THE LOCATION OF HYDRO
GEN IN THE CRYSTAL LATTICE . . . . . ] 45
I. LOCATION OF THE HYDROGEN IN A-PHASE HYDRIDES . .146
J. FACE-CENTRED-CUBIC SYMMETRY AND LATTICE VACANCIES IN
(3-PHASE HYDRIDES . . . . . . .147
K. CHANGES OF MAGNETIC SUSCEPTIBILITY AS A FUNCTION OF
HYDROGEN CONTENT . . . . . .147
L. CHANGES OF OTHER ELECTRICA [ PROPERTIES OF PALLADIUM AND
PALLADIUM ALLOYS AS A FUNCTION OF HYDROGEN CONTENT 149
CHAPTER 10. THEORETICAL MODELS FOR THE PD/H AND
RELATED SYSTEMS
A. POSSIBLE EXPLANATIONS OF CERTAIN RESULTS IN TERMS OF THE
BEHAVIOUR OF HYDROGEN CONTAINED IN FISSURES OR
RIFTS 152
B. THE PSEUDO-SILVER HYPOTHESIS . . . . 153
C. THE POSSIBILITY THAT THE HYDROGEN IS DISSOLVED AS
PROTONS . . . . . . . .154
D. THE POSSIBILITY OF ORDERING TO MORE COVALENT MOLECULAR
UNITS AT VERY LOW TEMPERATURES . . . .155
E. THEORETICAL DERIVATION OF P-C RELATIONSHIPS . .156
REFERENCES AND AUTHOR INDEX . . . . .161
SUBJECT INDEX ........ 175
|
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| id | DE-604.BV001941692 |
| illustrated | Illustrated |
| indexdate | 2024-07-09T15:37:37Z |
| institution | BVB |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-001265570 |
| oclc_num | 2118322 |
| open_access_boolean | |
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| owner_facet | DE-91G DE-BY-TUM DE-355 DE-BY-UBR DE-19 DE-BY-UBM DE-83 DE-210 DE-29T |
| physical | XII, 178 S. Ill., graph. Darst. |
| psigel | TUB-nveb |
| publishDate | 1967 |
| publishDateSearch | 1967 |
| publishDateSort | 1967 |
| publisher | Acad. Press |
| record_format | marc |
| spelling | Lewis, Frederick A. Verfasser aut The palladium hydrogen system F. A. Lewis London Acad. Press 1967 XII, 178 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Hydrure de palladium Metall-Wasserstoff-System swd Palladium gtt Palladium swd Systemen gtt Waterstof gtt Palladium-hydrogen HEBIS Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=001265570&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Lewis, Frederick A. The palladium hydrogen system Hydrure de palladium Metall-Wasserstoff-System swd Palladium gtt Palladium swd Systemen gtt Waterstof gtt Palladium-hydrogen |
| title | The palladium hydrogen system |
| title_auth | The palladium hydrogen system |
| title_exact_search | The palladium hydrogen system |
| title_full | The palladium hydrogen system F. A. Lewis |
| title_fullStr | The palladium hydrogen system F. A. Lewis |
| title_full_unstemmed | The palladium hydrogen system F. A. Lewis |
| title_short | The palladium hydrogen system |
| title_sort | the palladium hydrogen system |
| topic | Hydrure de palladium Metall-Wasserstoff-System swd Palladium gtt Palladium swd Systemen gtt Waterstof gtt Palladium-hydrogen |
| topic_facet | Hydrure de palladium Metall-Wasserstoff-System Palladium Systemen Waterstof Palladium-hydrogen |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=001265570&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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