Organometallics: a concise introduction
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| Main Authors: | , |
|---|---|
| Format: | Book |
| Language: | English German |
| Published: |
Weinheim [u.a.]
VCH
1989
|
| Edition: | 1. ed. |
| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Item Description: | Literaturverz. S. 442 - 456 |
| Physical Description: | XI, 479 S. zahlr. graph. Darst., Tab. |
| ISBN: | 3527278184 0895738694 |
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Record in the Search Index
| _version_ | 1804116294758301696 |
|---|---|
| adam_text | IMAGE 1
CHRISTOPH ELSCHENBROICH
ALBRECHT SALZER
ORGANOMETALLICS
A CONCISE INTRODUCTION
ZFS SA T
- 0 .
VCH
IMAGE 2
CONTENTS
PREFACE
INTRODUCTION L
1 H I S T O R I C AL D E V E L O P M E NT A ND C U R R E NT T R E N DS
IN O R G A N O M E T A L L IC C H E M I S T RY . .. 1
2 D E M A R C A T I ON A ND C L A S S I F I C A T I ON OF O R G A N O M
E T A L L IC C O M P O U N DS 7
3 ENERGY, POLARITY AND REACTIVITY OF THE M -C BOND 10
3.1 STABILITY OF MAIN-GROUP ORGANOMETALLICS 10
3.2 LABILITY OF MAIN-GROUP ORGANOMETALLICS 12
MAIN-GROUP ORGANOMETALLICS
4 METHODS OF PREPARATION IN PERSPECTIVE 15
5 ALKALI ORGANOMETALLICS 19
5.1 ORGANOLITHIUM COMPOUNDS 19
EXCURSION: 6 L I - A ND 7 LI-NMR OF ORGANOLITHIUM COMPOUNDS 24
5.2 ORGANYLS OF THE HEAVIER ALKALI METALS 33
EXCURSION: ESR SPECTROSCOPY OF ORGANOALKALI METAL COMPOUNDS 35
6 ORGANOMETALLICS OF GROUPS 2 AND 12 38
6.1 ORGANOMETALLICS OF THE ALKALINE EARTHS (GROUP 2) 38
6.1.1 ORGANOBERYLLIUM COMPOUNDS 38
6.1.2 ORGANOMAGNESIUM COMPOUNDS 40
6.1.3 ORGANOCALCIUM, -STRONTIUM AND -BARIUM COMPOUNDS 47
6.2 ORGANOMETALLICS OF ZN, CD, HG (GROUP 12) 48
6.2.1 ORGANOZINC COMPOUNDS 48
6.2.2 ORGANOCADMIUM COMPOUNDS 50
6.2.3 ORGANOMERCURY COMPOUNDS 50
EXCURSION: ORGANOMERCURY COMPOUNDS IN VIVO 54
7 ORGANOMETALLICS OF THE BORON GROUP (GROUP 13) 57
7.1 ORGANOBORON COMPOUNDS 57
7.1.1 ORGANOBORANES 57
IMAGE 3
VIII CONTENTS
7.1.2 BORON HETEROCYCLES 62
7.1.3 POLYHEDRAL BORANES, CARBABORANES AND HETEROCARBABORANES . . .. 66
EXCURSION: U B - N MR OF ORGANOBORON COMPOUNDS 73
7.2 ORGANOALUMINUM COMPOUNDS 75
7.3 GALLIUM-, INDIUM-, AND THALLIUM ORGANYLS 86
7.3.1 A ORGANYLS OF GA, IN, TL AND THEIR LEWIS-BASE ADDUCTS 86
7.3.2 N COMPLEXES OF GA, IN, AND TL 89
7.3.3 APPLICATIONS OF THALLIUM ORGANYLS IN ORGANIC SYNTHESIS 92
8 ORGANOELEMENT COMPOUNDS OF THE CARBON GROUP (GROUP 14) 94 8.1
ORGANOSILICON COMPOUNDS 95
8.1.1 SILICON ORGANYLS OF COORDINATION NUMBER 4 95
8.1.2 SILICON ORGANYLS OF COORDINATION NUMBERS 2 AND 3 AND THEIR
SUBSEQUENT PRODUCTS 105
8.2 ORGANOGERMANIUM COMPOUNDS 115
8.2.1 GERMANIUM ORGANYLS OF COORDINATION NUMBER 4 115
8.2.2 GERMANIUM ORGANYLS OF COORDINATION NUMBERS 2 AND 3 AND THEIR
SUBSEQUENT PRODUCTS 118
8.3 ORGANOTIN COMPOUNDS 121
EXCURSION: N9 SN-M6SSBAUER AND 119 SN-NMR SPECTROSCOPY 122
8.3.1 SN ORGANYLS OF COORDINATION NUMBERS 4, 5, AND 6 124
8.3.2 SN ORGANYLS OF COORDINATION NUMBERS 2 AND 3 131
8.4 ORGANOLEAD COMPOUNDS 137
8.4.1 PB IV ORGANYLS 138
8.4.2 PB 1 -AND PB ORGANYLS 143
9 ORGANOELEMENT COMPOUNDS OF THE NITROGEN GROUP (GROUP 15) 147 9.1
ELEMENT ORGANYLS (E = AS, SB, BI) 148
9.1.1 PENTAORGANOELEMENT COMPOUNDS R 5 E 148
9.1.2 ORGANOELEMENT DERIVATIVES R B EX 5 _ B 150
9.2 ELEMENT 1 ORGANYLS (E = AS, SB, BI) 152
9.2.1 TRISORGANOELEMENT COMPOUNDS R 3 E 152
9.2.2 ORGANOELEMENT DERIVATIVES R N EX 3 _ B 155
9.3 CHAINS AND RINGS CONTAINING E - E SINGLE BONDS 157
9.4 E = C AND E = E MULTIPLE BONDS 161
9.4.1 E = C(P N -P N ) BONDS 161
9.4.2 E = E(P 1T -PJ BONDS 165
10 ORGANOELEMENT COMPOUNDS OF SELENIUM AND TELLURIUM (GROUP 16) 167
11 ORGANOMETALLICS OF COPPER, SILVER AND GOLD (GROUP 11) 172
11.1 COPPER-AND SILVER ORGANYLS 172
11.2 GOLD ORGANYLS 178
IMAGE 4
CONTENTS IX
ORGANOMETALLIC COMPOUNDS OF THE TRANSITION ELEMENTS
12 THE 18-VALENCE-ELECTRON (18-VE) RULE 186
EXCURSION: CAN THE VSEPR CONCEPT (VALENCE JHELL ELECTRON-PAIR REPULSION,
GILLESPIE-NYHOLM MODEL) BE APPLIED TO TRANSITION-METAL COMPLEXES? . 191
13 R-DONOR LIGANDS 193
13.1 PREPARATION OF TRANSITION-METAL ALKYLS AND ARYLS 194
13.2 SELECTED PROPERTIES OF TRANSITION-METAL CR-ORGANOMETALLICS 197
13.2.1 THERMODYNAMIC STABILITY VERSUS KINETIC LABILITY 197
13.2.2 TRANSITION-METAL A-COMPLEXES IN VIVO 201
13.2.3 TRANSITION-METAL PERFLUOROCARBON R-COMPLEXES 204
14 FF-DONOR/N-ACCEPTOR LIGANDS . . . . * 206
14.1 TRANSITION-METAL ALKENYLS . * . 206
14.2 TRANSITION-METAL ALKYNYLS 208
14.3 TRANSITION-METAL CARBENE COMPLEXES 210
14.4 TRANSITION-METAL CARBYNE COMPLEXES 218
14.5 METAL CARBONYLS 220
14.5.1 PREPARATION, STRUCTURE AND PROPERTIES 221
14.5.2 VARIANTS OF CO BRIDGING 222
14.5.3 BONDING IN METAL CARBONYLS, THEORY AND EXPERIMENTAL EVIDENCE 226
14.5.4 PRINCIPAL REACTION TYPES OF METAL CARBONYLS 232
14.5.5 CARBONYLMETALLATES AND CARBONYL METAL HYDRIDES 234
14.5.6 CARBONYL METAL HALIDES 237
14.6 THIO-, SELENO-, AND TELLUROCARBONYL METAL COMPLEXES 238
14.7 ISOCYANIDE COMPLEXES (METAL ISONITRILES) 240
EXCURSION: PHOTOCHEMICAL REACTIVITY OF ORGANOTRANSITION METAL COMPLEXES
. 242
15 A, N-DONOR/N-ACCEPTOR LIGANDS . 252
15.1 OLEFIN COMPLEXES 252
15.1.1 HOMOALKENE COMPLEXES 252
15.1.2 HETEROALKENE COMPLEXES 270
15.2 ALKYNE COMPLEXES 272
15.2.1 HOMOALKYNE COMPLEXES 273
15.2.2 HETEROALKYNE COMPLEXES 279
15.3 ALLYL AND ENYL COMPLEXES 279
15.3.1 ALLYL COMPLEXES 280
15.3.2 DIENYL AND TRIENYL COMPLEXES 289
EXCURSION: 1 3 C - A N D H - N MR SPECTROSCOPY OF ORGANOMETALLICS 295
15.4 COMPLEXES OF THE CYCLIC RE-PERIMETERS C B H N 309
15.4.1 C 3 R^ AS A LIGAND 310
15.4.2 C 4 H 4 AS A LIGAND 311
15.4.3 C 5 HS AS A LIGAND 315
IMAGE 5
X CONTENTS
15.4.3.1 BINARY CYDOPENTADIENYL TRANSITION-METAL COMPLEXES 316 15.4.3.2
CYDOPENTADIENYL METAL CARBONYLS 333
15.4.3.3 CYDOPENTADIENYL METAL NITROSYLS 337
15.4.3.4 CYDOPENTADIENYL METAL HYDRIDES 339
15.4.3.5 CYDOPENTADIENYL METAL HALIDES 340
15.4.4 C 6 H 6 AS A LIGAND 342
15.4.4.1 BIS(ARENE)METAL COMPLEXES 343
15.4.4.2 ARENE METAL CARBONYLS 352
15.4.4.3 BENZENE CYDOPENTADIENYL METAL COMPLEXES 356
15.4.5 C 7 HJ AS A LIGAND 358
15.4.6 C 8 H 8 AS A LIGAND ^ 361
EXCURSION: TRANSITION METAL NMR IN ORGANOMETALLIC CHEMISTRY 370 15.5
METAL TT-COMPLEXES OF HETEROCYDES 376
15.5.1 NITROGEN-, PHOSPHORUS- AND SULFUR HETEROCYDES AS LIGANDS . . ..
376 15.5.2 BORON HETEROCYDES AS LIGANDS 380
15.5.3 BORON-NITROGEN HETEROCYLCES 385
16 METAL-METAL BONDS AND TRANSITION METAL ATOM CLUSTERS 386
16.1 FORMATION AND CRITERIA OF METAL -METAL BONDS 386
16.2 DINUCLEAR CLUSTERS 390
16.3 TRINUCLEAR CLUSTERS 392
16.4 TETRANUCLEAR CLUSTERS , . . 395
EXCURSION: STRUCTURE AND BONDING CONDITIONS IN CLUSTERS, THE ISOLOBAL
ANALOGY 396
16.5 APPROACHES TO SYSTEMATIC CLUSTER SYNTHESIS 402
16.6 PENTANUDEAR AND HIGHER NUDEARITY CLUSTERS 405
17 ORGANOMETALLIC CATALYSIS 411
17.1 CATALYTIC REACTIONS AND THE 16/18 VE RULE 412
17.2 TRANSITION METAL ASSISTED VALENCE ISOMERIZATIONS 415
EXCURSION: INTERACTION OF TRANSITION METAL FRAGMENTS WITH CYDOPROPANES .
4 16 17.3 ISOMERIZATION OF UNSATURATED MOLECULES 418
17.4 ARYLATION/VINYLATION OF OLEFINS (HECK REACTION) 419
17.5 ALKENE METATHESIS 419
17.6 OLIGOMERIZATION AND POLYMERIZATION 421
17.7 OLEFIN OXIDATION (WACKER PROCESS) 425
17.8 HYDROGENALION OF ALKENES 427
17.9 FISCHER-TROPSCH REACTIONS . 430
17.10 THE WATER-GAS SHIFT REACTION 432
17.11 MONSANTO ACETIC ACID PROCESS 433
17.12 HYDROFORMYLATION (OXO REACTION) 434
17.13 HYDROCYANATION 438
17.14 REPPE CARBONYLATION 438
17.15 ACTIVATION OF C-H BONDS IN ALKANES - A TOPICAL PROBLEM IN
ORGANOMETALLIC RESEARCH 439
IMAGE 6
CONTENTS XI
18 LITERATURE 442
APPENDIX 457
SYMBOLS AND ABBREVIATIONS 457
NOMENCLATURE OF ORGANOMETALLIC COMPOUNDS 459
AUTHOR INDEX 462
SUBJECT INDEX 467
|
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| id | DE-604.BV001809654 |
| illustrated | Illustrated |
| indexdate | 2024-07-09T15:36:14Z |
| institution | BVB |
| isbn | 3527278184 0895738694 |
| language | English German |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-001212984 |
| oclc_num | 19353879 |
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| owner_facet | DE-210 DE-20 DE-634 DE-83 DE-188 |
| physical | XI, 479 S. zahlr. graph. Darst., Tab. |
| publishDate | 1989 |
| publishDateSearch | 1989 |
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| publisher | VCH |
| record_format | marc |
| spelling | Elschenbroich, Christoph 1939- Verfasser (DE-588)124807410 aut Organometallchemie Organometallics a concise introduction Christoph Elschenbroich ; Albrecht Salzer 1. ed. Weinheim [u.a.] VCH 1989 XI, 479 S. zahlr. graph. Darst., Tab. txt rdacontent n rdamedia nc rdacarrier Literaturverz. S. 442 - 456 Chimie organométallique Composés organométalliques ram Organometallic chemistry Metallorganische Verbindungen (DE-588)4038906-6 gnd rswk-swf 1\p (DE-588)4123623-3 Lehrbuch gnd-content Metallorganische Verbindungen (DE-588)4038906-6 s DE-604 Salzer, Albrecht 1944- Verfasser (DE-588)13140069X aut HEBIS Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=001212984&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis 1\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk |
| spellingShingle | Elschenbroich, Christoph 1939- Salzer, Albrecht 1944- Organometallics a concise introduction Chimie organométallique Composés organométalliques ram Organometallic chemistry Metallorganische Verbindungen (DE-588)4038906-6 gnd |
| subject_GND | (DE-588)4038906-6 (DE-588)4123623-3 |
| title | Organometallics a concise introduction |
| title_alt | Organometallchemie |
| title_auth | Organometallics a concise introduction |
| title_exact_search | Organometallics a concise introduction |
| title_full | Organometallics a concise introduction Christoph Elschenbroich ; Albrecht Salzer |
| title_fullStr | Organometallics a concise introduction Christoph Elschenbroich ; Albrecht Salzer |
| title_full_unstemmed | Organometallics a concise introduction Christoph Elschenbroich ; Albrecht Salzer |
| title_short | Organometallics |
| title_sort | organometallics a concise introduction |
| title_sub | a concise introduction |
| topic | Chimie organométallique Composés organométalliques ram Organometallic chemistry Metallorganische Verbindungen (DE-588)4038906-6 gnd |
| topic_facet | Chimie organométallique Composés organométalliques Organometallic chemistry Metallorganische Verbindungen Lehrbuch |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=001212984&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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