Separation techniques in chemistry and biochemistry:
Gespeichert in:
| Format: | Tagungsbericht Buch |
|---|---|
| Sprache: | English |
| Veröffentlicht: |
New York
Dekker
1967
|
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | XVI, 415 S. Ill., zahlr. graph. Darst. |
Internformat
MARC
| LEADER | 00000nam a2200000 c 4500 | ||
|---|---|---|---|
| 001 | BV000978157 | ||
| 003 | DE-604 | ||
| 005 | 20131106 | ||
| 007 | t | ||
| 008 | 890315s1967 ad|| |||| 10||| eng d | ||
| 035 | |a (OCoLC)258798 | ||
| 035 | |a (DE-599)BVBBV000978157 | ||
| 040 | |a DE-604 |b ger |e rakwb | ||
| 041 | 0 | |a eng | |
| 049 | |a DE-19 |a DE-M49 | ||
| 050 | 0 | |a QD63.S4 | |
| 082 | 0 | |a 543 | |
| 084 | |a CHE 216f |2 stub | ||
| 245 | 1 | 0 | |a Separation techniques in chemistry and biochemistry |c [Nineteenth Annual Summer Symposium on Analytical Chemistry ... Edmonton, Alberta, Canada, in June, 1966]. Ed. by Roy A. Keller |
| 264 | 1 | |a New York |b Dekker |c 1967 | |
| 300 | |a XVI, 415 S. |b Ill., zahlr. graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 650 | 7 | |a Biomoleculen |2 gtt | |
| 650 | 7 | |a Chromatografie |2 gtt | |
| 650 | 7 | |a Elektroforese |2 gtt | |
| 650 | 7 | |a Scheidingstechnieken |2 gtt | |
| 650 | 4 | |a Séparation (Technologie) | |
| 650 | 4 | |a Chemistry Techniques, Analytical |v Congresses | |
| 650 | 4 | |a Chromatography |v Congresses | |
| 650 | 4 | |a Separation (Technology) | |
| 650 | 0 | 7 | |a Trennverfahren |0 (DE-588)4078395-9 |2 gnd |9 rswk-swf |
| 655 | 7 | |0 (DE-588)1071861417 |a Konferenzschrift |2 gnd-content | |
| 689 | 0 | 0 | |a Trennverfahren |0 (DE-588)4078395-9 |D s |
| 689 | 0 | |5 DE-604 | |
| 700 | 1 | |a Keller, Roy A. |e Sonstige |4 oth | |
| 711 | 2 | |a Summer Symposium on Analytical Chemistry |n 19 |d 1966 |c Edmonton, Alberta |j Sonstige |0 (DE-588)3056846-8 |4 oth | |
| 856 | 4 | 2 | |m HEBIS Datenaustausch |q application/pdf |u http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=000593715&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |3 Inhaltsverzeichnis |
| 999 | |a oai:aleph.bib-bvb.de:BVB01-000593715 | ||
Datensatz im Suchindex
| _version_ | 1804115403987746816 |
|---|---|
| adam_text | SEPARATION TECHNIQUES
IN CHEMISTRY AND BIOCHEMISTRY
edited by
ROY A KELLER
DEPARTMENT OF CHEMISTHY
UNIVERSITY OF ARIZONA
TUCSON, ARIZONA
MARCEL DEKKER, INC , NLYV YORK
CONTENTS
PREFACE V
CONTRIBUTORS vii
SEPARATION, IDENTIFICATION, AND ESTIMATION
OF HUMAN STEROID HORMONES AND THEIR ME
TABOLITES: APPLICATIONS TO ADRENOCORTICAL
STEROIDS 1
E C Horning, CJW Brooks, L Johnson, and W L
Gardiner
Summary 1
Separation Procedure 2
Identification Methods 9
Quantification 10
Acknowledgment 18
References 18
QUANTITATIVE ANALYSIS OF THE TWENTY NAT
URAL PROTEIN AMINO ACIDS BY GAS-LIQUID
CHROMATOGRAPHY 21
Charles W Gehrke and David L Stalling
Summary 21
Experimental Method 25
Results and Discussion 43
Summary and Conclusions 55
Acknowledgments 57
References 57
CONTINUOUS PARTICLE ELECTROPHORESIS: A
NEW ANALYTICAL AND PREPARATIVE CAPABILITY 59
Allen Strickier
Summary 59
Description 61
xi
xii CONTENTS
Performance Considerations 65
Electrophoretic Mobility Measurement 77
Acknowledgment 78
References 78
A CRITICAL EVALUATION OF GEL
CHROMATOGRAPHY 81
Robert L Pecsok and Dennis Saunders
Summary 81
Nature of the Gels 83
Proposed Mechanisms of the Separation 83
References 95
A COMPARISON OF MOBILE-PHASE PEAK DISPER
SION IN GAS AND LIQUID CHROMATOGRAPHY 97
D S Home, J H Knox, and Lilian McLaren
Summary 97
The Mechanism of Radial Dispersion 103
Longitudinal Dispersion 105
Experimental 107
Results 109
Discussion 116
Acknowledgment _ 119
Nomenclature 119
References 120
ULTRA-HIGH-PRESSURE GAS CHROMATOGRAPHY IN
MICRO COLUMNS TO 2000 ATMOSPHERES 121
Marcus N Myers and J Calvin Giddings
Summary 121
Relevant Properties of the High-Pressure Gases Used 123
Experimental 126
Results and Discussion 128
Acknowledgment 136
References 136
CONTENTS xiii
STRUCTURAL EFFECTS AND PROPERTIES OF OLI
GOMERS OF INTEREST IN SEPARATIONS 137
Hartland H Schmidt, Ronald K Clark, and Charles F Gay
Summary 137
Experimental Results 138
Combinatorial Entropy of Mixing 140
Regular Solution Models - 143
Corresponding-States Models 145
Discussion 148
References 150
INDETERMINATE ERRORS IN THE MEASUREMENT
OF CHROMATOGRAPHIC PEAKS 153
D L Ball, W E Harris, and H W Hab _ ood
Summary 153
Height-Width Method 155
Perimeter Methods 165
Acknowledgments 170
References 171
CRITERIA OF IDENTITY AND PURITY IN
CHROMATOGRAPHIC SEPARATIONS 173
Peter D Klein
Summary 173
System-Description Parameters and Their Measurement 175
Chromatographic Criteria of Purity and Identity 178
Capabilities and Limitations of Present Systems 187
Discussion 190
References 191
NONLINEAR DISTRIBUTION COEFFICIENTS IN GAS
CHROMATOGRAPHY 193
Paul Urone, Jon F Parcher, and Edward N Baylor
Summary 193
Apparatus and Procedure 194
Acknowledgments 209
References 210
xiv CONTENTS
EFFECT OF CARBON NUMBER, PHASE POLARITY,
TEMPERATURE, AND FLOW RATE ON PREPARATIVE
SCALE GAS-CHROMATOGRAPHIC SEPARATIONS OF
SATURATED METHYL ESTERS 211
Arthur Rose, D J Royer, and Robert S llenly
Summary 211
Nomenclature 213
Experimental 213
Results 214
Discussion 225
Acknowledgment 226
References 226
SUPPORT-COATED OPEN TUBULAR COLUMNS, V
COLUMNS WITH VARIOUS LIQUID-PHASE LOADINGS 229
L S Ettre,J E Purcell, and K Billeb
Summary 229
Experimental 230
Results and Discussions 233
Comparison with Theoretical Efficiency Values 244
Comparison with Results Obtained on Packed Columns 246
Columns with Very Low Liquid-Phase Loading 249
Conclusions 252
Acknowledgment 254
References 254
GAS-CHROMATOGRAPHIC BEHAVIOR OF
PRETREATED SILICA GELS 255
E K Hurley, M F Burke, J E Heveran, and L B Rogers
Summary 255
Experimental 256
Results and Discussion 258
Acknowledgments 262
References 262
INTRODUCTION OF GAS-CHROMAT( iGRAPHIC
SAMPLES TO A MASS SPECTROMETER 263
W H McFadden
Summary 263
CONTENTS xv
Introduction of Collected Samples 267
Direct Coupling of Mass Spectrometer and Gas Cinematograph ^ 272
References 282
OBSERVED PLATE HEIGHT IN TLC 287
George H Stewart
Summary 287
Theory 288
Experimental 292
Results and Discussion 292
Conclusions 299
Acknowledgments 299
References 300
THIN-LAYER CHROMATOGRAPHY OF THE N-SUBSTI-
TUTED MALEIMIDES ON ALUMINA: STEREOCHEM
ICAL FACTORS 301
John V Dichiaro, Roger A Bate, and Rot] A Keller
Summary 301
Experimental 309
Results and Discussion 315
Acknowledgments 328
References 328
AN AUTOMATED SYSTEM FOR SAMPLE COLLECTION
AND COMPUTER ANALYSIS OF THIN-LAYER RADIO-
CHROMATOGRAMS 331
Fred Snyder and Donna Smith
Summary 331
Experimental 332
Results and Discussion 339
Acknowledgments 344
References 344
QUANTITATIVE ANALYSIS BY LIQUID
CHROMATOGRAPHY 345
Arthur Karmen
Summary 345
xvi CONTENTS
Experimental 346
Results 348
Discussion 353
References 355
ADDUCT FORMATION WITH METAL CHELATES IN
VOLVED IN LIQUID—LIQUID EXTRACTION 357
Quintus Fernando
Summary 357
Acknowledgment 375
References 375
STUDIES IN SOLVENT SUBLATION: EXTRACTION OF
METHYL ORANGE AND RHODAMINE B 377
Barry L Karger, Alegria B Caragay, and Sandra B Lee
Summary 377
Experimental 379
Results and Discussion 382
Conclusion 400
References 401
Author Index 403
Subject Index 413
|
| any_adam_object | 1 |
| building | Verbundindex |
| bvnumber | BV000978157 |
| callnumber-first | Q - Science |
| callnumber-label | QD63 |
| callnumber-raw | QD63.S4 |
| callnumber-search | QD63.S4 |
| callnumber-sort | QD 263 S4 |
| callnumber-subject | QD - Chemistry |
| classification_tum | CHE 216f |
| ctrlnum | (OCoLC)258798 (DE-599)BVBBV000978157 |
| dewey-full | 543 |
| dewey-hundreds | 500 - Natural sciences and mathematics |
| dewey-ones | 543 - Analytical chemistry |
| dewey-raw | 543 |
| dewey-search | 543 |
| dewey-sort | 3543 |
| dewey-tens | 540 - Chemistry and allied sciences |
| discipline | Chemie / Pharmazie Chemie |
| format | Conference Proceeding Book |
| fullrecord | <?xml version="1.0" encoding="UTF-8"?><collection xmlns="http://www.loc.gov/MARC21/slim"><record><leader>01783nam a2200445 c 4500</leader><controlfield tag="001">BV000978157</controlfield><controlfield tag="003">DE-604</controlfield><controlfield tag="005">20131106 </controlfield><controlfield tag="007">t</controlfield><controlfield tag="008">890315s1967 ad|| |||| 10||| eng d</controlfield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(OCoLC)258798</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-599)BVBBV000978157</subfield></datafield><datafield tag="040" ind1=" " ind2=" "><subfield code="a">DE-604</subfield><subfield code="b">ger</subfield><subfield code="e">rakwb</subfield></datafield><datafield tag="041" ind1="0" ind2=" "><subfield code="a">eng</subfield></datafield><datafield tag="049" ind1=" " ind2=" "><subfield code="a">DE-19</subfield><subfield code="a">DE-M49</subfield></datafield><datafield tag="050" ind1=" " ind2="0"><subfield code="a">QD63.S4</subfield></datafield><datafield tag="082" ind1="0" ind2=" "><subfield code="a">543</subfield></datafield><datafield tag="084" ind1=" " ind2=" "><subfield code="a">CHE 216f</subfield><subfield code="2">stub</subfield></datafield><datafield tag="245" ind1="1" ind2="0"><subfield code="a">Separation techniques in chemistry and biochemistry</subfield><subfield code="c">[Nineteenth Annual Summer Symposium on Analytical Chemistry ... Edmonton, Alberta, Canada, in June, 1966]. Ed. by Roy A. Keller</subfield></datafield><datafield tag="264" ind1=" " ind2="1"><subfield code="a">New York</subfield><subfield code="b">Dekker</subfield><subfield code="c">1967</subfield></datafield><datafield tag="300" ind1=" " ind2=" "><subfield code="a">XVI, 415 S.</subfield><subfield code="b">Ill., zahlr. graph. Darst.</subfield></datafield><datafield tag="336" ind1=" " ind2=" "><subfield code="b">txt</subfield><subfield code="2">rdacontent</subfield></datafield><datafield tag="337" ind1=" " ind2=" "><subfield code="b">n</subfield><subfield code="2">rdamedia</subfield></datafield><datafield tag="338" ind1=" " ind2=" "><subfield code="b">nc</subfield><subfield code="2">rdacarrier</subfield></datafield><datafield tag="650" ind1=" " ind2="7"><subfield code="a">Biomoleculen</subfield><subfield code="2">gtt</subfield></datafield><datafield tag="650" ind1=" " ind2="7"><subfield code="a">Chromatografie</subfield><subfield code="2">gtt</subfield></datafield><datafield tag="650" ind1=" " ind2="7"><subfield code="a">Elektroforese</subfield><subfield code="2">gtt</subfield></datafield><datafield tag="650" ind1=" " ind2="7"><subfield code="a">Scheidingstechnieken</subfield><subfield code="2">gtt</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Séparation (Technologie)</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Chemistry Techniques, Analytical</subfield><subfield code="v">Congresses</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Chromatography</subfield><subfield code="v">Congresses</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Separation (Technology)</subfield></datafield><datafield tag="650" ind1="0" ind2="7"><subfield code="a">Trennverfahren</subfield><subfield code="0">(DE-588)4078395-9</subfield><subfield code="2">gnd</subfield><subfield code="9">rswk-swf</subfield></datafield><datafield tag="655" ind1=" " ind2="7"><subfield code="0">(DE-588)1071861417</subfield><subfield code="a">Konferenzschrift</subfield><subfield code="2">gnd-content</subfield></datafield><datafield tag="689" ind1="0" ind2="0"><subfield code="a">Trennverfahren</subfield><subfield code="0">(DE-588)4078395-9</subfield><subfield code="D">s</subfield></datafield><datafield tag="689" ind1="0" ind2=" "><subfield code="5">DE-604</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Keller, Roy A.</subfield><subfield code="e">Sonstige</subfield><subfield code="4">oth</subfield></datafield><datafield tag="711" ind1="2" ind2=" "><subfield code="a">Summer Symposium on Analytical Chemistry</subfield><subfield code="n">19</subfield><subfield code="d">1966</subfield><subfield code="c">Edmonton, Alberta</subfield><subfield code="j">Sonstige</subfield><subfield code="0">(DE-588)3056846-8</subfield><subfield code="4">oth</subfield></datafield><datafield tag="856" ind1="4" ind2="2"><subfield code="m">HEBIS Datenaustausch</subfield><subfield code="q">application/pdf</subfield><subfield code="u">http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=000593715&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA</subfield><subfield code="3">Inhaltsverzeichnis</subfield></datafield><datafield tag="999" ind1=" " ind2=" "><subfield code="a">oai:aleph.bib-bvb.de:BVB01-000593715</subfield></datafield></record></collection> |
| genre | (DE-588)1071861417 Konferenzschrift gnd-content |
| genre_facet | Konferenzschrift |
| id | DE-604.BV000978157 |
| illustrated | Illustrated |
| indexdate | 2024-07-09T15:22:04Z |
| institution | BVB |
| institution_GND | (DE-588)3056846-8 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-000593715 |
| oclc_num | 258798 |
| open_access_boolean | |
| owner | DE-19 DE-BY-UBM DE-M49 DE-BY-TUM |
| owner_facet | DE-19 DE-BY-UBM DE-M49 DE-BY-TUM |
| physical | XVI, 415 S. Ill., zahlr. graph. Darst. |
| publishDate | 1967 |
| publishDateSearch | 1967 |
| publishDateSort | 1967 |
| publisher | Dekker |
| record_format | marc |
| spelling | Separation techniques in chemistry and biochemistry [Nineteenth Annual Summer Symposium on Analytical Chemistry ... Edmonton, Alberta, Canada, in June, 1966]. Ed. by Roy A. Keller New York Dekker 1967 XVI, 415 S. Ill., zahlr. graph. Darst. txt rdacontent n rdamedia nc rdacarrier Biomoleculen gtt Chromatografie gtt Elektroforese gtt Scheidingstechnieken gtt Séparation (Technologie) Chemistry Techniques, Analytical Congresses Chromatography Congresses Separation (Technology) Trennverfahren (DE-588)4078395-9 gnd rswk-swf (DE-588)1071861417 Konferenzschrift gnd-content Trennverfahren (DE-588)4078395-9 s DE-604 Keller, Roy A. Sonstige oth Summer Symposium on Analytical Chemistry 19 1966 Edmonton, Alberta Sonstige (DE-588)3056846-8 oth HEBIS Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=000593715&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Separation techniques in chemistry and biochemistry Biomoleculen gtt Chromatografie gtt Elektroforese gtt Scheidingstechnieken gtt Séparation (Technologie) Chemistry Techniques, Analytical Congresses Chromatography Congresses Separation (Technology) Trennverfahren (DE-588)4078395-9 gnd |
| subject_GND | (DE-588)4078395-9 (DE-588)1071861417 |
| title | Separation techniques in chemistry and biochemistry |
| title_auth | Separation techniques in chemistry and biochemistry |
| title_exact_search | Separation techniques in chemistry and biochemistry |
| title_full | Separation techniques in chemistry and biochemistry [Nineteenth Annual Summer Symposium on Analytical Chemistry ... Edmonton, Alberta, Canada, in June, 1966]. Ed. by Roy A. Keller |
| title_fullStr | Separation techniques in chemistry and biochemistry [Nineteenth Annual Summer Symposium on Analytical Chemistry ... Edmonton, Alberta, Canada, in June, 1966]. Ed. by Roy A. Keller |
| title_full_unstemmed | Separation techniques in chemistry and biochemistry [Nineteenth Annual Summer Symposium on Analytical Chemistry ... Edmonton, Alberta, Canada, in June, 1966]. Ed. by Roy A. Keller |
| title_short | Separation techniques in chemistry and biochemistry |
| title_sort | separation techniques in chemistry and biochemistry |
| topic | Biomoleculen gtt Chromatografie gtt Elektroforese gtt Scheidingstechnieken gtt Séparation (Technologie) Chemistry Techniques, Analytical Congresses Chromatography Congresses Separation (Technology) Trennverfahren (DE-588)4078395-9 gnd |
| topic_facet | Biomoleculen Chromatografie Elektroforese Scheidingstechnieken Séparation (Technologie) Chemistry Techniques, Analytical Congresses Chromatography Congresses Separation (Technology) Trennverfahren Konferenzschrift |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=000593715&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT kellerroya separationtechniquesinchemistryandbiochemistry AT summersymposiumonanalyticalchemistryedmontonalberta separationtechniquesinchemistryandbiochemistry |