Quantitative analysis by gas chromatography:
Saved in:
| Main Author: | |
|---|---|
| Format: | Book |
| Language: | English |
| Published: |
New York u.a.
Dekker
1988
|
| Edition: | 2. ed., rev. and expanded |
| Series: | Chromatographic science
41 |
| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Physical Description: | XI, 277 S. |
| ISBN: | 0824778189 |
Staff View
MARC
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| 100 | 1 | |a Novák, Josef |e Verfasser |4 aut | |
| 245 | 1 | 0 | |a Quantitative analysis by gas chromatography |c Josef Novák |
| 250 | |a 2. ed., rev. and expanded | ||
| 264 | 1 | |a New York u.a. |b Dekker |c 1988 | |
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| 650 | 4 | |a Chemistry, Analytic |x Quantitative | |
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Record in the Search Index
| DE-BY-862_location | 2801 |
|---|---|
| DE-BY-FWS_call_number | 2801/1991:7722 |
| DE-BY-FWS_katkey | 30191 |
| DE-BY-FWS_media_number | 083100638716 |
| _version_ | 1824555270629490688 |
| adam_text | Quantitative Analysis by
Gas Chromatography
Second Edition
Revised and Expanded
Josef Novak
Institute of Analytical Chemistry
Czechoslovak Academy of Sciences
Brno Czechoslovakia
with a contribution by _** • • ••
PietA Leclercq-
Eindhoven University of Technology
Eindhoven, The Netherlands
t
MARCEL DEKKER, INC New York and Basel
Contents
Preface to the Second Edition iii
Preface to the First Edition v
1 INTRODUCTION 1
2 CONCENTRATION OF THE ANALYTE IN THE MOBILE
PHASE WITHIN THE CHROMATOGRAPHIC ZONE 5
I Amount of the Anaiyte in the Mobile Phase
within the Chromatographic Zone 5
II Volume of the Mobile Phase within the
Chromatographic Zone 6
III Mean and Peak-Maximum Concentrations of the
Anaiyte in the Mobile Phase within the
Chromatographic Zone 10
3 CHROMATOGRAPHIC DETECTORS 15
I Basic Concepts 15
II Traditional Classification of Chromatographic
Detectors 18
III Specification of Model Types of ^Detectors 23
IV General Classification of Chromatographic
Detectors 31
IX
x
t Contents
4 RELATIONS BETWEEN THE PEAK SIZE AND THE
AMOUNT OF ANALYTE CHROMATOGRAPHED 43
I Specification of the Problem 43
II Linearity of the Detector Response 44
III Relations Between the Integral of Detector
Response and the Total Amount of Anaiyte
Having Passed Through the Detector 50
IV Relations Between the Peak Height and the
Total Amount of Anaiyte Having Passed
Through the Detector 52
V Effect of an Auxiliary Stream of Fluid Added
to the Column Effluent 53
VI Detector Response Factors 57
VII Effect of Admixtures in the Mobile Phase on
the Detection of Analytes 62
5 SENSITIVITY OF CHROMATOGRAPHIC ANALYSIS 67
I Sensitivity of Detection 68
II Sensitivity of the Chromatographic Determina-
tion of Mass of Anaiyte 68
III Role of Extracolumn Broadening of the
Chromatographic Zone 71
IV Detectability and Determinability Limits 73
V Sensitivity of Analysis at Resolution-
Normalized Conditions 75
6 METHODS OF CALIBRATION 79
I Analysis of the Problem 79
II Presentation of Concentration 82
III Survey of Calibration Methods 85
IV Diluting of the Sample 106
V Determination of Detector Response Factors 111
7 MANUAL PROCESSING OF CHROMATOGRAMS 135
I Methods of Peak-Area Determination 135
II Analytical Significance and Interpretation of
the Peak Height 139
III Reliability of Results Obtained by Conven-
tional Calibration Methods 142
Contents xi
8 AUTOMATIC ACQUISITION AND HANDLING OF
CHROMATOGRAPHIC DATA 163
Piet A Leclercq
I Introduction 163
II Analog Signal Processing 166
III Digital Electronic Integrators 175
IV Digital Computers 183
V Conclusions 212
9 QUANTITATION IN TRACE ANALYSIS 215
I Concepts and Definitions of Trace Analysis 216
II Sample-Enrichment Procedures 217
III Headspace-Gas Analysis 222
IV Extraction of Liquid Sample with Liquid
Extrahent 235
References 257
Glossary ~ 267
Index 271
|
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| dewey-sort | 3545 3896 |
| dewey-tens | 540 - Chemistry and allied sciences |
| discipline | Chemie / Pharmazie Chemie |
| edition | 2. ed., rev. and expanded |
| format | Book |
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| id | DE-604.BV000783802 |
| illustrated | Not Illustrated |
| indexdate | 2025-02-20T07:05:00Z |
| institution | BVB |
| isbn | 0824778189 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-000490870 |
| oclc_num | 16901099 |
| open_access_boolean | |
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| owner_facet | DE-12 DE-91 DE-BY-TUM DE-355 DE-BY-UBR DE-703 DE-862 DE-BY-FWS DE-83 DE-11 |
| physical | XI, 277 S. |
| publishDate | 1988 |
| publishDateSearch | 1988 |
| publishDateSort | 1988 |
| publisher | Dekker |
| record_format | marc |
| series | Chromatographic science |
| series2 | Chromatographic science |
| spellingShingle | Novák, Josef Quantitative analysis by gas chromatography Chromatographic science Chromatographie Chromatographie en phase gazeuse Chemistry, Analytic Quantitative Gas chromatography Quantitative Analyse (DE-588)4125311-5 gnd Gaschromatographie (DE-588)4019330-5 gnd |
| subject_GND | (DE-588)4125311-5 (DE-588)4019330-5 |
| title | Quantitative analysis by gas chromatography |
| title_auth | Quantitative analysis by gas chromatography |
| title_exact_search | Quantitative analysis by gas chromatography |
| title_full | Quantitative analysis by gas chromatography Josef Novák |
| title_fullStr | Quantitative analysis by gas chromatography Josef Novák |
| title_full_unstemmed | Quantitative analysis by gas chromatography Josef Novák |
| title_short | Quantitative analysis by gas chromatography |
| title_sort | quantitative analysis by gas chromatography |
| topic | Chromatographie Chromatographie en phase gazeuse Chemistry, Analytic Quantitative Gas chromatography Quantitative Analyse (DE-588)4125311-5 gnd Gaschromatographie (DE-588)4019330-5 gnd |
| topic_facet | Chromatographie Chromatographie en phase gazeuse Chemistry, Analytic Quantitative Gas chromatography Quantitative Analyse Gaschromatographie |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=000490870&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| volume_link | (DE-604)BV000003251 |
| work_keys_str_mv | AT novakjosef quantitativeanalysisbygaschromatography |
Indexes
THWS Schweinfurt Magazin
| Call Number: |
2801 1991:7722 |
|---|---|
| Copy 1 | bestellbar aus dem Magazin Available Place a Hold |