Modern methods in the analysis and structural elucidation of mycotoxins:
Saved in:
| Format: | Book |
|---|---|
| Language: | English |
| Published: |
Orlando u.a.
Acad. Pr.
1986
|
| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Physical Description: | XII, 471 S. |
| ISBN: | 0121795152 |
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| 245 | 1 | 0 | |a Modern methods in the analysis and structural elucidation of mycotoxins |c ed. by Richard J. Cole |
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| adam_text | IMAGE 1
MODERN METHODS
IN THE ANALYSIS AND STRUCTURAL ELUCIDATION OF MYCOTOXINS
EDITED BY RICHARD J. COLE
U. S. DEPARTMENT OF AGRICULTURE AGRICULTURAL RESEARCH SERVICE NATIONAL
PEANUT RESEARCH LABORATORY DAWSON, GEORGIA
1986
ACADEMIC PRESS, INC.
HARCOURT BRACE JOVANOVICH, PUBLISHERS ORLANDO SAN DIEGO NEW YORK AUSTIN
BOSTON LONDON SYDNEY TOKYO TORONTO
IMAGE 2
CONTENTS
PREFACE XI
1 BIOLOGICAL SCREENING METHODS FOR MYCOTOXINS AND TOXIGENIC FUNGI
RICHARD J. COLE, HORACE C. CUTLER, AND JOE W. DORNER
I. INTRODUCTION 1
II. ANIMAL ASSAYS 3
III. PLANT ASSAYS 10
IV. MICROBIOLOGICAL ASSAYS 17
V. CONCLUSION .- 22
REFERENCES 23
2 SAMPLING AND SAMPLE PREPARATION METHODS FOR MYCOTOXIN ANALYSIS
J. W. DICKENS AND T. B. WHITAKER
I. INTRODUCTION 29
II. DISTRIBUTION OF MYCOTOXINS WITHIN THE PRODUCT 31
III. SOURCES OF ERROR IN MYCOTOXIN TESTS 32
V
IMAGE 3
VI CONTENTS
IV. ERROR REDUCTION 36
V. SAMPLING PROCEDURES 37
VI. SUBSAMPLING PROCEDURES 41
VII. PRESERVATION OF SAMPLES 44
VIII. SURVEY STUDIES 44
IX. QUALITY CONTROL 45
X. EXPERIMENTATION ^ 46
REFERENCES 47
3 CHEMICAL SURVEY METHODS FOR MYCOTOXINS
ODETTE L. SHOTWELL
I. INTRODUCTION 52
II. AFLATOXINS ,. 53
HI. ZEARALENONE , 70
IV. TRICHOTHECENES 74
V. OCHRATOXINS 80
VI. STERIGMATOCYSTIN 83
VII. CONCLUSION AND FUTURE DEVELOPMENTS 86
REFERENCES 87
APPLICATION OF ULTRAVIOLET AND INFRARED SPECTROSCOPY IN THE ANALYSIS AND
STRUCTURAL ELUCIDATION OF MYCOTOXINS
CHARLES P. GORST-ALLMAN
I. INTRODUCTION 95
II. INFRARED SPECTROSCOPY 96
III. ULTRAVIOLET SPECTROSCOPY 110
IV. CONCLUSION 117
REFERENCES 117
5 APPLICATION OF NUCLEAR MAGNETIC RESONANCE TO STRUCTURAL ELUCIDATION OF
MYCOTOXINS
RICHARD H. COX
I. INTRODUCTION 124
II. STRATEGIES IN STRUCTURAL DETERMINATION 126
III. ONE-DIMENSIONAL METHODS 127
IMAGE 4
CONTENTS VII
IV. SPECTRAL EDITING IN 13 C NMR SPECTRA 136
V. TWO-DIMENSIONAL METHODS 143
VI. CARBON-CARBON CONNECTIVITY 150
VII. BIOSYNTHETIC STUDIES 157
REFERENCES 159
X-RAY CRYSTALLOGRAPHY AS A TOOL FOR IDENTIFYING NEW MYCOTOXINS
JAMES P. SPRINGER
I. INTRODUCTION 163
II. HISTORY AND DESCRIPTION OF THE SINGLE-CRYSTAL X-RAY DIFFRACTION
EXPERIMENT 164
III. ADVANTAGES AND LIMITATIONS OF USING X-RAY DIFFRACTION .. 166 IV.
X-RAY DIFFRACTION OF MYCOTOXINS 168
V. CONCLUSIONS 173
REFERENCES 174
7 APPLICATION OF BIOSYNTHETIC TECHNIQUES IN THE STRUCTURAL STUDIES OF
MYCOTOXINS
PIETER S. STEYN AND ROBERT VLEGGAAR
I. INTRODUCTION 177
II. TECHNIQUES 178
III. BIOSYNTHESIS OF POLYKETIDES 181
IV. AMINO ACIDS IN THE BIOSYNTHESIS OF MYCOTOXINS 195 REFERENCES 203
8 IMMUNOASSAYS FOR MYCOTOXINS
F. S. CHU
I. INTRODUCTION 207
II. PRODUCTION OF ANTIBODY AGAINST MYCOTOXINS 209
III. CHARACTERIZATION OF ANTIBODY 213
IV. RADIOIMMUNOASSAY* FOR MYCOTOXINS 220
V. ENZYME-LINKED IMMUNOSORBENT ASSAY FOR MYCOTOXINS . .. 223 VI.
IMMUNOHISTOCHEMICAL METHODS AND OTHER STUDIES 229 VII. CONCLUDING
REMARKS 233
REFERENCES 233
IMAGE 5
VLLL CONTENTS
9 THIN-LAYER CHROMATOGRAPHY/HIGH-PERFORMANCE
THIN-LAYER CHROMATOGRAPHY AS A TOOL FOR MYCOTOXIN DETERMINATION
STANLEY NESHEIM AND MARY W. TRUCKSESS
I. INTRODUCTION 240
II. THIN-LAYER CHROMATOGRAPHIC PROCEDURES FOR MYCOTOXINS . 241 III.
ANALYSIS OF INDIVIDUAL MYCOTOXINS 252
IV. CONCLUSIONS 259
REFERENCES 260
10 GAS CHROMATOGRAPHY IN MYCOTOXIN ANALYSIS
RODNEY W. BEAVER
I. INTRODUCTION . 265
II. PRACTICAL ASPECTS OF GAS CHROMATOGRAPHY 266
III. USE OF GAS CHROMATOGRAPHY IN THE ANALYSIS OF MYCOTOXINS 276
REFERENCES 289
11 HIGH-PERFORMANCE LIQUID CHROMATOGRAPHY AND ITS APPLICATION TO THE
ANALYSIS OF MYCOTOXINS
MARTIN J. SHEPHERD
I. INTRODUCTION 294
II. HIGH-PERFORMANCE LIQUID CHROMATOGRAPHIC INSTRUMENTATION AND
METHODOLOGY 296
III. MANIPULATION OF HIGH-PERFORMANCE LIQUID CHROMATOGRAPHIC CONDITIONS
313
IV. HIGH-PERFORMANCE LIQUID CHROMATOGRAPHY: A LITERATURE REVIEW 319
V. CONCLUSIONS 329
REFERENCES 330
12 GAS CHROMATOGRAPHIC-MASS SPECTROMETRIC ANALYSIS OF MYCOTOXINS T
RONALD F. VESONDER AND WILLIAM K. ROHWEDDER
I. INTRODUCTION 335
II. HISTORY AND INSTRUMENTATION 336
III. COMPARISON OF MASS SPECTROMETRY TECHNIQUES 338
IMAGE 6
CONTENTS IX
IV. QUANTITATIVE ANALYSIS 339
V. MYCOTOXINS 340
VI. CONCLUSIONS 348
REFERENCES 349
13 MASS SPECTRA OF SELECTED TRICHOTHECENES
C. J. MIROCHA, S. V. PATHRE, R. J. PAWLOSKY, AND D. W. HEWETSON
I. INTRODUCTION 354
II. APPLICATION TO SELECTED TRICHOTHECENE MYCOTOXINS 355 III. ANALYSIS
OF A MIXTURE OF TRICHOTHECENES BY GAS CHROMATOGRAPHY AND IDENTIFICATION
OF SOME OF THE COMPONENTS BY SEARCHING A COMPUTER LIBRARY OF POSITIVE
CHEMICAL IONIZATION SPECTRA 388
IV. CONCLUSIONS . 390
REFERENCES 392
14 MASS SPECTROMETRY-MASS SPECTROMETRY AS A TOOL FOR MYCOTOXIN ANALYSIS
R. D. PLANNER
I. INTRODUCTION 393
II. MASS SPECTROMETRY-MASS SPECTROMETRY INSTRUMENTATION .. 395 III. MASS
SPECTROMETRY-MASS SPECTROMETRY TECHNIQUES AND EXPERIMENTS 398
IV. EXAMPLES OF MASS SPECTROMETRY-MASS SPECTROMETRY OF MYCOTOXINS 401
REFERENCES 413
15 TAXONOMIC APPROACHES TO MYCOTOXIN IDENTIFICATION (TAXONOMIC
INDICATION OF MYCOTOXIN CONTENT IN FOODS)
JENS C. FRISVAD
I. INTRODUCTION 415
II. FACTORS AFFECTING MYCOTOXIN PRODUCTION 416
III. MYCOLOGICAL EXAMINATION OF FOODS 417
IV. MYCOTOXINS AND FUNGAL TAXONOMY 420
V. IMPORTANT GENERA CONTAINING TOXIGENIC ISOLATES 422 REFERENCES 446
INDEX 459
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| physical | XII, 471 S. |
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| spelling | Modern methods in the analysis and structural elucidation of mycotoxins ed. by Richard J. Cole Orlando u.a. Acad. Pr. 1986 XII, 471 S. txt rdacontent n rdamedia nc rdacarrier Mycotoxines - Analyse Structure moléculaire Molecular structure Mycotoxins Analysis Mycotoxins analysis Mykotoxin (DE-588)4040984-3 gnd rswk-swf (DE-588)4143413-4 Aufsatzsammlung gnd-content Mykotoxin (DE-588)4040984-3 s DE-604 Cole, Richard J. Sonstige oth HEBIS Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=000378657&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
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| title | Modern methods in the analysis and structural elucidation of mycotoxins |
| title_auth | Modern methods in the analysis and structural elucidation of mycotoxins |
| title_exact_search | Modern methods in the analysis and structural elucidation of mycotoxins |
| title_full | Modern methods in the analysis and structural elucidation of mycotoxins ed. by Richard J. Cole |
| title_fullStr | Modern methods in the analysis and structural elucidation of mycotoxins ed. by Richard J. Cole |
| title_full_unstemmed | Modern methods in the analysis and structural elucidation of mycotoxins ed. by Richard J. Cole |
| title_short | Modern methods in the analysis and structural elucidation of mycotoxins |
| title_sort | modern methods in the analysis and structural elucidation of mycotoxins |
| topic | Mycotoxines - Analyse Structure moléculaire Molecular structure Mycotoxins Analysis Mycotoxins analysis Mykotoxin (DE-588)4040984-3 gnd |
| topic_facet | Mycotoxines - Analyse Structure moléculaire Molecular structure Mycotoxins Analysis Mycotoxins analysis Mykotoxin Aufsatzsammlung |
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