Electron magnetic resonance principles:
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| Main Authors: | , |
|---|---|
| Format: | Book |
| Language: | English |
| Published: |
Berlin ; Boston
De Gruyter
[2019]
Beijing Tsinghua University Press [2019] |
| Series: | De Gruyter Graduate
|
| Subjects: | |
| Online Access: | http://www.degruyter.com/search?f_0=isbnissn&q_0=9783110528008&searchTitles=true https://www.degruyter.com/doc/cover/9783110528008.jpg Inhaltsverzeichnis |
| Physical Description: | XIII, 450 Seiten Illustrationen, Diagramme 24 cm x 17 cm |
| ISBN: | 9783110528008 |
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| 084 | |a 540 |2 sdnb | ||
| 100 | 1 | |a Xu, Yuanzhi |d 1933- |e Verfasser |0 (DE-588)1193948819 |4 aut | |
| 245 | 1 | 0 | |a Electron magnetic resonance principles |c Yuanzhi Xu, Jia Yao |
| 264 | 1 | |a Berlin ; Boston |b De Gruyter |c [2019] | |
| 264 | 1 | |a Beijing |b Tsinghua University Press |c [2019] | |
| 264 | 4 | |c © 2019 | |
| 300 | |a XIII, 450 Seiten |b Illustrationen, Diagramme |c 24 cm x 17 cm | ||
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| 338 | |b nc |2 rdacarrier | ||
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| 700 | 1 | |a Yao, Jia |e Verfasser |0 (DE-588)1193948967 |4 aut | |
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| 776 | 0 | 8 | |i Erscheint auch als |n Online-Ausgabe, PDF |z 978-3-11-056857-8 |
| 776 | 0 | 8 | |i Erscheint auch als |n Online-Ausgabe, EPUB |z 978-3-11-062010-8 |
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| _version_ | 1804179507013222400 |
|---|---|
| adam_text | CONTENTS
FOREWORD
*
VII
AUTHOR
*
S
PREFACE
*
VIII
1
INTRODUCTION
*
1
1.1
ORIGIN
OF
EMR
*
1
1.2
EXPERIMENTAL
APPARATUS
*
3
1.2.1
MICROWAVE
SOURCE
*
4
1.2.2
RESONANT
CAVITY
AND
COUPLING
SYSTEM
*
5
1.2.3
MAGNET
*
10
1.2.4
DETECTION
SYSTEM
*
12
1.2.5
DATA
TREATMENT
SYSTEM
*
12
1.3
TARGET
OF
RESEARCH
*
13
1.4
PROSPECTS
FOR
FUTURE
*
13
REFERENCES
*
14
2
THEORETICAL
BASICS
*
16
2.1
PHENOMENAL
DESCRIPTION
OF
EMR
*
16
2.2
ANGULAR
MOMENTUM
AND
MAGNETIC
MOMENT
*
17
2.2.1
ORBITAL
MOTION
OF
ELECTRON
AND
ITS
MAGNETIC
MOMENT
*
17
2.2.2
EIGEN
MOTION
OF
ELECTRONS
AND
ITS
MAGNETIC
MOMENT
*
20
2.2.3
SPIN
ANGULAR
MOMENTUM
AND
MAGNETIC
MOMENT
OF
ATOMIC
NUCLEUS
*
23
2.2.4
ELECTRIC
QUADRUPOLE
MOMENT
OF
ATOMIC
NUCLEUS
*
25
2.3
UNIT
OF
MAGNETIC
FIELD
*
26
2.4
THE
INTERACTION
BETWEEN
EXTERNAL
FIELDS
AND
MAGNETIC
MOMENT
*
28
2.5
INTERACTION
OF
MAGNETIC
MOMENT
WITH
ELECTROMAGNETIC
FIELD
IN
THE
EXTERNAL
MAGNETIC
FIELD
*
30
2.6
INTERACTION
OF
NUCLEAR
MAGNETIC
MOMENT
WITH
ELECTRON
MAGNETIC
MOMENT
IN
THE
EXTERNAL
MAGNETIC
FIELD
*
33
REFERENCES
*
34
FURTHER
READING
*
34
3
G-TENSOR
THEORY
*
35
3.1
LANDS
FACTOR
*
35
3.2
MATRIX
PRESENTATION
OF
G-TENSOR
*
37
3.2.1
G-TENSOR
OF
COLOUR
CENTER
(CUBIC
SYMMETRY
AND
UNIAXIAL
SYMMETRY
SYSTEM)
*
37
3.2.2
THE
G-TENSOR
OF
NONAXISYMMETRIC
(LOWER
THAN
UNIAXIAL
SYMMETRY)
SYSTEM
*
39
X
*
CONTENTS
3.3
3.3.1
3.3.2
G-TENSOR
OF
IRREGULAR
ORIENTATION
SYSTEM
*
46
G-TENSOR
OF
AXISYMMETRIC
SYSTEM
*
46
G-TENSOR
OF
NONAXISYMMETRIC
SYSTEM
*
50
REFERENCES
*
52
FURTHER
READING
*
52
4
ISOTROPIC
HYPERFINE
STRUCTURE
*
53
4.1
THEORETICAL
EXPLORATION
OF
HYPERFINE
INTERACTION
*
53
4.1.1
DIPOLE-DIPOLE
INTERACTION
*
53
4.1.2
FERMI
CONTACT
INTERACTION
*
54
4.2
ENERGY
OPERATOR
OF
ISOTROPIC
HYPERFINE
INTERACTION
*
55
4.2.1
SPIN
OPERATOR
AND
HAMILTONIANS
-----
55
4.2.2
ZEEMAN
INTERACTION
OF
ELECTRONS
AND
NUCLEI
*
57
4.2.3
SPIN
HAMILTONIAN
OF
ISOTROPIC
HYPERFINE
INTERACTION
*
59
4.3
SPECTRAL
ISOTROPIC
HYPERFINE
STRUCTURE
*
60
4.3.1
SYSTEM
WITH
ONE
MAGNETIC
NUCLEUS
AND
ONE
UNPAIRED
ELECTRON
*
60
4.3.2
MULTIMAGNETIC
NUCLEI
WITH
ONE
UNPAIRED
ELECTRON
SYSTEM
*
65
4.3.3
HYPERFINE
SPLITTING
ARISING
FROM
OTHER
MAGNETIC
NUCLEI
*
71
4.3.4
ENCOUNTERED
PROBLEMS
IN
ISOTROPIC
RADICAL
SPECTRA
*
75
4.4
HYPERFINE
STRUCTURE
OF
ORGANIC
RR-FREE
RADICAL
SPECTRUM
*
76
4.4.1
HYPERFINE
COUPLING
CONSTANT
OF
ORGANIC
N-RADICAL
*
76
4.4.2
MCCONNELL
SEMIEMPIRICAL
FORMULA
*
76
4.4.3
HIICKEL
MOLECULAR
ORBITAL
(HMO)
THEORY
*
77
4.4.4
CALCULATION
OF
PROBABILITY
DENSITY
DISTRIBUTION
OF
UNPAIRED
ELECTRON
*
79
4.4.5
THE
Q
VALUE
OF
THE
RADICAL
WITH
FULLY
SYMMETRICAL
STRUCTURE
*
85
4.4.6
HYPERFINE
COUPLING
CONSTANT
A
VALUE
OF
THE
EVEN
ALTERNANT
HYDROCARBONS
*
86
4.4.7
HYPERFINE
COUPLING
CONSTANT
A
VALUE
OF
THE
EVEN
ALTERNANT
HETEROCYCLIC
HYDROCARBONS
*
89
4.4.8
HYPERFINE
COUPLING
CONSTANT
A
VALUE
OF
THE
ODD
ALTERNANT
AND
NONALTERNANT
HYDROCARBONS
*
90
4.5
MECHANISM
OF
HYPERFINE
SPLITTING
IN
THE
SPECTRUM
OF
CONJUGATED
SYSTEMS
*
91
4.5.1
*
ELECTRONIC
CORRELATION
*
EFFECT
*
91
4.5.2
THE
SIGN
OF
PROTON
HYPERFINE
SPLITTING
CONSTANT
*
93
4.5.3
NEGATIVE
SPIN
DENSITY
*
96
4.5.4
ABOUT
THE
Q
VALUE
PROBLEM
*
96
4.5.5
HYPERFINE
SPLITTING
AND
HYPERCONJUGATION
EFFECT
OF
METHYL
PROTONS
*
98
4.6
HYPERFINE
SPLITTING
OF
OTHER
(NON-PROTON)
NUCLEI
*
101
4.6.1
HYPERFINE
SPLITTING
OF
13
C
NUCLEUS
*
101
CONTENTS
*
XI
4.6.2
4.6.3
4.6.4
HYPERFINE
SPLITTING
OF
14
N
NUCLEUS
*
103
HYPERFINE
SPLITTING
OF
19
F
NUCLEUS
*
104
HYPERFINE
SPLITTINGS
OF
17
O
AND
33
S
NUCLEI
*
105
REFERENCES
*
105
FURTHER
READINGS
*
106
5
5.1
5.2
5.3
5.4
5.4.1
5.4.2
5.4.3
5.4.4
5.5
5.6
ANISOTROPIC
HYPERFINE
STRUCTURE
*
107
ANISOTROPIC
HYPERFINE
INTERACTION
*
107
MATRIX
INTERPRETATION
OF
ANISOTROPIC
HYPERFINE
INTERACTION
*
110
EXAMPLE
DEMONSTRATION
*
116
ANISOTROPIC
HYPERFINE
COUPLING
TENSOR
AND
STRUCTURE
OF
RADICAL
*
122
HYPERFINE
COUPLING
TENSOR
OF
CENTRAL
ATOM
*
122
HYPERFINE
COUPLING
TENSOR
OF
A-HYDROGEN
ATOM
*
127
HYPERFINE
COUPLING
TENSOR
OF
/3-HYDROGEN
ATOM
*
130
HYPERFINE
COUPLING
TENSOR
OF
O-TYPE
ORGANIC
RADICALS
*
132
ANISOTROPY
OF
THE
COMBINATION
OF
G-TENSOR
AND
A-TENSOR
*
133
ANISOTROPY
OF
A
TENSOR
IN
THE
IRREGULAR
ORIENTATION
SYSTEM
*
133
REFERENCES
*
135
FURTHER
READINGS
*
136
6
6.1
6.2
6.2.1
6.2.2
6.3
6.3.1
FINE
STRUCTURE
*
137
ZERO-FIELD
SPLITTING
*
138
SPIN
HAMILTONIAN
OF
TWO-ELECTRON
INTERACTION
*
140
EXCHANGE
INTERACTION
OF
ELECTRON
SPIN
*
140
DIPOLE
INTERACTION
OF
ELECTRON-ELECTRON
*
144
THE
TRIPLET
MOLECULE
(S
=
1)
SYSTEM
*
153
ENERGY
LEVELS
AND
WAVE
FUNCTIONS
OF
TRIPLET
MOLECULES
UNDER
THE
ACTION
OF
EXTERNAL
MAGNETIC
FIELD
*
153
6.3.2
6.3.3
6.3.4
6.3.5
6.4
6.5
EXAMPLES
OF
TRIPLET
STATE
EXCITED
BY
LIGHT
*
156
EXAMPLES
OF
THERMAL
EXCITATION
TRIPLET
STATE
*
157
EXAMPLES
OF
OTHER
EXCITED
TRIPLET
*
159
EXAMPLES
OF
GROUND
TRIPLET
STATE
*
159
TRIPLET
SYSTEM
OF
IRREGULAR
ORIENTATION
*
162
BIRADICAL
*
166
REFERENCES
*
169
FURTHER
READING
*
170
7
7.1
7.1.1
7.1.2
7.1.3
RELAXATION
AND
LINE
SHAPE
AND
LINEWIDTH
*
171
MODEL
OF
SPIN
RELAXATION
*
171
SPIN
TEMPERATURE
AND
BOLTZMANN
DISTRIBUTION
*
171
SPIN
PARTICLE
TRANSITION
DYNAMICS
*
173
MECHANISM
OF
THE
EFFECT
OF
RELAXATION
TIME
RJ
ON
LINEWIDTH
*
175
XII
*
CONTENTS
7.1.4
MAGNETIZATION
IN
STATIC
MAGNETIC
FIELD
*
177
7.1.5
BLOCH
EQUATION
IN
THE
STATIC
MAGNETIC
FIELD
*
178
7.1.6
BLOCH
EQUATION
IN
THE
STATIC
MAGNETIC
FIELD
COUPLED
WITH
THE
OSCILLATING
MAGNETIC
FIELD
*
180
7.1.7
STATIONARY
SOLUTIONS
OF
BLOCH
EQUATION
*
181
7.2
SHAPE,
WIDTH,
AND
INTENSITY
OF
SPECTRAL
LINE
*
182
7.2.1
LINE
SHAPE
FUNCTION
*
182
7.2.2
LINEWIDTH
*
186
7.2.3
LINE
BROADENING
*
188
7.2.4
LINE
INTENSITY
*
188
7.3
DYNAMIC
EFFECTS
OF
LINE
SHAPE
*
189
7.3.1
GENERALIZED
BLOCH
EQUATION
*
189
7.3.2
CHEMICAL
EXCHANGE
BROADENING
MECHANISM
*
193
7.3.3
MECHANISM
OF
THE
SPECTRAL
LINES
BROADENING
CAUSED
BY
PHYSICAL
MOTION
*
200
7.4
SATURATION
TRANSFER
OF
SPECTRA
*
214
7.5
INTENSITY
OF
SIGNAL
DEPENDENT
ON
TIME
*
214
7.5.1
FREE
RADICAL
CONCENTRATION
CHANGES
WITH
TIME
*
214
7.5.2
CHEMICAL-INDUCED
DYNAMIC
ELECTRON
POLARIZATION
(CIDER)
*
215
REFERENCES
*
217
FURTHER
READINGS
*
218
8
QUANTITATIVE
DETERMINATION
*
220
8.1
MAIN
FACTORS
OF
INFLUENCE
FOR
QUANTITATIVE
DETERMINATION
*
221
8.1.1
FACTORS
OF
INSTRUMENT
*
221
8.1.2
INFLUENCE
OF
OPERATING
FACTORS
*
228
8.2
SELECTION
AND
PREPARATION
OF
STANDARD
SAMPLES
*
235
8.3
KEY
PARAMETERS
AND
ITS
EFFECT
ON
THE
INTENSITY
OF
EMR
SIGNAL
*
237
8.4
ACHIEVABLE
ACCURACY
OF
QUANTITATIVE
DETERMINATION
*
239
REFERENCES
*
240
9
PARAMAGNETIC
GASES
AND
INORGANIC
RADICALS
*
242
9.1
SPECTRA
OF
PARAMAGNETIC
GASES
*
242
9.1.1
MONOATOMIC
PARAMAGNETIC
GASES
*
242
9.1.2
DIATOMIC
PARAMAGNETIC
GAS
*
245
9.1.3
GASEOUS
MOLECULES
OF
TRIATOM
AND
POLYATOM
*
256
9.2
EXPANDING
OF
EMR
TECHNIQUE
FOR
STUDY
ON
PARAMAGNETIC
GAS
*
257
9.2.1
LASER
ELECTRONIC
MAGNETIC
RESONANCE
*
257
9.2.2
MAGNETIC
RESONANCE
INDUCED
BY
ELECTRON
*
257
9.3
INORGANIC
RADICALS
*
258
9.4
POINT
DEFECTS
IN
SOLID
STATES
*
261
9.5
SPECTRA
OF
CONDUCTOR
AND
SEMICONDUCTOR
*
265
CONTENTS
*
XIII
9.6
STRUCTURE
OF
A
MOLECULE
STRUCTURE
OF
A
MOLECULE
ESTIMATED FROM
THE
DATA
OF
EMR
*
268
REFERENCES
*
269
FURTHER
READINGS
*
272
10
IONS
OF
TRANSITION
ELEMENTS
AND
THEIR
COMPLEXES
*
273
10.1
ELECTRON
GROUND
STATE
OF
TRANSITION
ELEMENT
ION
*
273
10.2
ORBITAL
DEGENERACY
IS
RESCINDED
IN
LIGAND
FIELD
*
275
10.3
ELECTRIC
POTENTIAL
OF
LIGAND
FIELD
*
278
10.4
ENERGY-LEVEL
SPLITTING
OF
TRANSITION
METAL
ION
IN
LIGAND
FIELD
*
282
10.4.1
P-
STATE
ION
IN
OCTAHEDRON
FIELD
(L
=
1)
*
282
10.4.2
D-STATE
ION
-----
283
10.4.3
ABOUT
F-STATE
ION
*
286
10.5
SPIN-ORBIT
COUPLING
AND
SPIN
HAMILTONIAN
*
288
10.6
GROUND-STATE
ION
WITH
ORBITAL
NONDEGENERACY
*
294
10.6.1
D-STATE
IONS
OF
GROUND-STATE
ORBITAL
NONDEGENERATE
*
295
10.6.2
F-STATE
IONS
OF
GROUND-STATE
ORBITAL
NONDEGENERATE
*
298
10.6.3
S-STATE
IONS
OF
THE
GROUND-STATE
ORBITAL
NONDEGENERATE
*
305
10.7
GROUND-STATE
IONS
WITH
ORBITAL
DEGENERACY
*
310
10.7.1
D-STATE
IONS
*
310
10.7.2
F-STATE
IONS
*
316
10.7.3
JAHN-TELLER
DISTORTION
*
320
10.7.4
THE
PALLADIUM
GROUP
(4D)
AND
PLATINUM
GROUP
(5D)
IONS
*
321
10.8
EMR
SPECTRA
OF
RARE
EARTH
IONS
*
321
10.8.1
LANTHANIDE
ION
*
321
10.8.2
ACTINIDE
IONS
*
323
10.9
EMR
SPECTRA
OF
TRANSITION
METAL
COMPLEXES
*
324
REFERENCES
*
325
FURTHER
READINGS
*
327
APPENDIX
1:
EXTENSION
AND
EXPANSION
OF
EMR
*
328
APPENDIX
2:
MATHEMATICAL
PREPARATION
*
399
APPENDIX
3:
ANGULAR
MOMENTUM
AND
STABLE-STATE
PERTURBATION
THEORY
IN
QUANTUM
MECHANICS
*
421
APPENDIX
4:
FUNDAMENTAL
CONSTANTS
AND
USEFUL
CONVERSION
ACTORS
*
442
APPENDIX
5:
THE
NATURAL
ABUNDANCE,
NUCLEAR
SPIN,
NUCLEAR
MAGNETOGYRIC
RATIO
OF
SOME
MAGNETIC
NUCLEI
AND
THEIR
HYPERFINE
COUPLING
PARAMETERS
*
445
INDEX
*
451
|
| any_adam_object | 1 |
| author | Xu, Yuanzhi 1933- Yao, Jia |
| author_GND | (DE-588)1193948819 (DE-588)1193948967 |
| author_facet | Xu, Yuanzhi 1933- Yao, Jia |
| author_role | aut aut |
| author_sort | Xu, Yuanzhi 1933- |
| author_variant | y x yx j y jy |
| building | Verbundindex |
| bvnumber | BV045540490 |
| classification_rvk | UM 3700 UP 9340 VG 9700 |
| classification_tum | CHE 248f |
| ctrlnum | (OCoLC)1113726466 (DE-599)DNB1156288606 |
| discipline | Chemie / Pharmazie Physik Chemie |
| format | Book |
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| id | DE-604.BV045540490 |
| illustrated | Illustrated |
| indexdate | 2024-07-10T08:20:57Z |
| institution | BVB |
| institution_GND | (DE-588)10095502-2 |
| isbn | 9783110528008 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-030924423 |
| oclc_num | 1113726466 |
| open_access_boolean | |
| owner | DE-29 DE-91G DE-BY-TUM DE-83 DE-11 DE-20 DE-19 DE-BY-UBM |
| owner_facet | DE-29 DE-91G DE-BY-TUM DE-83 DE-11 DE-20 DE-19 DE-BY-UBM |
| physical | XIII, 450 Seiten Illustrationen, Diagramme 24 cm x 17 cm |
| publishDate | 2019 |
| publishDateSearch | 2019 |
| publishDateSort | 2019 |
| publisher | De Gruyter Tsinghua University Press |
| record_format | marc |
| series2 | De Gruyter Graduate |
| spelling | Xu, Yuanzhi 1933- Verfasser (DE-588)1193948819 aut Electron magnetic resonance principles Yuanzhi Xu, Jia Yao Berlin ; Boston De Gruyter [2019] Beijing Tsinghua University Press [2019] © 2019 XIII, 450 Seiten Illustrationen, Diagramme 24 cm x 17 cm txt rdacontent n rdamedia nc rdacarrier De Gruyter Graduate Elektronenspinresonanz (DE-588)4132116-9 gnd rswk-swf Elektronenspinresonanzspektroskopie (DE-588)4151888-3 gnd rswk-swf Fachhochschul-/Hochschulausbildung Elektronenspinresonanz (DE-588)4132116-9 s DE-604 Elektronenspinresonanzspektroskopie (DE-588)4151888-3 s Yao, Jia Verfasser (DE-588)1193948967 aut Walter de Gruyter GmbH & Co. KG (DE-588)10095502-2 pbl Erscheint auch als Online-Ausgabe, PDF 978-3-11-056857-8 Erscheint auch als Online-Ausgabe, EPUB 978-3-11-062010-8 X:MVB http://www.degruyter.com/search?f_0=isbnissn&q_0=9783110528008&searchTitles=true X:MVB https://www.degruyter.com/doc/cover/9783110528008.jpg DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=030924423&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Xu, Yuanzhi 1933- Yao, Jia Electron magnetic resonance principles Elektronenspinresonanz (DE-588)4132116-9 gnd Elektronenspinresonanzspektroskopie (DE-588)4151888-3 gnd |
| subject_GND | (DE-588)4132116-9 (DE-588)4151888-3 |
| title | Electron magnetic resonance principles |
| title_auth | Electron magnetic resonance principles |
| title_exact_search | Electron magnetic resonance principles |
| title_full | Electron magnetic resonance principles Yuanzhi Xu, Jia Yao |
| title_fullStr | Electron magnetic resonance principles Yuanzhi Xu, Jia Yao |
| title_full_unstemmed | Electron magnetic resonance principles Yuanzhi Xu, Jia Yao |
| title_short | Electron magnetic resonance principles |
| title_sort | electron magnetic resonance principles |
| topic | Elektronenspinresonanz (DE-588)4132116-9 gnd Elektronenspinresonanzspektroskopie (DE-588)4151888-3 gnd |
| topic_facet | Elektronenspinresonanz Elektronenspinresonanzspektroskopie |
| url | http://www.degruyter.com/search?f_0=isbnissn&q_0=9783110528008&searchTitles=true https://www.degruyter.com/doc/cover/9783110528008.jpg http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=030924423&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT xuyuanzhi electronmagneticresonanceprinciples AT yaojia electronmagneticresonanceprinciples AT walterdegruytergmbhcokg electronmagneticresonanceprinciples |