The synthesis of novel Lewis acid catalysts and their use in Friedel-Crafts alkylation reactions:
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
Berlin
Mensch-und-Buch-Verl.
2002
|
| Schriftenreihe: | Forschungsberichte aus den Naturwissenschaften
|
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | Zugl.: Aachen, Techn. Hochsch., Diss., 2001 |
| Beschreibung: | IV, 135 S. graph. Darst. : 21 cm |
| ISBN: | 3898203840 |
Internformat
MARC
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| 100 | 1 | |a Valkenberg, Michael Hubert |e Verfasser |4 aut | |
| 245 | 1 | 0 | |a The synthesis of novel Lewis acid catalysts and their use in Friedel-Crafts alkylation reactions |c vorgelegt von Michael Hubert Valkenberg |
| 246 | 1 | |a The synthesis of novel Lewis-acid catalysts and their use in Friedel-Crafts alkylation reactions | |
| 264 | 1 | |a Berlin |b Mensch-und-Buch-Verl. |c 2002 | |
| 300 | |a IV, 135 S. |b graph. Darst. : 21 cm | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 490 | 0 | |a Forschungsberichte aus den Naturwissenschaften | |
| 500 | |a Zugl.: Aachen, Techn. Hochsch., Diss., 2001 | ||
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| 943 | 1 | |a oai:aleph.bib-bvb.de:BVB01-010070224 | |
Datensatz im Suchindex
| _version_ | 1808226456468193280 |
|---|---|
| adam_text |
CONTENT
1.
INTRODUCTION
AND
AIMS
1
2.
GENERAL
PART
4
2.1
THE
FRIEDEL-CRAFTS
ALKYLATION
REACTION
4
2.1.1
ALKYLATION
OF
BENZENE
WITH
DODECENE
8
2.1.2
ALKYLATION
OF
NAPHTHALENE
10
2.1.3
ALKYLATION
OF
PHENOL
11
2.2
IONIC
LIQUIDS
13
2.3
CATALYSIS
17
2.4
IMMOBILISATION
19
2.4.1
SUPPORT
MATERIALS
21
2.4.2
IMMOBILISATION
METHODS
24
3.
RESULTS
AND
DISCUSSION
39
3.1NLACSI
40
3.1.1
INCIPIENT
WETNESS
METHOD
40
3.1.2
TWO-STEP
IMMOBILISATION
48
3.2NLACSII
51
3.3
NLACS
HI
71
3.3.2
TWO-STEP
SYNTHESIS
OF
THE
ORGANICALLY
MODIFIED
HMS
79
3.4
ALKYLATION
EXPERIMENTS
84
3.4.1
ALKYLATION
OF
BENZENE
WITH
DODECENE
85
3.4.2
ALKYLATION
OF
NAPHTHALENE
WITH
DODECENE
102
3.4.3
ALKYLATION
OF
PHENOL
WITH
DODECENE
105
4.
SUMMARY
AND
OUTLOOK
108
5.
EXPERIMENTAL
111
5.1
GASES
111
5.2
ORGANIC
CHEMICALS
111
5.2.1
ORGANIC
STARTING
MATERIALS
111
5.2.2
ORGANIC
SOLVENTS
111
5.3
INORGANIC
CHEMICALS
112
CONTENT
7.
APPENDICES
5.4
ANALYTICAL
METHODS
112
5.4.1
GAS
CHROMATOGRAPHY
112
5.4.2
MASS
SPECTROSCOPY
113
5.4.3
CHN
ANALYSIS
114
5.4.4
NITROGEN
SORPTION
114
5.4.5
THERMOGRAVIMETRY
115
5.4.6
X-RAY
DIFFRACTOMETRY
115
5.4.7
ICP-AES
117
5.4.8
MASNMR
117
5.5
PREPARATION
OF
THE
CATALYSTS
119
5.5.1
PREPARATION
OF
THE
ILS
119
5.5.2
PREPARATION
OF
THE
NLACS
I
120
5.5.3
PREPARATION
OF
THE
NLACS
II
120
5.5.4
PREPARATION
OF
THE
NLACS
III
121
5.5.5
PREPARATION
OF
ALUMINIUM(III)
CHLORIDE
ON
SILICA
122
5.6
ORGANIC
REACTIONS
122
5.6.1
BATCH
REACTIONS
122
5.6.2
CONTINUOUS
LIQUID-PHASE
REACTIONS
123
6.
LITERATURE
124
133 |
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| genre_facet | Hochschulschrift |
| id | DE-604.BV014894405 |
| illustrated | Illustrated |
| indexdate | 2024-08-24T00:25:29Z |
| institution | BVB |
| isbn | 3898203840 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-010070224 |
| oclc_num | 76436535 |
| open_access_boolean | |
| owner | DE-91 DE-BY-TUM |
| owner_facet | DE-91 DE-BY-TUM |
| physical | IV, 135 S. graph. Darst. : 21 cm |
| publishDate | 2002 |
| publishDateSearch | 2002 |
| publishDateSort | 2002 |
| publisher | Mensch-und-Buch-Verl. |
| record_format | marc |
| series2 | Forschungsberichte aus den Naturwissenschaften |
| spelling | Valkenberg, Michael Hubert Verfasser aut The synthesis of novel Lewis acid catalysts and their use in Friedel-Crafts alkylation reactions vorgelegt von Michael Hubert Valkenberg The synthesis of novel Lewis-acid catalysts and their use in Friedel-Crafts alkylation reactions Berlin Mensch-und-Buch-Verl. 2002 IV, 135 S. graph. Darst. : 21 cm txt rdacontent n rdamedia nc rdacarrier Forschungsberichte aus den Naturwissenschaften Zugl.: Aachen, Techn. Hochsch., Diss., 2001 Homogene Katalyse (DE-588)4160579-2 gnd rswk-swf Lewis-Säure (DE-588)4300358-8 gnd rswk-swf Katalysator (DE-588)4029919-3 gnd rswk-swf Friedel-Crafts-Reaktion (DE-588)4123234-3 gnd rswk-swf (DE-588)4113937-9 Hochschulschrift gnd-content Lewis-Säure (DE-588)4300358-8 s Katalysator (DE-588)4029919-3 s Homogene Katalyse (DE-588)4160579-2 s DE-604 Friedel-Crafts-Reaktion (DE-588)4123234-3 s DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=010070224&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Valkenberg, Michael Hubert The synthesis of novel Lewis acid catalysts and their use in Friedel-Crafts alkylation reactions Homogene Katalyse (DE-588)4160579-2 gnd Lewis-Säure (DE-588)4300358-8 gnd Katalysator (DE-588)4029919-3 gnd Friedel-Crafts-Reaktion (DE-588)4123234-3 gnd |
| subject_GND | (DE-588)4160579-2 (DE-588)4300358-8 (DE-588)4029919-3 (DE-588)4123234-3 (DE-588)4113937-9 |
| title | The synthesis of novel Lewis acid catalysts and their use in Friedel-Crafts alkylation reactions |
| title_alt | The synthesis of novel Lewis-acid catalysts and their use in Friedel-Crafts alkylation reactions |
| title_auth | The synthesis of novel Lewis acid catalysts and their use in Friedel-Crafts alkylation reactions |
| title_exact_search | The synthesis of novel Lewis acid catalysts and their use in Friedel-Crafts alkylation reactions |
| title_full | The synthesis of novel Lewis acid catalysts and their use in Friedel-Crafts alkylation reactions vorgelegt von Michael Hubert Valkenberg |
| title_fullStr | The synthesis of novel Lewis acid catalysts and their use in Friedel-Crafts alkylation reactions vorgelegt von Michael Hubert Valkenberg |
| title_full_unstemmed | The synthesis of novel Lewis acid catalysts and their use in Friedel-Crafts alkylation reactions vorgelegt von Michael Hubert Valkenberg |
| title_short | The synthesis of novel Lewis acid catalysts and their use in Friedel-Crafts alkylation reactions |
| title_sort | the synthesis of novel lewis acid catalysts and their use in friedel crafts alkylation reactions |
| topic | Homogene Katalyse (DE-588)4160579-2 gnd Lewis-Säure (DE-588)4300358-8 gnd Katalysator (DE-588)4029919-3 gnd Friedel-Crafts-Reaktion (DE-588)4123234-3 gnd |
| topic_facet | Homogene Katalyse Lewis-Säure Katalysator Friedel-Crafts-Reaktion Hochschulschrift |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=010070224&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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