Structural studies of reactive metal electrodes: dissolution and passivation of nickel and etching of aluminum
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Abschlussarbeit Buch |
| Sprache: | English |
| Veröffentlicht: |
2001
|
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | Ulm, Univ., Diss., 2001. - Enth. Zsfassung in engl. und dt. Sprache |
| Beschreibung: | 224 S. Ill., graph. Darst. : 21 cm |
Internformat
MARC
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| 100 | 1 | |a Scherer, Jürgen |d 1971- |e Verfasser |0 (DE-588)123552265 |4 aut | |
| 245 | 1 | 0 | |a Structural studies of reactive metal electrodes |b dissolution and passivation of nickel and etching of aluminum |c vorgelegt von Jürgen Scherer |
| 264 | 1 | |c 2001 | |
| 300 | |a 224 S. |b Ill., graph. Darst. : 21 cm | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 500 | |a Ulm, Univ., Diss., 2001. - Enth. Zsfassung in engl. und dt. Sprache | ||
| 502 | |a Ulm, Univ., Diss., 2001 | ||
| 650 | 4 | |a Aluminiumfolie - Schwefelsäure - Chloridion - Nassätzen - Oberflächenanalyse | |
| 650 | 4 | |a Nickel - Elektrode - Schwefelsäure - Elektrochemische Korrosion - Oberflächenanalyse | |
| 650 | 0 | 7 | |a Chloridion |0 (DE-588)4147794-7 |2 gnd |9 rswk-swf |
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| 650 | 0 | 7 | |a Schwefelsäure |0 (DE-588)4180424-7 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Elektrochemische Korrosion |0 (DE-588)4197345-8 |2 gnd |9 rswk-swf |
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Datensatz im Suchindex
| _version_ | 1807504185582682112 |
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| adam_text |
CONTENTS
1
INTRODUCTION
.
1
2
FUNDAMENTALS
OF
ELECTROCHEMICAL
CORROSION
.
4
2.1
THERMODYNAMICS
AND
KINETICS
OF
ELECTROCHEMICAL
CORROSION
.
4
2.2
ANODIC
DISSOLUTION
.
8
2
J
PASSIVATION
.
11
2.4
PITTING
CORROSION
.
17
3
EXPERIMENTAL
.
21
3.1
ELECTROCHEMICAL
METHODS
.
21
3.1.1
FUNDAMENTALS
OF
ELECTROCHEMICAL
METHODS
.
21
3.1.2
EXPERIMENTAL
SETUP
AND
PROCEDURES
.
22
3.2
SURFACE
X-RAY
SCATTERING
.
24
3.2.1
FUNDAMENTALS
OF
X-RAY
SCATTERING
.
24
3.2.2
FUNDAMENTALS
OF
SURFACE
X-RAY
SCATTERING
.
27
3.2.3
THE
SURFACE
X-RAY
SCATTERING
EXPERIMENT
.
32
3.2.4
EXPERIMENTAL
SETUP
AND
PROCEDURES
.
34
3.2.5
COORDINATE
SYSTEM
.
36
33
SCANNING
TUNNELING
MICROSCOPY
.
38
3.3.1
FUNDAMENTALS
OF
SCANNING
TUNNELING
MICROSCOPY
.
38
3.3.2
SCANNING
TUNNELING
MICROSCOPY
AT
SOLID/LIQUID
INTERFACES
(IN
SITU
STM)
.
40
3.3.3
EXPERIMENTAL
SETUP
AND
PROCEDURES
.
41
3.3.4
PREPARATION
OF
TUNNELING
TIPS
.
44
3.4
ATOMIC
FORCE
MICROSCOPY
.
45
3.4.1
FUNDAMENTALS
OF
ATOMIC
FORCE
MICROSCOPY
(AFM)
.
45
3.4.2
EXPERIMENTAL
SETUP
AND
PROCEDURES
.
48
3.5
SAMPLE
PREPARATION
.
50
3.5.1
NICKEL(LLL)
SINGLE
CRYSTALS
.
50
3.5.2
ALUMINUM
FOILS
.
51
4
SURFACE
STRUCTURE,
DISSOLUTION
AND
PASSIVATION
OF
NICKEL(L
11)
IN
SULFURIC
ADD
SOLUTION
.
53
4.1
INTRODUCTION
.
53
4.2 ELECTROCHEMICAL
RESULTS
.
58
4.2.1
CYCLIC
VOLTAMMETRY
.
58
4.2.2
POLARIZATION
MEASUREMENTS
.
60
4.2.3
POTENTIAL
STEP
EXPERIMENTS
.
61
43
SURFACE
X-RAY SCATTERING
RESULTS.
64
4.3.1
STRUCTURE
OF
AIR-FORMED
OXIDE
ON
NI(
111)
.
64
4.3.2
STRUCTURE
OF
ELECTROCHEMICALLY
FORMED
PASSIVE
OXIDE
ON
NI(L
11)
.
71
4.3.3
DEPENDENCE
OF
THE
OXIDE
FILM
STRUCTURE
ON
THE
ENVIRONMENT
.
86
4.3.4
SPECULAR
X-RAY
REFLECTIVITY
.
91
4.4
SCANNING
TUNNELING
MICROSCOPY
RESULTS
.
97
4.4.1
SURFACE
STRUCTURE
OF
AIR-FORMED
OXIDE
ON
NI(L
11)
IN
AIR
.
97
4.4.2
SURFACE
STRUCTURE
OF
NI(L
11)
IN
0.05
M
H
2
SO
4
.
101
4.4.3
ANODIC
DISSOLUTION
OF
NI(L
11)
IN
0.05
M
H
2
SO
4
.
105
4.4.4
PASSIVE
FILM
FORMATION
ON
NI(L
11)
IN
0.05
M
H
2
SO
4
.
111
4.4.5
STRUCTURE
OF
AIR-FORMED
OXIDE
ON
NI(L
11)
AFTER
IMMERSION
INTO
0.05
M
H
2
SO
4
.
116
4.5
COMPARATIVE
DISCUSSION
AND
CONCLUSIONS
.119
4.5.1
STRUCTURE
OF
AIR-FORMED
OXIDE
ON
NI(L
11)
.
119
4.5.2
REDUCTION
OF
AIR-FORMED
OXIDE
ON
NI(L
11)
IN
0.05
M
H2SO4
AND
MORPHOLOGY
OF
REDUCED
SAMPLES
.
126
4.5.3
ATOMIC
SCALE
SURFACE
STRUCTURE
OF
REDUCED
NI(L
11)
IN
0.05
MH2SO4
.
130
4.5.4
ANODIC
DISSOLUTION
OF
NI(L
11)
IN
0.05
MH2SO4
.
132
4.5.5
PASSIVE
FILM
FORMATION
ON
NI(L
11)
IN
0.05
M
H2SO4.
135
4.5.6
PASSIVE
FILM
STRUCTURE
ON
NI(L
11)
.
139
4.5.7
DEPENDENCE
OF
THE
PASSIVE
FILM
STRUCTURE
ON
POTENTIAL
AND
SOLUTION
PH
.
147
4.5.8
CHANGES
OF
PASSIVE
FILMS
UPON
EMERSION
FROM
THE
ELECTROLYTE
SOLUTION
.
149
4.5.9
CHANGES
OF
AIR-FORMED
OXIDE
UPON
IMMERSION
INTO
THE
ELECTROLYTE
SOLUTION
.
150
4.5.10
SUMMARY
AND
CONCLUSIONS
.
152
5
ETCHING
OF
ALUMINUM
FOILS
IN
HOT,
CHLORIDE
CONTAINING
SULFURIC
ADD
SOLUTION
.
155
5.1
INTRODUCTION
.155
5.2
RESULTS
.
159
5.2.1
INITIAL
MORPHOLOGY
OF
AL
FOILS
.
159
5.2.2
MORPHOLOGICAL
CHANGES
DURING
CHEMICAL
ETCHING
.
164
5.2.3
ELECTROCHEMICAL
CHARACTERIZATION
OF
THE ETCH
PROCESS
.
166
5.2.4
MORPHOLOGICAL
CHANGES
DURING
ELECTROCHEMICAL
ETCHING
.
168
5.2.5
OCCURRENCE
AND
MORPHOLOGY
OF
HILLS
.
178
5.3
COMPARATIVE
DISCUSSION
AND
CONCLUSIONS
.
181
5.3.1
MORPHOLOGICAL
CHANGES
DURING
THE
FIRST
PERIOD
OF
ETCHING
(STAGE
I)
.
181
5.3.2
MORPHOLOGICAL
CHANGES
DURING
LONGER
GALVANOSTATIC
ETCHING
(STAGES
H
AND
III)
.
183
5.3.3
OCCURRENCE
OF
HILLS
DURING
THE
ETCH
PROCESS
.
186
6.
SUMMARY
.188
6.1
WORK
ON
NICKEL(LLL)
SINGLE
CRYSTALS
.
188
6.2
WORK
ON
ALUMINUM
FOILS
.
192
7
BIBLIOGRAPHY
.194
8.
ZUSAMMENFASSUNG
IN
DEUTSCHER
SPRACHE
.
.
.
211
8.1
UNTERSUCHUNGEN
AN
NL(L
11)
EINKRISTALLEN
.211
8.2
UNTERSUCHUNGEN
AN
ALUMINIUMFOLIEN
.
215
9
APPENDIX
.
218
A
ABBREVIATIONS
.
218
B
PUBLICATIONS
.
219
C
PRESENTATIONS.
.222
D
CURRICULUM
VITAE
(LEBENSLAUF)
.
223
E
ACKNOWLEDGEMENTS
.
.224 |
| any_adam_object | 1 |
| author | Scherer, Jürgen 1971- |
| author_GND | (DE-588)123552265 |
| author_facet | Scherer, Jürgen 1971- |
| author_role | aut |
| author_sort | Scherer, Jürgen 1971- |
| author_variant | j s js |
| building | Verbundindex |
| bvnumber | BV014224226 |
| ctrlnum | (OCoLC)248738402 (DE-599)BVBBV014224226 |
| format | Thesis Book |
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| genre | (DE-588)4113937-9 Hochschulschrift gnd-content |
| genre_facet | Hochschulschrift |
| id | DE-604.BV014224226 |
| illustrated | Illustrated |
| indexdate | 2024-08-16T01:05:16Z |
| institution | BVB |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-009752536 |
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| open_access_boolean | |
| owner | DE-355 DE-BY-UBR DE-29T DE-188 |
| owner_facet | DE-355 DE-BY-UBR DE-29T DE-188 |
| physical | 224 S. Ill., graph. Darst. : 21 cm |
| publishDate | 2001 |
| publishDateSearch | 2001 |
| publishDateSort | 2001 |
| record_format | marc |
| spelling | Scherer, Jürgen 1971- Verfasser (DE-588)123552265 aut Structural studies of reactive metal electrodes dissolution and passivation of nickel and etching of aluminum vorgelegt von Jürgen Scherer 2001 224 S. Ill., graph. Darst. : 21 cm txt rdacontent n rdamedia nc rdacarrier Ulm, Univ., Diss., 2001. - Enth. Zsfassung in engl. und dt. Sprache Ulm, Univ., Diss., 2001 Aluminiumfolie - Schwefelsäure - Chloridion - Nassätzen - Oberflächenanalyse Nickel - Elektrode - Schwefelsäure - Elektrochemische Korrosion - Oberflächenanalyse Chloridion (DE-588)4147794-7 gnd rswk-swf Nickel (DE-588)4042133-8 gnd rswk-swf Nassätzen (DE-588)4332374-1 gnd rswk-swf Oberflächenanalyse (DE-588)4172243-7 gnd rswk-swf Elektrode (DE-588)4014247-4 gnd rswk-swf Aluminiumfolie (DE-588)4129193-1 gnd rswk-swf Schwefelsäure (DE-588)4180424-7 gnd rswk-swf Elektrochemische Korrosion (DE-588)4197345-8 gnd rswk-swf (DE-588)4113937-9 Hochschulschrift gnd-content Nickel (DE-588)4042133-8 s Elektrode (DE-588)4014247-4 s Schwefelsäure (DE-588)4180424-7 s Elektrochemische Korrosion (DE-588)4197345-8 s Oberflächenanalyse (DE-588)4172243-7 s DE-604 Aluminiumfolie (DE-588)4129193-1 s Chloridion (DE-588)4147794-7 s Nassätzen (DE-588)4332374-1 s DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=009752536&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Scherer, Jürgen 1971- Structural studies of reactive metal electrodes dissolution and passivation of nickel and etching of aluminum Aluminiumfolie - Schwefelsäure - Chloridion - Nassätzen - Oberflächenanalyse Nickel - Elektrode - Schwefelsäure - Elektrochemische Korrosion - Oberflächenanalyse Chloridion (DE-588)4147794-7 gnd Nickel (DE-588)4042133-8 gnd Nassätzen (DE-588)4332374-1 gnd Oberflächenanalyse (DE-588)4172243-7 gnd Elektrode (DE-588)4014247-4 gnd Aluminiumfolie (DE-588)4129193-1 gnd Schwefelsäure (DE-588)4180424-7 gnd Elektrochemische Korrosion (DE-588)4197345-8 gnd |
| subject_GND | (DE-588)4147794-7 (DE-588)4042133-8 (DE-588)4332374-1 (DE-588)4172243-7 (DE-588)4014247-4 (DE-588)4129193-1 (DE-588)4180424-7 (DE-588)4197345-8 (DE-588)4113937-9 |
| title | Structural studies of reactive metal electrodes dissolution and passivation of nickel and etching of aluminum |
| title_auth | Structural studies of reactive metal electrodes dissolution and passivation of nickel and etching of aluminum |
| title_exact_search | Structural studies of reactive metal electrodes dissolution and passivation of nickel and etching of aluminum |
| title_full | Structural studies of reactive metal electrodes dissolution and passivation of nickel and etching of aluminum vorgelegt von Jürgen Scherer |
| title_fullStr | Structural studies of reactive metal electrodes dissolution and passivation of nickel and etching of aluminum vorgelegt von Jürgen Scherer |
| title_full_unstemmed | Structural studies of reactive metal electrodes dissolution and passivation of nickel and etching of aluminum vorgelegt von Jürgen Scherer |
| title_short | Structural studies of reactive metal electrodes |
| title_sort | structural studies of reactive metal electrodes dissolution and passivation of nickel and etching of aluminum |
| title_sub | dissolution and passivation of nickel and etching of aluminum |
| topic | Aluminiumfolie - Schwefelsäure - Chloridion - Nassätzen - Oberflächenanalyse Nickel - Elektrode - Schwefelsäure - Elektrochemische Korrosion - Oberflächenanalyse Chloridion (DE-588)4147794-7 gnd Nickel (DE-588)4042133-8 gnd Nassätzen (DE-588)4332374-1 gnd Oberflächenanalyse (DE-588)4172243-7 gnd Elektrode (DE-588)4014247-4 gnd Aluminiumfolie (DE-588)4129193-1 gnd Schwefelsäure (DE-588)4180424-7 gnd Elektrochemische Korrosion (DE-588)4197345-8 gnd |
| topic_facet | Aluminiumfolie - Schwefelsäure - Chloridion - Nassätzen - Oberflächenanalyse Nickel - Elektrode - Schwefelsäure - Elektrochemische Korrosion - Oberflächenanalyse Chloridion Nickel Nassätzen Oberflächenanalyse Elektrode Aluminiumfolie Schwefelsäure Elektrochemische Korrosion Hochschulschrift |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=009752536&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT schererjurgen structuralstudiesofreactivemetalelectrodesdissolutionandpassivationofnickelandetchingofaluminum |