Organic chemistry laboratory operations:
Gespeichert in:
| Hauptverfasser: | , |
|---|---|
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
New York [u.a.]
MacMillan
1962
|
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | VIII, 216 S. Ill. |
Internformat
MARC
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| 100 | 1 | |a Renfrow, William Burns |d 1914- |e Verfasser |0 (DE-588)173322220 |4 aut | |
| 245 | 1 | 0 | |a Organic chemistry laboratory operations |c W. R. Renfrow and P. J. Hawkins |
| 264 | 1 | |a New York [u.a.] |b MacMillan |c 1962 | |
| 300 | |a VIII, 216 S. |b Ill. | ||
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| 700 | 1 | |a Hawkins, Peter Jack |d 1922- |e Verfasser |0 (DE-588)173322239 |4 aut | |
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Datensatz im Suchindex
| _version_ | 1804152283294859264 |
|---|---|
| adam_text | RGANIC CHEMISTRY
LABORATORY OPERATIONS
W B Renfrow amp;PJ Hawkins
Oberlin College: Oberlin, Ohio
THE MACMILLAN COMPANY : NEW YORK
MACMILLANNEWYORK,LONDON
A DIVISION OF THE CROWELL-COLLIER PUBLISHING COMPANY
contents
General Instructions 1
1 Distillation 9
2 Fractional Distillation 13
3 Determination of Melting Point 16
4 Solubility Behavior of Organic Compounds 19
5 Extraction 23
6 Crystallization 27
7 Reactions of Hydrocarbons 31
8 1-Bromobutane from 1-Butanol 34
9 Etlianol from Sucrose by Fermentation 38
10 Ethyl Ether from Ethanol 40
11 2-Methyl-2-butene from 2-Methyl-2-butanol 43
12 jo-Xylene Sulfonic Acid from p-Xylene, an Electrophilic Substitution 46
13 Bromobenzene from Benzene 48
14 Benzoic Acid from Bromobenzene, the Preparation and Carbonation of a Grignard Reaction 50
15 Methyl Benzoate from Benzoic Acid and Methanol 52
16 2-Methyl-2-hexene from 1-Bromobutane and Acetone 54
17 Acetyl Chloride from Acetic Acid and Phosphorous Trichloride 56
18 Acetophenone from Benzene and Acetyl Chloride 58
19 Acetylsalicylic Acid (Aspirin) from Salicylic Acid 60
20 1-Phenoxybutane froip 1-Bromobutane and Phenol A Williamson Synthesis 62
21 A Diels-Alder Reaction 3, 6-Oxo-l, 2, 3, 6-tetrahydrophthalic Anhydride from Furan and
Maleic Anhydride 63
22 Mandelic Acid 65
23 An Aldol Condensation 1 5-Di phenyl penta-1 4-diene-3-on from Benzaldehyde and Acetone
Dibenalacetone 67
24 Benzoin, Benzil, and Benzilic Acid from Benzaldehyde 69
25 2, 2-Z?is-(p-chlorophenyl)-l, 1, 1-trichloroethane from Chloral and Chlorobenzene DDT 71
26 Nitrobenzene from Benzene 73
27 Acetanilide from Nitrobenzene 74
28 Sulfanilamide from Acetanilide 77
29 m-Nitrobenzoic Acid from Methyl Benzoate 79
30 The Hinsberg Method for Characterization of Amines 80
31 JV-(Benzenesulfo)-6-aminocaproic Acid from Cyclohexanol 82
32 m-Dichlorobenzene from m-Chloroaniline 84
33 Congo Red An Azo Dye and an Indicator 86
34 Polymerization Polysterene and Nylon 88
35 Amytal from Diethyl Ethyl-isopentylmalonate and Urea 90
36 Caffeine from Tea 92
37 Alkylation and Ketonic Cleavage of Acetoacetic Ester 93
vi
38 Some Properties of Sugars 96
39 Tyrosine from Casein 100
40 o-Chlorobenzoic Acid from Anthranilic Acid 102
41 m-Nitrobenzamide from m-Nitrobenzoic Acid 103
42 Detection of Sulfur, Nitrogen, and Halogens in Organic Compounds 105
43 Qualitative Organic Analysis 108
44 Qualitative Analysis of Mixtures of Organic Compounds 126
45 Extraction and Distribution 131
46 47, and 48 , Chromatography 136
46 Column Chromatography 139
47 Paper Chromatography 140
48 Gas Chromatography 142
49 Vacuum Distillation 143
50 and 51 Advanced Fractional Distillation 147
50 Separation of a Three-Component Mixture with a Packed Column 151
51 Separation of a Three-Component Mixture with a S[tinning Band Column 152
52 and 53 Hydrogenation and Hydrogenolysis 153
52 Low Pressure Hydrogenation 155
53 High Pressure Hydrogenation 157
54 and 55 Determination of Molecular Weight by the Rast Method 160
54 Macro Rast 161
55 Semimicro Rast 163
56 Catalytic Dehydration of Cyclohexanol A Hot Tube Reaction 165
57 Use of the Library Technical Reports 167
58 Use of Punched Cards for Filing and Recovering Information 171
59 Anhydrous Ethanol 175
60-64 Density, Refractive Index, Optical Rotation, Absorption Spectroscopy 176
60 Determination of the Density of a Liquid 177
61 Measurement of Refractive Index 179
62 Measurement of Optical Rotation 181
63 and 64 Absorption Spectroscopy 184
63 Infrared Spectroscopy 186
64 Ultraviolet Spectroscopy 197
65 and 66 Ionization Constants and Reaction Rates 202
65 The Determination of Acid Dissociation Constants 203
66 Determination of Rate Constants 205
Appendixes
I Starting Materials 209
II Concentration of Common Reagents; Common Solvents; Atomic Weights 210
TI Suggested Apparatus List 211
vii
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| illustrated | Illustrated |
| indexdate | 2024-07-10T01:08:15Z |
| institution | BVB |
| language | English |
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| physical | VIII, 216 S. Ill. |
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| spelling | Renfrow, William Burns 1914- Verfasser (DE-588)173322220 aut Organic chemistry laboratory operations W. R. Renfrow and P. J. Hawkins New York [u.a.] MacMillan 1962 VIII, 216 S. Ill. txt rdacontent n rdamedia nc rdacarrier Hawkins, Peter Jack 1922- Verfasser (DE-588)173322239 aut HEBIS Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=027360500&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Renfrow, William Burns 1914- Hawkins, Peter Jack 1922- Organic chemistry laboratory operations |
| title | Organic chemistry laboratory operations |
| title_auth | Organic chemistry laboratory operations |
| title_exact_search | Organic chemistry laboratory operations |
| title_full | Organic chemistry laboratory operations W. R. Renfrow and P. J. Hawkins |
| title_fullStr | Organic chemistry laboratory operations W. R. Renfrow and P. J. Hawkins |
| title_full_unstemmed | Organic chemistry laboratory operations W. R. Renfrow and P. J. Hawkins |
| title_short | Organic chemistry laboratory operations |
| title_sort | organic chemistry laboratory operations |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=027360500&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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