Polyacrylate- und Poly-N-Isopropylacrylamid-Copolymere mit chemisch verknüpften Seitenketten und Fluoreszenzmarkern als "intelligente Materialien" für den Aufbau von Sensoren und Nanoreaktoren: = Labeled polyacrylate and poly-N-isopropylacrylamide-copolymers as advanced tools for the design of sensors and nanoreactors
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Buch |
| Sprache: | English German |
| Veröffentlicht: |
2002
|
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | Karlsruhe, Univ., Diss., 2002 |
| Beschreibung: | XXXI, 183 S. Ill., graph. Darst. |
Internformat
MARC
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| 035 | |a (DE-599)BVBBV014489128 | ||
| 040 | |a DE-604 |b ger |e rakwb | ||
| 041 | 0 | |a eng |a ger | |
| 049 | |a DE-91 |a DE-83 | ||
| 100 | 1 | |a Pokhrel, Megh Raj |e Verfasser |4 aut | |
| 245 | 1 | 0 | |a Polyacrylate- und Poly-N-Isopropylacrylamid-Copolymere mit chemisch verknüpften Seitenketten und Fluoreszenzmarkern als "intelligente Materialien" für den Aufbau von Sensoren und Nanoreaktoren |b = Labeled polyacrylate and poly-N-isopropylacrylamide-copolymers as advanced tools for the design of sensors and nanoreactors |c von Megh Raj Pokhrel |
| 246 | 1 | 1 | |a Labeled polyacrylate and poly-N-isopropylacrylamide-copolymers as advanced tools for the design of sensors and nanoreactors |
| 264 | 1 | |c 2002 | |
| 300 | |a XXXI, 183 S. |b Ill., graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 500 | |a Karlsruhe, Univ., Diss., 2002 | ||
| 650 | 0 | 7 | |a Copolymere |0 (DE-588)4010542-8 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Polyacrylsäurederivate |0 (DE-588)4378092-1 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Seitenkette |0 (DE-588)4330425-4 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Fluoreszenzmarkierte Verbindungen |0 (DE-588)4154828-0 |2 gnd |9 rswk-swf |
| 655 | 7 | |0 (DE-588)4113937-9 |a Hochschulschrift |2 gnd-content | |
| 689 | 0 | 0 | |a Polyacrylsäurederivate |0 (DE-588)4378092-1 |D s |
| 689 | 0 | 1 | |a Copolymere |0 (DE-588)4010542-8 |D s |
| 689 | 0 | 2 | |a Fluoreszenzmarkierte Verbindungen |0 (DE-588)4154828-0 |D s |
| 689 | 0 | 3 | |a Seitenkette |0 (DE-588)4330425-4 |D s |
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| 943 | 1 | |a oai:aleph.bib-bvb.de:BVB01-009881376 | |
Datensatz im Suchindex
| _version_ | 1807504112108961792 |
|---|---|
| adam_text |
III
CONTENTS
CONTENTS
III
LIST
OF
FIGURES
VIII
LIST
OF
TABLES
XVI
LIST
OF
SCHEMES
XVIII
GOALS
AND LIMITATIONS
OF
THE
WORK
XIX
KURZFASSUNG
XXIII
ABSTRACT
XXVIII
1.
GENERAL
INTRODUCTION
1
2.
THEORETICAL
BACKGROUND
8
2.1
AN
INTRODUCTION
TO
PHOTOPHYSICAL
PROCESSES
8
2.2
FLUORESCENCE
POLARIZATION
AND
ANISOTROPY
10
2.3
PHOTOPHYSICS
OF
PYRENE
AND
PYRENE
LABELED
POLYMERS
16
2.4
FREE
RADICAL
POLYMERIZATION
21
2.5
KINETICS
AND
THERMODYNAMICS
OF
FREE
RADICAL
COPOLYMERIZATION
23
2.5.1
KINETICS
OF
COPOLYMERIZATION
24
2.5.1.1
THE
COPOLYMER EQUATION
24
2.5.1.2
MONOMER
REACTIVITY
RATIOS
25
2.5.1.3
TYPES
OF
COPOLYMERIZATION
25
2.5.2
THERMODYNAMICS
OF
FREE
RADICAL
COPOLYMERIZATION
26
2.6
DETERMINATION
OF
POLYMER
MOLECULAR
WEIGHTS
27
2.7
HYDROGELS
28
2.8
REFERENCES
30
3.
EXPERIMENTAL
SECTION
32
3.1
MATERIALS
32
3.2
SYNTHETIC
PROCEDURES
FOR
THE
PREPARATION
OF
COPOLYMERS
32
3.2.1
SYNTHESIS
OF
COPOLYMERS
OFN-ISOPROPYLACRYLAMIDE
AND ACRYLIC
ACID
(PNIPAM
PAA)
32
3.2.2
SYNTHESIS
OF
COPOLYMERS
OF
N-ISOPROPYLACRYLAMIDE
AND
ACRYLIC ACID
FEATURING
PERFLUORINATED
SIDE CHAINS (PNIPAM-PAA-C
8
F
I7
)
33
IV
3.2.3
SYNTHESIS
OF
COPOLYMERS
OF
N-ISOPROPYLACRYLAMIDE
AND
ACRYLIC
ACID
FEATURING
PERFLUORINATED
SIDE
CHAINS
AND
CHEMICALLY
LINKED
PYRENE
(PNIPAM-PAA-C
G
F,
7
-PY)
3.2.4
SYNTHESIS
OF
HIGH MOLECULAR
WEIGHT
POLYACRYLIC
ACID
DERIVATIES
POSSESSING
34
PERFLUORINATED
SIDE
CHAINS AND
CHEMICALLY
LINKED
PYRENE
(PAA-C
G
F,,-PY)
3.2.5
PHOTOINITIATED
POLYMERIZATION
OF
LATEX
PARTICLES
34
4.
SAMPLE
PREPARATIONS
AND
MEASUREMENTS
36
4.1
DIFFERENTIAL
SCANNING
CALORIMETRY
(DSC)
36
4.2
IR-SPECTROSCOPY
-
36
4.3
UV-VIS
SPECTROSCOPY
37
4.4
FLUORESCENCE
SPECTROSCOPY
37
4.5
PHASE
DIAGRAM
39
4.6
GEL
PERMEATION
CHROMATOGRAPHY
40
4.7
VISCOSITY
MEASUREMENTS
40
4.8
ELEMENTARY
ANALYSIS
40
4.9
ACID-BASE
TITRATION
40
4.10
DOC-MEASUREMENTS
41
4.11
HPLC
DETERMINATION
OF
THE
PHOTOINITIATOR
CONCENTRATION
41
4.12
TEM-SAMPLE
PREPARATION
41
4.13
TRANSMISSION
MEASUREMENTS
42
4.14
REFERENCES
42
5.
SYNTHESIS,
CHARACTERIZATION
AND
FIRST
APPLICATION
OF
HIGH
MOLECULAR
WEIGHT
POLYACRYLIC
ACID
DERIVATIVES
POSSESSING
PERFLUORINATED
SIDE
CHAINS
AND
CHEMICALLY
43
LINKED
PYRENE
LABELS
5.1
INTRODUCTION
43
5.2
SYNTHESIS
45
5.3
CHARACTERIZATION
OF
THE
NOVEL
MACROMOLECULES
46
5.3.1
DETERMINATION
OF
THE
PYRENE
CONTENT
46
V
5.3.2
DETERMINATION
OF
THE
PERFLUORO-OCTYLESTER
CONTENT
46
5.4
VISCOSITY
MEASUREMENTS
OF
PAA/PYRENE/-C
G
F
17
MACROMOLECULES
DISSOLVED
IN
WATER
49
5.5
GPC-CHARACTERIZATION
50
5.6
STEADY
STATE
FLUORESCENCE
MEASUREMENTS
51
5.7
TIME
RESOLVED
FLUORESCENCE
MEASUREMENTS
55
5.7.1
PAA-PYRENE/151-C
8
F
L7
/2.85
56
5.7.2
PAA-PYRENE/271-C
8
F
17
/7.95:
PAA-PYRENE/313-C
8
F
I7
/12.5:
58
P
AA-PYRENE/469-C
8
F
YY/30.
5
5.8
DESIGN
OF
A
FLUORESCENCE
SENSOR
FOR
PH-MEASUREMENTS
59
5.9
CONCLUSIONS
60
5.10
REFERENCES
64
6.
SYNTHESIS
AND
CHARACTERIZATION
OF
PH
AND
TEMPERATURE
SENSITIVE
COPOLYMERS
OF
N-ISOPROPYLACRYLAMIDE
AND
ACRYLIC
ACID
(PNIPAM-PAA)
POSSESSING
PERFLUORINATED
(-C,F|
7
)
SIDE
CHAINS
(PNIPAM-PAA
C,F
N
)
AS
WELL
AS
CHEMICALLY
LINKED
PYRENE
LABEL
(PNIPAM-PAA
C,F,
7
PY)
68
6.1
INTRODUCTION
68
6.2
RESULTS
AND
DISCUSSIONS
7
6.2.1
SYNTHESIS
OF
COPOLYMERS
7
6.2.1.1
SYNTHESIS
OF
PNIPAM-PAA
COPOLYMERS
YY
6.2.1.2
SYNTHESIS
OFPNIPAM-PAA-C
8
F
17
-PY
COPOLYMERS
6.2.1.3
SYNTHESIS
OF
PNIPAM-PAA-PY
COPOLYMERS
76
6.2.2
CHARACTERIZATION
OF
COPOLYMERS
7
6
6.2.2.1
ACID-BASE
TITRATION
7
6
6.2.2.2
UV-VIS
SPECTROSCOPY
78
6.2.2.2.
1
CALCULATION
OF
PYRENE CONTENT
7
$
6.2.2.2.2
PEAK-VALLEY-RATIO
80
6.2.2.3
IR-SPECTROSCOPY
82
VI
6.2.2.4
DIFFERENTIAL
SCANNING
CALOMETRY
(DSC)
85
6.2.2.4.
1
PHASE
TRANSITION
OF
THE
COPOLYMERS
85
6.2.2.4.2
DEPENDENCE
OF
PHASE
TRANSITION
TEMPERATURE
OF
THE
COPOLYMERS
ON
PH
88
6.2.2.4.3
DEPENDENCE
OF
PHASE
TRANSITION
ENTHALPY
OF
THE
COPOLYMERS
ON
PH
89
6.2.2.5
GEL
PERMEATION
CHROMATOGRAPHY
90
6.2.3
PHASE
DIAGRAMS
OF
COPOLYMERS
IN
WATER/ORGANIC
SOLVENTS
92
6.2.3.1
COPOLYMER/WATER/METHANOL
TERNARY
SYSTEM
92
6.2.3.2
COPOLYMER/WATER/DMF
TERNARY
SYSTEM
94
6.2.3.3
COPOLYMER/WATER/THF
TERNARY
SYSTEM
97
6.2.4
EFFECTS
OF
IONIC
STRENGTH
ON
PHASE
TRANSITION
TEMPERATURE
OF
THE
COPOLYMERS
98
6.2.4
EFFECT
OF
DTAC
AND
METAL
IONS
(CA
2+
,
MG
2
*,
AL
2+
)
98
6.2.5
TRANSMISSION
MEASUREMENTS
OF
AN
AQUEOUS
SOLUTION
OF
THE
PNIPAM
AND
102
PNIPAM-PAA,
PNIPAM-PAA-C
S
F
J
7
COPOLYMERS
6.2.6
PHOTOPHYSICAL
STUDIES
OF
THE
COPOLYMERS
'98
6.2.6.1
STEADY
STATE
FLUORESCENCE
MEASUREMENTS
'08
6.2.6.1.1
PNIPAM
AND
PNIPAM-PAA
'
'0
6.2.6.1.2
PNIPAM-PAA-PY
AND
PNIPAM-PAA-C
8
F
17
-PY
1
'
9
6.2.6.2
TIME
RESOLVED
FLUORESCENCE
MEASUREMENTS
130
6.2.6.2.1
PNIPAM-PAA-C
8
F
17
-PY
131
6.2.6.2.2
PNIPAM-PAA-PY
132
6.2.6.3
ROTATIONAL
RELAXATION TIME FOR
PYRENE
MONOMER
AND
EXCIMER
EMISSION
OF
YY
135
PNIPAM-PAA-PY
AND
PNIPAM-PAA-C
8
F
17
COPOLYMERS
6.3
CONCLUSIONS
137
6.4
REFERENCES
140
VII
7.
PHOTOINITIATED
SYNTHESIS
AND
CHARACTERIZATION
OF
P(MMA/DPB)POLYMER
NANOPARTICLES
USING
POLY(N-ISOPROPYLACRYLAMIDE)IN
AQUEOUS
SOLUTION
AS
TEMPLATE
142
7.1
INTRODUCTION
142
7.2
RESULTS AND DISCUSSIONS
144
7.2.1
FERRIOXALATE ACTINOMETRY,
APPARENT
QUANTUM
YIELD
AND
REACTION RATE
CONSTANTS
OF
PHOTOINITIATOR
CONSUMPTION
IN
PNIPAM/H
2
O/DMF
144
7.2.2
FORMATION
OF
P(MMA/DPB)
LATEX
PARTICLES
IN
PNIPAM/H
2
O/DMF
148
7.2.3
GPC-ANALYSIS
148
7.2.4
TEM-CHARACTERIZATION
151
7.2.5
COMPUTER-ASSISTED
ANALYSIS
OF
THE
P(MMA/DPB)-MORPHOLOGY
AND
SIZE
DISTRIBUTION
155
7.2.6
CHN-ANALYSIS
157
7.3
CONCLUSIONS
158
7.4 REFERENCES
159
8.
ACKNOWLEDGEMENTS
163
9.
APPENDIX
164
10.
ABBREVIATIONS
181 |
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| genre | (DE-588)4113937-9 Hochschulschrift gnd-content |
| genre_facet | Hochschulschrift |
| id | DE-604.BV014489128 |
| illustrated | Illustrated |
| indexdate | 2024-08-16T01:04:08Z |
| institution | BVB |
| language | English German |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-009881376 |
| oclc_num | 248744166 |
| open_access_boolean | |
| owner | DE-91 DE-BY-TUM DE-83 |
| owner_facet | DE-91 DE-BY-TUM DE-83 |
| physical | XXXI, 183 S. Ill., graph. Darst. |
| publishDate | 2002 |
| publishDateSearch | 2002 |
| publishDateSort | 2002 |
| record_format | marc |
| spelling | Pokhrel, Megh Raj Verfasser aut Polyacrylate- und Poly-N-Isopropylacrylamid-Copolymere mit chemisch verknüpften Seitenketten und Fluoreszenzmarkern als "intelligente Materialien" für den Aufbau von Sensoren und Nanoreaktoren = Labeled polyacrylate and poly-N-isopropylacrylamide-copolymers as advanced tools for the design of sensors and nanoreactors von Megh Raj Pokhrel Labeled polyacrylate and poly-N-isopropylacrylamide-copolymers as advanced tools for the design of sensors and nanoreactors 2002 XXXI, 183 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Karlsruhe, Univ., Diss., 2002 Copolymere (DE-588)4010542-8 gnd rswk-swf Polyacrylsäurederivate (DE-588)4378092-1 gnd rswk-swf Seitenkette (DE-588)4330425-4 gnd rswk-swf Fluoreszenzmarkierte Verbindungen (DE-588)4154828-0 gnd rswk-swf (DE-588)4113937-9 Hochschulschrift gnd-content Polyacrylsäurederivate (DE-588)4378092-1 s Copolymere (DE-588)4010542-8 s Fluoreszenzmarkierte Verbindungen (DE-588)4154828-0 s Seitenkette (DE-588)4330425-4 s DE-604 DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=009881376&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Pokhrel, Megh Raj Polyacrylate- und Poly-N-Isopropylacrylamid-Copolymere mit chemisch verknüpften Seitenketten und Fluoreszenzmarkern als "intelligente Materialien" für den Aufbau von Sensoren und Nanoreaktoren = Labeled polyacrylate and poly-N-isopropylacrylamide-copolymers as advanced tools for the design of sensors and nanoreactors Copolymere (DE-588)4010542-8 gnd Polyacrylsäurederivate (DE-588)4378092-1 gnd Seitenkette (DE-588)4330425-4 gnd Fluoreszenzmarkierte Verbindungen (DE-588)4154828-0 gnd |
| subject_GND | (DE-588)4010542-8 (DE-588)4378092-1 (DE-588)4330425-4 (DE-588)4154828-0 (DE-588)4113937-9 |
| title | Polyacrylate- und Poly-N-Isopropylacrylamid-Copolymere mit chemisch verknüpften Seitenketten und Fluoreszenzmarkern als "intelligente Materialien" für den Aufbau von Sensoren und Nanoreaktoren = Labeled polyacrylate and poly-N-isopropylacrylamide-copolymers as advanced tools for the design of sensors and nanoreactors |
| title_alt | Labeled polyacrylate and poly-N-isopropylacrylamide-copolymers as advanced tools for the design of sensors and nanoreactors |
| title_auth | Polyacrylate- und Poly-N-Isopropylacrylamid-Copolymere mit chemisch verknüpften Seitenketten und Fluoreszenzmarkern als "intelligente Materialien" für den Aufbau von Sensoren und Nanoreaktoren = Labeled polyacrylate and poly-N-isopropylacrylamide-copolymers as advanced tools for the design of sensors and nanoreactors |
| title_exact_search | Polyacrylate- und Poly-N-Isopropylacrylamid-Copolymere mit chemisch verknüpften Seitenketten und Fluoreszenzmarkern als "intelligente Materialien" für den Aufbau von Sensoren und Nanoreaktoren = Labeled polyacrylate and poly-N-isopropylacrylamide-copolymers as advanced tools for the design of sensors and nanoreactors |
| title_full | Polyacrylate- und Poly-N-Isopropylacrylamid-Copolymere mit chemisch verknüpften Seitenketten und Fluoreszenzmarkern als "intelligente Materialien" für den Aufbau von Sensoren und Nanoreaktoren = Labeled polyacrylate and poly-N-isopropylacrylamide-copolymers as advanced tools for the design of sensors and nanoreactors von Megh Raj Pokhrel |
| title_fullStr | Polyacrylate- und Poly-N-Isopropylacrylamid-Copolymere mit chemisch verknüpften Seitenketten und Fluoreszenzmarkern als "intelligente Materialien" für den Aufbau von Sensoren und Nanoreaktoren = Labeled polyacrylate and poly-N-isopropylacrylamide-copolymers as advanced tools for the design of sensors and nanoreactors von Megh Raj Pokhrel |
| title_full_unstemmed | Polyacrylate- und Poly-N-Isopropylacrylamid-Copolymere mit chemisch verknüpften Seitenketten und Fluoreszenzmarkern als "intelligente Materialien" für den Aufbau von Sensoren und Nanoreaktoren = Labeled polyacrylate and poly-N-isopropylacrylamide-copolymers as advanced tools for the design of sensors and nanoreactors von Megh Raj Pokhrel |
| title_short | Polyacrylate- und Poly-N-Isopropylacrylamid-Copolymere mit chemisch verknüpften Seitenketten und Fluoreszenzmarkern als "intelligente Materialien" für den Aufbau von Sensoren und Nanoreaktoren |
| title_sort | polyacrylate und poly n isopropylacrylamid copolymere mit chemisch verknupften seitenketten und fluoreszenzmarkern als intelligente materialien fur den aufbau von sensoren und nanoreaktoren labeled polyacrylate and poly n isopropylacrylamide copolymers as advanced tools for the design of sensors and nanoreactors |
| title_sub | = Labeled polyacrylate and poly-N-isopropylacrylamide-copolymers as advanced tools for the design of sensors and nanoreactors |
| topic | Copolymere (DE-588)4010542-8 gnd Polyacrylsäurederivate (DE-588)4378092-1 gnd Seitenkette (DE-588)4330425-4 gnd Fluoreszenzmarkierte Verbindungen (DE-588)4154828-0 gnd |
| topic_facet | Copolymere Polyacrylsäurederivate Seitenkette Fluoreszenzmarkierte Verbindungen Hochschulschrift |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=009881376&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT pokhrelmeghraj polyacrylateundpolynisopropylacrylamidcopolymeremitchemischverknupftenseitenkettenundfluoreszenzmarkernalsintelligentematerialienfurdenaufbauvonsensorenundnanoreaktorenlabeledpolyacrylateandpolynisopropylacrylamidecopolymersasadvancedtoolsforthedesignofse AT pokhrelmeghraj labeledpolyacrylateandpolynisopropylacrylamidecopolymersasadvancedtoolsforthedesignofsensorsandnanoreactors |