Simultaneous thermoanalytical examinations by means of the derivatograph:
Gespeichert in:
| Hauptverfasser: | , |
|---|---|
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
Amsterdam [u.a.]
Elsevier
1981
|
| Schriftenreihe: | Wilson and Wilson's comprehensive analytical chemistry
12,A : Thermal analysis |
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | Literaturverz. S. 211 - 258 |
| Beschreibung: | XVIII, 277 S. Ill., graph. Darst. |
| ISBN: | 0444419497 |
Internformat
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| 100 | 1 | |a Paulik, J. |e Verfasser |4 aut | |
| 245 | 1 | 0 | |a Simultaneous thermoanalytical examinations by means of the derivatograph |c by J. Paulik and F. Paulik |
| 264 | 1 | |a Amsterdam [u.a.] |b Elsevier |c 1981 | |
| 300 | |a XVIII, 277 S. |b Ill., graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 490 | 1 | |a Wilson and Wilson's comprehensive analytical chemistry |v 12,A : Thermal analysis | |
| 500 | |a Literaturverz. S. 211 - 258 | ||
| 650 | 7 | |a Analyse thermique |2 ram | |
| 650 | 7 | |a Chimie analytique |2 ram | |
| 650 | 7 | |a Thermogravimétrie |2 ram | |
| 650 | 4 | |a Thermogravimetry | |
| 700 | 1 | |a Paulik, Ferenc |e Verfasser |4 aut | |
| 830 | 0 | |a Wilson and Wilson's comprehensive analytical chemistry |v 12,A : Thermal analysis |w (DE-604)BV000900805 |9 12,1 | |
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| 999 | |a oai:aleph.bib-bvb.de:BVB01-000642817 | ||
Datensatz im Suchindex
| _version_ | 1804115479266066432 |
|---|---|
| adam_text | Wilson and Wilson s
COMPREHENSIVE ANALYTICAL CHEMISTRY
Edited by
G SVEHLA, PH D,D SC ,FRIC
Reader in Analytical Chemis t r y
The Queen s Un iv ersityof Be l fa s t
VOLUME XII
THERMAL ANALYSIS
WW WENDLANDT (ADVISORY EDITOR)
PART A
SIMULTANEOUS THERMOANALYTICAL
EXAMINATIONS BY MEANS OF THE
DERIVATOGRAPH
BY J PAULIK AND F PAULIK
ELSEVIER SCIENTIFIC PUBLISHING COMPANY
AMSTERDAM OXFORD NEW YORK
XIII
Contents
Theory and techniques
1 Introduction 1-6
1 1 Development of derivative and simultaneous
methods 1
1 2 Information-multiplying ei fect of simul
taneous examinations 3
1 3 Resolution of tliermoanaly ileal cLirves 5
2 Derivative thermogravimetry 7-8
3 Simultaneous DTA, TG and DTG 8—22
3 1 Influence of experimental conditions 8
3 2 Method for simultaneous TG, DTG and DTA 14
3 3 Interpretation and evaluation of simul
taneously recorded curves 16
3 4 Accuracy of the determinaiion in the case
of overlapping reactions 20
4 Derivative dilatometry 22-29
4 1 Method for simultaneous T]», DTD and DTA 23
4 2 Method for simultaneous T]», DTD TG,
* DTG and DTA 25
4 3 Application of dilatometrii c examinations 28
5 Means for increasing the selectsity 29—34
5 1 Selectivity of examinatioi 29
5 2 Multi-plate sample holder 31
6 Thermogas titrimetry 35-47
6 1 Method for simultaneous T])T, DTGT,
TG, DTG, and DTA 35
6 2 Some examples of thermogas titrimetric
1 examinations 40
7 Quasi-isothermal quasi-isobaric i tiermogravimetry 47-71
7 1 Normalization of experimental conditions 47
7 2 Quasi-isothermal heating i echnique 48
7 3 Formation of quasi-isobaric conditions as a
result of quasi-isothermal heating 50
XIV
7 4, Labyrinth crucible 34
7 5 Method for quasi-isothermal quasi-isobaric
thermogravimetry (Q-TG) 56
751 Interpretation of quasi-isothermal quasi-
-isobaric TG curvet from the kinetic aspect 56
752 Interpretation of cjuasi-isothermal quasi-
—isobaric TG curves from the aspect of
reaction mechanism 67
8, Simultaneous TG and TGT examination under quasi-
—isothermal quasi-isobaric conditions 71-79
8, Quasi-isothermal thermodil tometry 79—85
Applications
10, Inorganic compounds 86-128
Fe^O^ xH^O 86
Ge02 86
CaC O^ HgO + SrC20^ H20 + BaC^ 0 51^0 88
MeNH^PO^ (Me = Be, Zn, Cd, Co, Mg) 88
BaSO^ 89
KAl(S04)2 2i+H20 89
uo3 91
Co(OH)^ 9^
BaCl2 2H20, SrCl2 6H20, CiC12 6H20, MgCl2 6H20 jh
j BeS0 k kH z 0 9(
CaS04 2H20 97
Rb2S04 3Li2S0^ 2H20, CsSO l+ 3L±2SO^ 21^0 98
ZnSxFg 6H20, CdS±Fg 6H20 9S
(NH 4)6 (M o?02;+)te20 99
KH(JO3)2 100
LaCo(C20it)3 9H20, CeCo( CgO^) 9H20 101
Ag203 101
KClOg 102
, K4P2°8 ^ p208-te20 K2H2P2°8 103
Na2S2°8 K2S2°8 105
Ca2X209 9H20, Ba2I20 9H20 106
Ag202 106
ZnO 106
Mn02, Mn02 + C 107
Sr(0H)2 8H20 108
XV
MnC03 xH20 109
PbCO^ 111
L±2C03 + A1203, KagCO^ + Al^, K2C03 + A12°3 111
NaHCC 3 112
CaC03 113
Alkali metal ha lides 115
BaF2 4 5HF, SrF 2 5HF, CaF2_2HF 115
NaHSO^ HgO 115
PdCl2, RhCl3 4H20 116
AgSe03NAe2 3NH3 2H20, AgSO^Agg 1NH3 2«20 117
MnCgO^ 2H20, CoC20^ 2H,0, NiC^^HgO 118
BaC20^ 0 5H20 119
NaH2P0^ H2O, NaP03 120
Chromium(II)phosphate polymers 122
NH^N03 124
NH^N03 + KC1 125
CoNH^PO^ HgO, MnNH^PO^ HgO, CdNffl ^PO^ H20 127
11, Complexes 128-144
Mn, Co, Ni, Cu, Zn and Cd pyridine halldes 128
MgCd(edta),9H20 129
Zn(edta) 6H20 130
(NHu)2[Fe(CN)6], (NH^)2[Fe(CN)gNO] 131
Metal and me talammine cyanometalLate 132
ZnS206 6H2 0, Zn(NH3)4S20g, Zn(CH ,NH2) 134
[Co(»p)^(NCS)2] 134
Catecholgermanic acid 135
[Ni(H 0)2(NN-deen) ]Cl2, [Ni(H20 2(NN-deen)2
[N±(H20)2(NN-deen)2JBr2 H20 137
[CrHedta(H20) ] , [CrHpdta(H 0) ] H ,0 137
[CoBr2pn2] (H^) Br2 , [CoClgPn,,] (1^0,,) Cl2
[CrBr2pn2]Br H20 139
Ni(NCS)2(NH3)/+ 139
Cu(NH3),+S0it H20 l4l
Ni(NH3)gCl2 143
Tungsten and molybdenum organic complexes 144
Pt(NH2CH3)2I2 144
Complexes of methyl or ethyl—2—hydroxy-
methylpropanedlol-1,3 with boric acid ikk
XVI
12, Catalysts 145-149
Raney nickel 1 45
ZnO + Zii(PO^)2 146
Decomposition of CH^ catalyzed by nickel 147
Sorption of cumene vapour on NaY zeolite 149
Iron oxide + chromium oxide catalyst 149
13 Minerals 150-167
Goethite 150
Silurian graptolite sliale 151
Reactions between pyrlte and metal carbonates 152
Bauxite 152
Gibbsite 154
Effect of the griridin j on boehmite 157
Effect of the grinding 011 gibbsite 159
Formation of a-Al^O^ 159
Roasting of bauxites 160
Effect of the grinding on kaolinite 3 61
Montmorillonite l6l
Rehydration of clay minerals 162
Zeolites 163
Salt hydrate minerals 163
Clay minerals attacked by organic acids 165
Phosphate fertilizers 166
Talk-saponite regular mixed layer clay mineral 166
*14, Silicates 167-174
Examination of raw materials 167
Hydration of Portland cement 168
Retardation and acceleration of the
setting of cements 169
Determination of the type of cement 170
Carbonatization of portlandit in concrete 171
Demaging effect of m:i neral acids on concrete 171
Titanium dioxide-comaining enamels 172
» Mechanical properties of porcelain in
dependence on additiA es 172
Dilatation of glasses 173
15 Organic compounds 174-183
Thallium(l) salts of fatty acids 174
Nitrocellulose 177
XVII
l-oxy-2—diazo—naphthalene—5—sulphochloride 177
Polysaccharides 180
Vitamine B^2 181
Tetran 182
Estrone 182
Aminophenazonbarbiturate derival Ives 183
16 Plastics 184-194
Poly(vinyl chloride), poly(vinyJ acetate) 184
Reducing effect of iron compound 5 oil the
oxidation of polyamides 185
Poly(ethylene terephtlialate) 186
Polyolefins 186
Wander peak of PET 188
Polymerization of allyl esters initiated by
organic peroxides 189
Stabilization of PVC 190
Polyethylene 191
Insulating layer of foil film condensers 192
Varnish layer on enamel wires 192
Heat stability of polymer resins 193
Ageing of polymers 193
17 Biological applications 194-201
Changes taking place in proteins with
progress of age 194
Changes taking place in the tiss ies of
organs- of motion due to immobilanation 195
Changes taking place in proteins upon injury
and in the period of recovery 196
Atherosclerotic lesions 197
Kidney stones 197
Dental stones 200
Bone stones 200
18 Miscellaneous 202-210
Determination of the age of buri ?d bones 202 t
Loading ingredients for rubber 203
Sediment dust 204
Pb-PbO, 3Pb0 PbS0^ nH 0, pt)02 205
Mn02 + FeSi90, Mn02 + Pb 0^ 207
XVIII
Basic papers
List of publications
Subject index
|
| any_adam_object | 1 |
| author | Paulik, J. Paulik, Ferenc |
| author_facet | Paulik, J. Paulik, Ferenc |
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| dewey-full | 545/.4 543 |
| dewey-hundreds | 500 - Natural sciences and mathematics |
| dewey-ones | 545 - [Unassigned] 543 - Analytical chemistry |
| dewey-raw | 545/.4 543 |
| dewey-search | 545/.4 543 |
| dewey-sort | 3545 14 |
| dewey-tens | 540 - Chemistry and allied sciences |
| discipline | Chemie / Pharmazie |
| format | Book |
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| id | DE-604.BV001062295 |
| illustrated | Illustrated |
| indexdate | 2024-07-09T15:23:16Z |
| institution | BVB |
| isbn | 0444419497 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-000642817 |
| oclc_num | 7639050 |
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| owner_facet | DE-19 DE-BY-UBM DE-83 DE-188 DE-355 DE-BY-UBR |
| physical | XVIII, 277 S. Ill., graph. Darst. |
| publishDate | 1981 |
| publishDateSearch | 1981 |
| publishDateSort | 1981 |
| publisher | Elsevier |
| record_format | marc |
| series | Wilson and Wilson's comprehensive analytical chemistry |
| series2 | Wilson and Wilson's comprehensive analytical chemistry |
| spelling | Paulik, J. Verfasser aut Simultaneous thermoanalytical examinations by means of the derivatograph by J. Paulik and F. Paulik Amsterdam [u.a.] Elsevier 1981 XVIII, 277 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Wilson and Wilson's comprehensive analytical chemistry 12,A : Thermal analysis Literaturverz. S. 211 - 258 Analyse thermique ram Chimie analytique ram Thermogravimétrie ram Thermogravimetry Paulik, Ferenc Verfasser aut Wilson and Wilson's comprehensive analytical chemistry 12,A : Thermal analysis (DE-604)BV000900805 12,1 HEBIS Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=000642817&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Paulik, J. Paulik, Ferenc Simultaneous thermoanalytical examinations by means of the derivatograph Wilson and Wilson's comprehensive analytical chemistry Analyse thermique ram Chimie analytique ram Thermogravimétrie ram Thermogravimetry |
| title | Simultaneous thermoanalytical examinations by means of the derivatograph |
| title_auth | Simultaneous thermoanalytical examinations by means of the derivatograph |
| title_exact_search | Simultaneous thermoanalytical examinations by means of the derivatograph |
| title_full | Simultaneous thermoanalytical examinations by means of the derivatograph by J. Paulik and F. Paulik |
| title_fullStr | Simultaneous thermoanalytical examinations by means of the derivatograph by J. Paulik and F. Paulik |
| title_full_unstemmed | Simultaneous thermoanalytical examinations by means of the derivatograph by J. Paulik and F. Paulik |
| title_short | Simultaneous thermoanalytical examinations by means of the derivatograph |
| title_sort | simultaneous thermoanalytical examinations by means of the derivatograph |
| topic | Analyse thermique ram Chimie analytique ram Thermogravimétrie ram Thermogravimetry |
| topic_facet | Analyse thermique Chimie analytique Thermogravimétrie Thermogravimetry |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=000642817&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| volume_link | (DE-604)BV000900805 |
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