Nanostructuring of chemoresponsive hydrogels for sensing applications in microelectromechanical systems:
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| Main Author: | |
|---|---|
| Format: | Thesis Book |
| Language: | English |
| Published: |
München
Verlag Dr. Hut
2020
|
| Edition: | 1. Auflage |
| Series: | Verfahrenstechnik
|
| Subjects: | |
| Online Access: | Inhaltstext http://www.dr.hut-verlag.de/978-3-8439-4625-4.html Inhaltsverzeichnis |
| Physical Description: | XXIII, 157 Seiten Illustrationen, Diagramme 21 cm x 14.8 cm, 286 g |
| ISBN: | 9783843946254 3843946256 |
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Record in the Search Index
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| adam_text | Nanostructuring of Chemoresponsive Hydrogels
for Sensing Applications in
Microelectromechanical Systems
Dem Fachbereich Maschinenbau und Verfahrenstechnik
der Technischen Universität Kaiserslautern
zur Erlangung des akademischen Grades
Doktor-Ingenieur (Dr -Ing )
genehmigte,
’ Dissertation
von Herrn
Jutian Menges
aus Deidesheim
Dekan: Prof Dr -Ing Tilmann Beck
Prüfungskommission:
Prüfungsvorsitzender: Prof Dr rer nat Roland Ulber
1 Berichterstatter: Prof Dipl -Ing Dr techn Hans-Jörg Bart
2 Berichterstatter: Prof Dr Egbert Oesterschulze
Eingereicht am: 03 07 2020
Tag der mündlichen Prüfung: 09 10 2020
Kaiserslautern 2020
D386
Content
) Preface Vv
li) Abstract vi
1) Kurzfassung IX
IV) List of figures Xl
V) List of tables XX!
Vl) Nomenclature and abbreviations XXill
1 Motivation and aim 1
2 Introduction 3
2 1 Polymers and polymerization 3
211 Polymer properties 3
212 Polymerization 5
213 Copolymers 7
214 Rheology of polymer solutions 8
2 2 Hydrogels 9
221 Basic concepts and properties of hydrogels nmmmussonnsseconnennnenssssonssunessssnennunnee 9
222 Responsive hydrogels 9
223 Functional monomers in this WOrK sscesssssssssseesssssssseoussssesennassssseseeeessneessseeeeeeness i1
2 24 Molecular imprinted polymers (MIP) csssssssessssssrosssssscssrssssesessssssesssesesseteceesatseeaente 13
225 Hydrogel surface attachment and molecular brush amp;s „nennen 16
226 Macroinitiators and macromers 17
2 3 _Photolithography 19
231 General methods 19
232 Functional layer deposition 20
233 Reactive-ion dry etching 22
2 4 Photolithography of hydrogels/ microsensors
2 5 Muttiphoton lithography 26
26_ Micromechanical chemical microsensors «uunnsssssossesssneeeessssssssunennnensmnesssssssssenesennne 29
2 7 Hybrid bridge microresonator
271 Concept
272 Manufacturing procedure
275 Measuring setup
28 Surface modification
3 Molecular brushes
3 1 Molecular brushes on oxidic surfaces
3 2 Molecular brushes on gold
3 3 Application on microresonators
4 Hydrogels for spincoating applications
41 Challenges
42_ Macroinitiators,
453 Plasma dry etching
44 Screening of spincoating-solutions
441 Layer thickness:
442 Film morphology
45 Application on resonators
5 Hydrogel functionalized cantilever
5 1 Manufacturing
5 2 fon strength measurements
6 Direct laser writing (multiphoton lithography)
6 1 General approach to hydrogel resins
611 Choice of photoinitiator
612 Choice of monomers
6 2 Challenges and approaches
6 53 General synthesis
631 Synthesis of macromers
632 General preparation of prepolymer solutions
633 Sample preparation for DLW
6 4 — Polymerization of hydrogels OM reSOMAtOTS sssssseenseeesesecnnmnssseeseereennnetssensseeonets 79
641 Pretiminary experiment: 79
642 Laser setting screening 86
643 Polymerization of non-volatile solutions
644 Optimization of the primer solutions
6 5 Measurements
651 Measurement setup
652 Results
7 _FRAB experiments for molecular imprinted hydrogels nssssesmensenueneeemmnoentennmerrnee 115
8 Conclusion and future prospects 119
References 123
Appendix 143
A Materials and Methods 145
B Student Theses 151
C Publications, Presentations and Posters
D Curriculum Vitae 155
E Declaration of Authorship 157
ul
|
| adam_txt |
Nanostructuring of Chemoresponsive Hydrogels
for Sensing Applications in
Microelectromechanical Systems
Dem Fachbereich Maschinenbau und Verfahrenstechnik
der Technischen Universität Kaiserslautern
zur Erlangung des akademischen Grades
Doktor-Ingenieur (Dr -Ing )
genehmigte,
’ Dissertation
von Herrn
Jutian Menges
aus Deidesheim
Dekan: Prof Dr -Ing Tilmann Beck
Prüfungskommission:
Prüfungsvorsitzender: Prof Dr rer nat Roland Ulber
1 Berichterstatter: Prof Dipl -Ing Dr techn Hans-Jörg Bart
2 Berichterstatter: Prof Dr Egbert Oesterschulze
Eingereicht am: 03 07 2020
Tag der mündlichen Prüfung: 09 10 2020
Kaiserslautern 2020
D386
Content
) Preface Vv
li) Abstract vi
1) Kurzfassung IX
IV) List of figures Xl
V) List of tables XX!
Vl) Nomenclature and abbreviations XXill
1 Motivation and aim 1
2 Introduction 3
2 1 Polymers and polymerization 3
211 Polymer properties 3
212 Polymerization 5
213 Copolymers 7
214 Rheology of polymer solutions 8
2 2 Hydrogels 9
221 Basic concepts and properties of hydrogels nmmmussonnsseconnennnenssssonssunessssnennunnee 9
222 Responsive hydrogels 9
223 Functional monomers in this WOrK sscesssssssssseesssssssseoussssesennassssseseeeessneessseeeeeeness i1
2 24 Molecular imprinted polymers (MIP) csssssssessssssrosssssscssrssssesessssssesssesesseteceesatseeaente 13
225 Hydrogel surface attachment and molecular brush amp;s „nennen 16
226 Macroinitiators and macromers 17
2 3 _Photolithography 19
231 General methods 19
232 Functional layer deposition 20
233 Reactive-ion dry etching 22
2 4 Photolithography of hydrogels/ microsensors
2 5 Muttiphoton lithography 26
26_ Micromechanical chemical microsensors «uunnsssssossesssneeeessssssssunennnensmnesssssssssenesennne 29
2 7 Hybrid bridge microresonator
271 Concept
272 Manufacturing procedure
275 Measuring setup
28 Surface modification
3 Molecular brushes
3 1 Molecular brushes on oxidic surfaces
3 2 Molecular brushes on gold
3 3 Application on microresonators
4 Hydrogels for spincoating applications
41 Challenges
42_ Macroinitiators,
453 Plasma dry etching
44 Screening of spincoating-solutions
441 Layer thickness:
442 Film morphology
45 Application on resonators
5 Hydrogel functionalized cantilever
5 1 Manufacturing
5 2 fon strength measurements
6 Direct laser writing (multiphoton lithography)
6 1 General approach to hydrogel resins
611 Choice of photoinitiator
612 Choice of monomers
6 2 Challenges and approaches
6 53 General synthesis
631 Synthesis of macromers
632 General preparation of prepolymer solutions
633 Sample preparation for DLW
6 4 — Polymerization of hydrogels OM reSOMAtOTS sssssseenseeesesecnnmnssseeseereennnetssensseeonets 79
641 Pretiminary experiment: 79
642 Laser setting screening 86
643 Polymerization of non-volatile solutions
644 Optimization of the primer solutions
6 5 Measurements
651 Measurement setup
652 Results
7 _FRAB experiments for molecular imprinted hydrogels nssssesmensenueneeemmnoentennmerrnee 115
8 Conclusion and future prospects 119
References 123
Appendix 143
A Materials and Methods 145
B Student Theses 151
C Publications, Presentations and Posters
D Curriculum Vitae 155
E Declaration of Authorship 157
ul |
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| author | Menges, Julian 1989- |
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| author_facet | Menges, Julian 1989- |
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| building | Verbundindex |
| bvnumber | BV047148875 |
| classification_tum | CHE 713 |
| ctrlnum | (OCoLC)1238067367 (DE-599)DNB1224565827 |
| discipline | Chemie |
| discipline_str_mv | Chemie |
| edition | 1. Auflage |
| format | Thesis Book |
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| spelling | Menges, Julian 1989- Verfasser (DE-588)1237720613 aut Nanostructuring of chemoresponsive hydrogels for sensing applications in microelectromechanical systems Julian Menges 1. Auflage München Verlag Dr. Hut 2020 XXIII, 157 Seiten Illustrationen, Diagramme 21 cm x 14.8 cm, 286 g txt rdacontent n rdamedia nc rdacarrier Verfahrenstechnik Dissertation Technische Universität Kaiserslautern 2020 Hydrogel (DE-588)4160909-8 gnd rswk-swf Chemischer Sensor (DE-588)4259288-4 gnd rswk-swf Responsivität (DE-588)4395138-7 gnd rswk-swf MEMS (DE-588)4824724-8 gnd rswk-swf Chemical Sensors MEMS Responsive Hydrogels (DE-588)4113937-9 Hochschulschrift gnd-content MEMS (DE-588)4824724-8 s Chemischer Sensor (DE-588)4259288-4 s Responsivität (DE-588)4395138-7 s Hydrogel (DE-588)4160909-8 s DE-604 Verlag Dr. Hut (München) (DE-588)10174118-2 pbl X:MVB text/html http://deposit.dnb.de/cgi-bin/dokserv?id=df7c581aa54f4c778bf1a5eb0db48695&prov=M&dok_var=1&dok_ext=htm Inhaltstext X:MVB http://www.dr.hut-verlag.de/978-3-8439-4625-4.html HEBIS Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=032554654&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis 1\p vlb 20210106 DE-101 https://d-nb.info/provenance/plan#vlb |
| spellingShingle | Menges, Julian 1989- Nanostructuring of chemoresponsive hydrogels for sensing applications in microelectromechanical systems Hydrogel (DE-588)4160909-8 gnd Chemischer Sensor (DE-588)4259288-4 gnd Responsivität (DE-588)4395138-7 gnd MEMS (DE-588)4824724-8 gnd |
| subject_GND | (DE-588)4160909-8 (DE-588)4259288-4 (DE-588)4395138-7 (DE-588)4824724-8 (DE-588)4113937-9 |
| title | Nanostructuring of chemoresponsive hydrogels for sensing applications in microelectromechanical systems |
| title_auth | Nanostructuring of chemoresponsive hydrogels for sensing applications in microelectromechanical systems |
| title_exact_search | Nanostructuring of chemoresponsive hydrogels for sensing applications in microelectromechanical systems |
| title_exact_search_txtP | Nanostructuring of chemoresponsive hydrogels for sensing applications in microelectromechanical systems |
| title_full | Nanostructuring of chemoresponsive hydrogels for sensing applications in microelectromechanical systems Julian Menges |
| title_fullStr | Nanostructuring of chemoresponsive hydrogels for sensing applications in microelectromechanical systems Julian Menges |
| title_full_unstemmed | Nanostructuring of chemoresponsive hydrogels for sensing applications in microelectromechanical systems Julian Menges |
| title_short | Nanostructuring of chemoresponsive hydrogels for sensing applications in microelectromechanical systems |
| title_sort | nanostructuring of chemoresponsive hydrogels for sensing applications in microelectromechanical systems |
| topic | Hydrogel (DE-588)4160909-8 gnd Chemischer Sensor (DE-588)4259288-4 gnd Responsivität (DE-588)4395138-7 gnd MEMS (DE-588)4824724-8 gnd |
| topic_facet | Hydrogel Chemischer Sensor Responsivität MEMS Hochschulschrift |
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| work_keys_str_mv | AT mengesjulian nanostructuringofchemoresponsivehydrogelsforsensingapplicationsinmicroelectromechanicalsystems AT verlagdrhutmunchen nanostructuringofchemoresponsivehydrogelsforsensingapplicationsinmicroelectromechanicalsystems |