Methods of quantitative inorganic analysis: an encyclopedia of gravimetric, titrimetric and colorimetric methods
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| Format: | Book |
| Language: | English |
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New York [u.a.]
Interscience Publ.
1963
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| Online Access: | Inhaltsverzeichnis |
| Physical Description: | XIV, 507 S. graph. Darst. |
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| 100 | 1 | |a Kodama, Kazunobu |e Verfasser |4 aut | |
| 245 | 1 | 0 | |a Methods of quantitative inorganic analysis |b an encyclopedia of gravimetric, titrimetric and colorimetric methods |c Kazunobu Kodama |
| 264 | 1 | |a New York [u.a.] |b Interscience Publ. |c 1963 | |
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| _version_ | 1804122719027986432 |
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| adam_text | Methods of
QUANTITATIVE
INORGANIC
ANALYSIS
An Encyclopedia of Gravimetric, Titrimetric and
Colorimetric Methods
byKAZUNOBUKODAMA
Nagoya Municipal Industrial Research Institute
Nagoya, Japan
INTERSCIENCEPUBLISHERS
a division of John Wiley amp; Sons—New York—London
CONTENTS
PREFACE v
LIST OF ABBREVIATIONS USED x
PARTIGENERALCONSIDERATIONS
Chapter 1 Introduction
Chapter 2 General Procedures 6
1 The Sample 6
2 The Attack 6
2 1 H2O 6
2 2 Acids 6
2 3 Alkalies 8
2 4 Fluxes 8
2 5 Heating in gases 8
2 6 Organic compounds 9
3 Group separation by classical methods 9
3 1 Acids 10
32 H2S and its substitutes 11
33 NH4OH afid its substitutes 12
3 4 (NH4)2HP04 14
3 5 Organic reagents 15
4 Other methods of separation 15
Chapter 3 Gravimetry 16
1 Formation of precipitates 16
2 Separation of precipitates 16
2 1 Filtration 16
2 2 Centrifugation 17
2 3 Washing 17
3 Heating of precipitates 17
4 Cooling, weighing, and the conversion
factor 17
Chapter 4 Electrolytic Deposition
Chapter 5
Titrimetry
Introduction
Neutralization titrations
Primary standards
Neutralization indicators
Titrations involving precipitation or
complex-formation: argentimetry and
mercurimetry
Primary standards
Indicators
4 Titrations involving precipitation and
complex-formation: chelatometry 24
4 1 Reagents 24
4 2 Indicators 24
4 3 Titration of mixtures 30
5 Redox titrations 31
5 1 Redox potentials 31
5 2 Preliminary reduction 32
5 3 Preliminary oxidation 32
5 4 Primary standards 33
5 5 Redox indicators 33
6 Oxidation titrations 33
6 1 KMn04 titrations 33
6 2 Ce4+ titrations (cerimetry) 34
6 3 K2Cr207 titrations 34
6 4 Mn3+ titrations 34
6 5 NH4VO3 titrations 34
6 6 FeCl3 titrations 34
6 7 Methylene blue or thionine titrations 35
6 8 K3Fe(CN)„ titrations 35
6 9 Periodatocuprate titrations 35
6 10 Co3+ titrations 35
6 11 H202 titrations 35
6 12 Cu2+ titrations 35
7 Iodimetry and its analogs 35
7 1 Iodimetry 35
7 2 KIO3 titrations 36
7 3 KBr03 titrations 36
7 4 Chloramine T titrations 36
7 5 NaOCl or Ca(OCl)2 titrations 36
7 6 Br2 (Manchot s method) or NaOBr
titrations 37
7 7 KCIO3 titrations 37
7 8 NaC102 or Ca(C102)2 titrations 37
7 9 ICI3 titrations 37
7 10 IC1 titrations 37
7 11 C102 titrations 37
7 12 KIO4 titrations 37
8 Reduction titrations 37
8 1 Ti3+ titrations 37
8 2 Cr2+ titrations 37
8 3 Fe2+ titrations 37
viiiC ON TEN TS
; 4 Sn2+ titrations 37 8 12 N2H4-H2S04 titrations 38
1 5 As3+ titrations 37 8 13 Ascorbic acid titrations 38
i 6 Cu+ titrations 37 8 14 Hydroquinone and other org titrants 38
; 7 V4+, V3 + and V2+ titrations 33 8 15 Na2S203 titrations 38
: 8 W3+ and W5+ titrations 33 9 Instrumental methods of end-point
; 9 Mo5+ and Mo3+ titrations 33 detection 38
10 U4+ titrations 33
: n Hg2(N03)2 titrations 33 Chapter 6 Optical Methods 41
PARTIIORGANICREAGENTSININORGANICANALYSIS
Chapter 7 Introduction
Chapter 8 Reagents Forming Inner Complexes
1 Compounds containing N and —OH,
—COOH, =CO, —CHO
1 1 Oxine
1 2 Derivatives and analogs of oxine
1 3 Salicylimine and its analogs
1 4 a-Dioximes
1 5 Cupron and salicylaldoxime analogs
1 6 Oximes contg additional N atoms
1 7 Hydroxamic acids
1 8 Miscellaneous oximes
1 9 Nitroso compounds
1 10 Cupferron and its analogs
1 11 Quinaldic acid and its analogs
1 12 Anthranilic acid and its derivatives
1 13 Aminopolycarboxylic acids
1 14 Miscellaneous compounds containing
N and —COOH groups
1 15 Urea derivs contg the =CO group
1 16 Miscellaneous compounds
2 Compounds containing S
2 1 Rhodanine and its derivs
2 2 Thiourea and its derivs
2 3 Dithizone and its analogs
2 4 Thiazole derivatives and analogs
2 5 Miscellaneous compds contg S and N
2 6 Thioglycolic acid and its derivatives
2 7 Miscellaneous carboxylic acids con
taining S
2 8 Thioacid derivatives
2 9 Thiols
2 10 Miscellaneous compounds
Chapter 9 Nitrogen Compounds
1 o-Phenanthroline and its analogs
2 Miscellaneous nitrogen compounds
Chapter 10 Hydroxy Compounds
1 Compounds forming complexes mainly
with Fe, Ti, or Cu
1 1 Aromatic compounds
1 2 Aliphatic compounds
2 /?-Diketones
3 Compounds forming esters with boric
or germanic acid
5
5 !
5;i
5:i
5 )
6 (
6 !
6:i
Chapter 11 Acids Forming Sparingly Soluble Salts 86
1 With mainly Group 1V and V elements 86
1 1 With mainly Group V elements 86
1 2 Polyhydroxy acids 87
1 3 Miscellaneous compounds 87
2 Carboxylic acids selective for Th, Zr,
etc 88
3 Arsonic, phosphonic, sulfinic, seleninic
acids 88
3 1 Arsonic acids 88
3 2 Phosphonic and phosphinic acids 90
3 3 Sulfinic and seleninic acids 90
Chapter 12 Adsorption Compounds and Miscellaneous
Complexes 92
1 Tannin 92
2 Anthraquinone derivatives and analogs 92
3 Other polyhydroxy compounds 94
4 Azo and other nitrogen-containing
compounds 95
4 1 o-Hydroxy monoazo compounds 95
4 2 Other azo dyes 97
4 3 Reagents for B and Ge 97
4 4 Other reagents for Mg 98
4 5 Gallocyanine and resorufin 98
5 Phthalein analogs 98
6 Adsorption indicators 99
Chapter 13 Ion Exchange Resins and Cellulose
Columns 101
6N 1 Ion exchange resins 101
6N 1 1 General remarks 101
71 1 2 Experimental techniques 104
71 1 3 Factors affecting separation 104
75 1 4 Applications in inorg analysis 105
75 2 Simple separations 105
! ( • 2 1 Cationites 105 ! ( •
2 2 Anionites 108
82 2 3 Combined uses 112
3 Concentration 113
82 4 Separation of similar ions 113
82 4 1 Lanthanides 113
83 4 2 Actinides 114
83 4 3 Polyvalent ions such as Ti, Zr, Hf, Nb,
Ta- 114
84 4 4 Other ions 115
C ON TENTS ix
5 Other uses 116
6 Cellulose columns 116
Chapter 14 Compounds Forming Precipitates with
Anions 122
1 Precipitants for NOj, ReOj, F-, etc 122
2 Precipitants for SO|~, WOphospho-
or silico-molybdic acid 123
Chapter IS Redox Reactions 125
1 Reactions with oxidants 125
2 Strong reductants 130
3 Compounds reacting with reductants 131
4 Redox indicators 131
4 1 Ferroin and its analogs 131
4 2 Diphenylamine and its derivatives and
analogs 132
4 3 Dyes 133
4 4 Miscellaneous indicators 134
Chapter 16 Solvents for Extraction 135
Chapter 17 Miscellaneous Reagents 141
1 Miscellaneous reactions 141
1 1 Detection and colorimetric determin
ation of NH3 141
1 2 Detection of S and S compounds 141
1 3 Detection of As and Sb 141
1 4 Detection and determination of other
metals 141
1 5 Detection of halogens and pseudo-
halogens 1 141
1 6 Reactions with H20 142
1 7 Others 142
2 Protective colloids and coagulating
agents 142
3 Other reagents 142
PARTIIIDETERMIN
Hydrogen Sulfide Group
Ag, Hg, Pb, Bi, Cu, Cd, Re; As, Sb, Sn, Ge, Mo,
Se, Te; Au, Ru, Rh, Pd, Os, Ir, Pt
I ELEMENTS FORMING SULFIDES INSOLUBLE IN
ACID amp; AND ALKALI SULFIDES
Ag, Hg, Pb, Bi, Cu, Cd, Re (and Ru, Rh, Pd, Os)
Chapter 18 Silver 145
Attack 145
Fire assay 145
Separation 145
Determination 146
Chapter 19 Mercury 150
Attack 150
Separation 150
Determination 151
Chapter 20 Lead 157
Attack 157
Separation 157
Determination 158
Chapter 21 Bismuth 165
Attack 165
Separation 165
Determination 165
Chapter 22 Copper 172
Attack 172
TIONOFELEMENTS
Separation 172
Determination 173
Chapter 23 Cadmium 184
Attack 184
Separation 184
Determination 184
Chapter 24 Rhenium 189
AtUick 189
Separation 189
Determination 190
II ELEMENTS FORMING SULFIDES INSOLUBLE IN
ACIDS BUT SOLUBLE IN ALKALI SULFIDES
As, Sb, Sn, Ge, Mo, Se, Te (and Au, Pt, Ir)
Chapter 25 Arsenic 192
Attack 192
Separation 192
Determination 193
Chapter 26 Antimony 198
Attack 198
Separation 198
Determination 199
Chapter 27 Tin 203
Attack • 203
Separation 203
Determination 204
X C ON TEN TS
Chapter 28 Germanium
Attack
Separation
Determination
Chapter 29 Molybdenum
Attack
Separation
Determination
Chapter 30 Selenium and Tellurium
Attack
Separation
Determination: Selenium
Tellurium
III NOBLE METALS
Au, Ru, Rh, Pd, Os, Ir, Pt
Chapter 31 Gold
Attack
Fire assay
Wet assay
Separation
Concentration
Determination
209 Chapter 35 Cobalt
209 Attack
209 Separation
210 Determination
Chapter 32 Platinum Metals 231
Attack 231
Fire assay 231
Separation 232:
Schemes for the separation and determination
of platinous metals 234
Determination: Osmium 236
Ruthenium 239
Platinum 241
Palladium 242
Rhenium 246
Iridium 248
Chapter 36 Zinc
Attack
Separation
Determination
Chapter 37 Manganese
Attack
Separation
Determination
Chapter 38 Vanadium
Attack
Separation
Determination
Chapter 39 Uranium
Attack
Separation
Determination
Chapter 40 Thallium
Attack
Separation
Determination
Chapter 41 Indium
Attack
Separation
Determination
Ammonium Sulfide Group
Fe, Ni, Co, Zn, Mn, V, U, TI, In, Ga; Al, Be,
Cr, Th, Sc
Rare earth elements, Zr, Hf, Ti, Nb, Ta
I ELEMENTS FORMING SULFIDES SOLUBLE IN ACIDS
Fe, Ni, Co, Zn, Mn, V, U, TI, In, Ga
Chapter 33 Iron
Attack
Separation
Determination
Chapter 34 Nickel
Separation
Determination
Chapter 42 Gallium
Attack
Separation
Determination
II ELEMENTS FORMING HYDROXIDES OR BASIC
COMPOUNDS
Al, Be, Cr, Th, Sc, rare earth elements, Zr, Hf,
Ti, Nb, Ta
Chapter 43 Aluminum
Attack
Separation
Determination
CONTENTS xi
Alkaline Earth Metals and Magnesium
Ca, Sr, Ba, Mg
Chapter 44 Beryllium 325
Attack 325
Separation 325
Concentration 326
Determination 327
Chapter 45 Chromium 331
Attack 331
Separation 332
Determination 332
Chapter 46 Thorium 337
Attack 337
Separation 337
Determination 339
Chapter 47 Scandium 344
Attack 344
Separation 344
Determination 345
Chapter 48 Rare Earth Elements 347
Attack 348
Separation 348
Determination: Cerium 349
Total amount of other rare
earth metals 351
Separation into Cerium and
Yttrium groups 351
Europium 352
Ytterbium 352
Praseodymium, Neodymium,
Samarium, Europium, Gado
linium, Ytterbium, the Erbium
group 352
Lanthanum 352
Neodymium 352
Terbium 352
Praseodymium 352
Chapter 49 Zirconium and Hafnium 354
Attack 354
Separation 354
Determination 355
Chapter 50 Titanium 360
Attack 360
Separation 360
Determination 361
Chapter 51 Niobium and Tantalum 365
Attack 365
Separation 373
Determination 378
Chapter 52 Alkaline Earth Metals 385
Attack 385
Separation 385
Determination: Calcium 388
Strontium 391
Barium 392
Chapter 53 Magnesium 396
Attack 396
Separation 396
Determination 396
Alkali Metals
Li, Na, K, Rb, Cs
Chapter 54 Alkali Metals 401
Attack 401
Separation 402
Determination: Lithium 404
Sodium 407
Potassium 408
Rubidium and Cesium 411
Acid-forming Elements
Si, W, P, S, CI, Br, I, F, B, C, H, N
Chapter 55 Silicon 415
Attack 415
Separation 416
Determination 416
Chapter 56 Tungsten 420
Attack 420
Separation 420
Determination 422
Chapter 57 Phosphorus 426
Attack 426
Separation 426
Determination 427
Chapter 58 Sulfur 434
Attack 434
Separation 435
Determination 435
xii C ON TEN TS
Chapter 59 Chlorine, Bromine and Iodine 440
Attack 440
Separation 440
Concentration 441
Determination: Chlorine 44 [
Bromine 445
Iodine 444
Chapter 60 Fluorine 44 3
Attack 443
Separation 443
Determination 44 )
Chapter 61 Boron 45(3
Attack 456
Separation 456
Determination 457
Chapter 62 Carbon and Hydrogen 460
Attack 460
Determination: Carbon 460
Hydrogen 461
Chapter 63 Nitrogen 462
Ammonium 462
Nitrate 463
Nitrite 466
Cyanide 467
General Index 471
Organic Reagent Index 485
t
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| illustrated | Illustrated |
| indexdate | 2024-07-09T17:18:20Z |
| institution | BVB |
| language | English |
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| spelling | Kodama, Kazunobu Verfasser aut Methods of quantitative inorganic analysis an encyclopedia of gravimetric, titrimetric and colorimetric methods Kazunobu Kodama New York [u.a.] Interscience Publ. 1963 XIV, 507 S. graph. Darst. txt rdacontent n rdamedia nc rdacarrier Chemistry, Analytic Quantitative Encyclopedias Chemistry, Inorganic Encyclopedias Quantitative Analyse (DE-588)4125311-5 gnd rswk-swf Chemie (DE-588)4009816-3 gnd rswk-swf Quantitative Analyse (DE-588)4125311-5 s Chemie (DE-588)4009816-3 s DE-604 HEBIS Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=005499864&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Kodama, Kazunobu Methods of quantitative inorganic analysis an encyclopedia of gravimetric, titrimetric and colorimetric methods Chemistry, Analytic Quantitative Encyclopedias Chemistry, Inorganic Encyclopedias Quantitative Analyse (DE-588)4125311-5 gnd Chemie (DE-588)4009816-3 gnd |
| subject_GND | (DE-588)4125311-5 (DE-588)4009816-3 |
| title | Methods of quantitative inorganic analysis an encyclopedia of gravimetric, titrimetric and colorimetric methods |
| title_auth | Methods of quantitative inorganic analysis an encyclopedia of gravimetric, titrimetric and colorimetric methods |
| title_exact_search | Methods of quantitative inorganic analysis an encyclopedia of gravimetric, titrimetric and colorimetric methods |
| title_full | Methods of quantitative inorganic analysis an encyclopedia of gravimetric, titrimetric and colorimetric methods Kazunobu Kodama |
| title_fullStr | Methods of quantitative inorganic analysis an encyclopedia of gravimetric, titrimetric and colorimetric methods Kazunobu Kodama |
| title_full_unstemmed | Methods of quantitative inorganic analysis an encyclopedia of gravimetric, titrimetric and colorimetric methods Kazunobu Kodama |
| title_short | Methods of quantitative inorganic analysis |
| title_sort | methods of quantitative inorganic analysis an encyclopedia of gravimetric titrimetric and colorimetric methods |
| title_sub | an encyclopedia of gravimetric, titrimetric and colorimetric methods |
| topic | Chemistry, Analytic Quantitative Encyclopedias Chemistry, Inorganic Encyclopedias Quantitative Analyse (DE-588)4125311-5 gnd Chemie (DE-588)4009816-3 gnd |
| topic_facet | Chemistry, Analytic Quantitative Encyclopedias Chemistry, Inorganic Encyclopedias Quantitative Analyse Chemie |
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