Sulphonyl azide dyes for dyeing in supercritical carbon dioxide: synthesis, properties and application
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
1999
|
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | Dresden, Techn. Univ., Diss., 1999 |
| Beschreibung: | 165 S. graph. Darst. : 21 cm |
Internformat
MARC
| LEADER | 00000nam a2200000 c 4500 | ||
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| 001 | BV013665776 | ||
| 003 | DE-604 | ||
| 007 | t | ||
| 008 | 010327s1999 gw d||| m||| 00||| eng d | ||
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| 035 | |a (OCoLC)247577984 | ||
| 035 | |a (DE-599)BVBBV013665776 | ||
| 040 | |a DE-604 |b ger |e rakddb | ||
| 041 | 0 | |a eng | |
| 044 | |a gw |c DE | ||
| 049 | |a DE-29T | ||
| 100 | 1 | |a Hudson, Andrew |d 1971- |e Verfasser |0 (DE-588)12139123X |4 aut | |
| 245 | 1 | 0 | |a Sulphonyl azide dyes for dyeing in supercritical carbon dioxide |b synthesis, properties and application |c von Hudson, Andrew |
| 264 | 1 | |c 1999 | |
| 300 | |a 165 S. |b graph. Darst. : 21 cm | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 500 | |a Dresden, Techn. Univ., Diss., 1999 | ||
| 650 | 0 | 7 | |a Kohlendioxid |0 (DE-588)4031648-8 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Azide |0 (DE-588)4143789-5 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Farbstoff |0 (DE-588)4016465-2 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Überkritischer Zustand |0 (DE-588)4186602-2 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Sulfonylgruppe |0 (DE-588)4184062-8 |2 gnd |9 rswk-swf |
| 655 | 7 | |0 (DE-588)4113937-9 |a Hochschulschrift |2 gnd-content | |
| 689 | 0 | 0 | |a Farbstoff |0 (DE-588)4016465-2 |D s |
| 689 | 0 | 1 | |a Azide |0 (DE-588)4143789-5 |D s |
| 689 | 0 | 2 | |a Sulfonylgruppe |0 (DE-588)4184062-8 |D s |
| 689 | 0 | 3 | |a Kohlendioxid |0 (DE-588)4031648-8 |D s |
| 689 | 0 | 4 | |a Überkritischer Zustand |0 (DE-588)4186602-2 |D s |
| 689 | 0 | |5 DE-604 | |
| 856 | 4 | 2 | |m DNB Datenaustausch |q application/pdf |u http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=009338138&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |3 Inhaltsverzeichnis |
| 943 | 1 | |a oai:aleph.bib-bvb.de:BVB01-009338138 | |
Datensatz im Suchindex
| _version_ | 1807504932139433984 |
|---|---|
| adam_text |
1.
INTRODUCTION
AND
AIMS
1
1.1
INTRODUCTION
1
1.2
AIM
4
2.
THEORETICAL
SECTION
6
2.1
THE
DYEING
PROCESS
6
2.1.1
THE
DYEING
MECHANISM
6
2.1.2
DYEING
THERMODYNAMICS
AND
KINETICS
12
2.1.2.1
DYEING EQUILIBRIUM
12
2.1.2.2
DYEING
KINETICS
17
2.1.3
FACTORS
WHICH
AFFECT
THE
DYEING
19
2.1.3.1
DYE
INFLUENCE
ON
THE
DYEING
19
2.1.3.2
DYEING
MEDIUM
20
2.1.3.3
FIBRE
INFLUENCE
21
2.2
STRUCTURE-DYEABILITY-RELATIONS
FOR
SOME
HYDROPHOBIC
FIBRES
22
2.2.1
POLYETHYLENE
TEREPHTHALATE
23
22.2
POLYPROPYLENE
27
22.3
POLYAMIDE
6.6
29
2.3
SULPHONYL
AZIDES AS
POTENTIAL
REACTIVE
DYES
33
2.3.1
FORMATION,
PROPERTIES
AND
DECOMPOSITION
OF
SULPHONYL
33
AZIDES
23.2
FORMATION,
PROPERTIES
AND
REACTIONS
OF
SULPHONYLNITRENES
37
23.3
COLOURED
SULPHONYL
AZIDES
40
2.4
SUPERCRITICAL
FLUIDS,
IN
PARTICULAR
CARBON
DIOXIDE
44
2.4.1
PHASE
BEHAVIOUR
OF
CARBON
DIOXIDE
44
2.4.2
PHASE
DIAGRAM
FOR
A
TYPICAL
BINARY
SYSTEM
46
2.4.3
SOLVENT
POWER
AND
RATES
OF
MASS
TRANSFER
48
2.4.4
DYEING
IN
SUPERCRITICAL
CARBON
DIOXIDE
50
2.4.4.1
DYE
CLASS
50
2.4.4.2
FIBRE
CLASSES
52
2.4.4.3
PARAMETER
EFFECTS
IN
SUPERCRITICAL
DYEING
55
2.4.5
ADVANTAGES
OF
DYEING
IN
CCH
57
3
RESULTS
AND
DISCUSSION
59
3.1
SULPHONYL
AZIDE
DYES
59
3.1.1
SYNTHESIS
59
3.1.1.1
AZO
DYES
61
3.1.1.2
ANTHRAQUINONE
AND
INDIGOIDE
DYES
64
3.1.2
CHARACTERISATION
66
3.1.2.1
VIS
ABSORPTION
DATA
67
3.1.2.2
EXPLOSIVITY
TESTS
70
3.1.2.3
LIPOPHILICITY
71
3.1.2.4
D.S.C
DATA
73
3.1.2.5
THERMAL
STABILITY
OF
THE
SULPHONYL
AZIDE
GROUP
IN
SUPERCRITICAL
CO2
76
3.1.2.6
STABILITY
TO
HYDROLYSIS
UNDER
SUPERCRITICAL
CONDITIONS
80
3.2
DYEINGS FROM
SUPERCRITICAL
CARBON
DIOXIDE
81
3.2.1
DYEING
OF
PETP
81
3.2.1.1
DYE
SCREENING
81
3.2.1.2
DYE
UPTAKE
UNDER
EQUILIBRIUM
CONDITIONS
85
3.2.1.3
DEGREES
OF
COVALENT
BOND
FORMATION
OF
THE
DYE
WITH
THE
FIBRE
101
3.2.1.4
FASTNESS
PROPERTIES
106
3.2.2
DYEING
OF
PA 6.6
108
3.2.3
DYEING
OF
PP
110
3.3
ABSORPTION
MAXIMA
OF
THE
DYED
MATERIALS
113
3.4 TYPE
OF
FIBRE-DYE
BOND
114
4
EXPERIMENTAL
PART
118
4.1
MATERIALS
USED
118
4.1.1
CHEMICALS
AND
SOLVENTS
118
4.1.2
FIBRES
119
4.1.3
DYES
120
4.1.3.1
DYES
FROM
DIAZOTISED
4-AMINOPHENYLSULPHONYLAZIDE
AND
M-SULPHONYLAZIDO-4-METHOXYOXYANILINE
120
4.1.3.2
DYES
FROM
ACID
AND
DIRECT
DYES
128
4.1.3.3
OTHER
DYES
133
4.2
DYE
CHARACTERISATION
140
4.2.1
THIN
LAYER
CHROMATOGRAPHY
140
4.2.2
VIS
MEASUREMENTS
140
4.2.3
EXPLOSIVITY TESTS
140
4.2.4
LIPOPHILICITY
141
4.2.5
DSC
MEASUREMENTS
141
4.2.6
STABILITY
OF
THE
SULPHONYL
AZIDE
GROUP
TOWARDS
HYDROLYSIS
141
4.2.7
THERMAL
STABILITY
OF
THE
SULPHONYL
AZIDE
GROUP
YY
142
4.3
DYEING
INVESTIGATIONS
143
4.3.1
THE
DYEING
APPARATUS
143
4.3.2
MEASUREMENT
OF
DYEBATH
EXHAUSTION
144
4.3.3
THERMODYNAMIC
PARAMETERS
145
4.3.4
DEGREES
OF
COVALENT
BOND
FORMATION
OF
DIE
DYE
WITH
THE
FIBRE
146
4.3.5
FASTNESS
PROPERTIES
147
4.3.6
IRRADIATION
OF
POLYPROPYLENE
147
4.3.7
DYEING
OF
POLYPROPYLENE
147
4.3.8
DYEING
OF
POLYAMIDE
148
4.3.9
TYPE
OF
POLYMER-DYE
BOND
148
5.
CONCLUSIONS
150
6.
LITERATURE
159 |
| any_adam_object | 1 |
| author | Hudson, Andrew 1971- |
| author_GND | (DE-588)12139123X |
| author_facet | Hudson, Andrew 1971- |
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| genre | (DE-588)4113937-9 Hochschulschrift gnd-content |
| genre_facet | Hochschulschrift |
| id | DE-604.BV013665776 |
| illustrated | Illustrated |
| indexdate | 2024-08-16T01:17:09Z |
| institution | BVB |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-009338138 |
| oclc_num | 247577984 |
| open_access_boolean | |
| owner | DE-29T |
| owner_facet | DE-29T |
| physical | 165 S. graph. Darst. : 21 cm |
| publishDate | 1999 |
| publishDateSearch | 1999 |
| publishDateSort | 1999 |
| record_format | marc |
| spelling | Hudson, Andrew 1971- Verfasser (DE-588)12139123X aut Sulphonyl azide dyes for dyeing in supercritical carbon dioxide synthesis, properties and application von Hudson, Andrew 1999 165 S. graph. Darst. : 21 cm txt rdacontent n rdamedia nc rdacarrier Dresden, Techn. Univ., Diss., 1999 Kohlendioxid (DE-588)4031648-8 gnd rswk-swf Azide (DE-588)4143789-5 gnd rswk-swf Farbstoff (DE-588)4016465-2 gnd rswk-swf Überkritischer Zustand (DE-588)4186602-2 gnd rswk-swf Sulfonylgruppe (DE-588)4184062-8 gnd rswk-swf (DE-588)4113937-9 Hochschulschrift gnd-content Farbstoff (DE-588)4016465-2 s Azide (DE-588)4143789-5 s Sulfonylgruppe (DE-588)4184062-8 s Kohlendioxid (DE-588)4031648-8 s Überkritischer Zustand (DE-588)4186602-2 s DE-604 DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=009338138&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Hudson, Andrew 1971- Sulphonyl azide dyes for dyeing in supercritical carbon dioxide synthesis, properties and application Kohlendioxid (DE-588)4031648-8 gnd Azide (DE-588)4143789-5 gnd Farbstoff (DE-588)4016465-2 gnd Überkritischer Zustand (DE-588)4186602-2 gnd Sulfonylgruppe (DE-588)4184062-8 gnd |
| subject_GND | (DE-588)4031648-8 (DE-588)4143789-5 (DE-588)4016465-2 (DE-588)4186602-2 (DE-588)4184062-8 (DE-588)4113937-9 |
| title | Sulphonyl azide dyes for dyeing in supercritical carbon dioxide synthesis, properties and application |
| title_auth | Sulphonyl azide dyes for dyeing in supercritical carbon dioxide synthesis, properties and application |
| title_exact_search | Sulphonyl azide dyes for dyeing in supercritical carbon dioxide synthesis, properties and application |
| title_full | Sulphonyl azide dyes for dyeing in supercritical carbon dioxide synthesis, properties and application von Hudson, Andrew |
| title_fullStr | Sulphonyl azide dyes for dyeing in supercritical carbon dioxide synthesis, properties and application von Hudson, Andrew |
| title_full_unstemmed | Sulphonyl azide dyes for dyeing in supercritical carbon dioxide synthesis, properties and application von Hudson, Andrew |
| title_short | Sulphonyl azide dyes for dyeing in supercritical carbon dioxide |
| title_sort | sulphonyl azide dyes for dyeing in supercritical carbon dioxide synthesis properties and application |
| title_sub | synthesis, properties and application |
| topic | Kohlendioxid (DE-588)4031648-8 gnd Azide (DE-588)4143789-5 gnd Farbstoff (DE-588)4016465-2 gnd Überkritischer Zustand (DE-588)4186602-2 gnd Sulfonylgruppe (DE-588)4184062-8 gnd |
| topic_facet | Kohlendioxid Azide Farbstoff Überkritischer Zustand Sulfonylgruppe Hochschulschrift |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=009338138&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT hudsonandrew sulphonylazidedyesfordyeinginsupercriticalcarbondioxidesynthesispropertiesandapplication |