Thermo-mechanical properties of mixed ion electron conducting membrane materials:
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| 1. Verfasser: | |
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| Format: | Abschlussarbeit Buch |
| Sprache: | English |
| Veröffentlicht: |
Jülich
Forschungszentrum, Zentralbibliothek
2011
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| Schriftenreihe: | Schriften des Forschungszentrums Jülich
Reihe Energie & Umwelt ; Bd. 124 |
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | 130 S. Ill., graph. Darst. 24 cm |
| ISBN: | 9783893367467 |
Internformat
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Datensatz im Suchindex
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|---|---|
| adam_text | IMAGE 1
TABLE OF CONTENTS
INTRODUCTION 4
1. LITERATURE REVIEW 6
1.1 TRANSPORT MECHANISMS 6
1.2 PEROVSKITES AND K 2NIF4 STRUCTURED MATERIAL 7
1.2.1 BA 0.5SRO.5COO.,FEO.20M (BSCF) 9
1.2.2 LAOASRO.4COOJ.FEO.2OW (LSCF) 10
1.2.3 OXYGEN PERMEATION FLUX DATA FOR PEROVSKITES 12
1.2.4 LA 2NI04+6 (LNO) 13
1.2.5 OXYGEN PERMEATION OF BSCF, LSCF AND LNO 15
1.3 THERMAL AND CHEMICAL EXPANSION 16
1.4 SPIN TRANSITION 22
1.5 FRACTURE STRESS, FRACTURE TOUGHNESS AND YOUNG S MODULUS 22
1.6 CREEP 30
2. EXPERIMENTS 34
2.1 BSCF AND LSCF PEROVSKITES 34
2.1.1 RING-ON-RING TESTS 35
2.1.2 MICRO-INDENTATION 36
2.1.3 X-RAY DIFFRACTION 39
2.1.4 THERMAL PROPERTY CHARACTERIZATION 40
2.1.5 TRANSMISSION ELECTRON MICROSCOPY 40
2.1.6 CREEP TESTS 40
2.2 EXPERIMENTS WITH LA 2NIO4*6 (LNO) 41
2.2.1 FOUR POINT BENDING TESTS 42
2.2.2 COMPLEMENTARY CHARACTERIZATIONS 43
3. RESULTS AND DISCUSSION 44
3.1 BSCF 44
3.1.1 YOUNG S MODULUS AND FRACTURE STRESS 44
BIBLIOGRAFISCHE INFORMATIONEN HTTP://D-NB.INFO/1019095709
DIGITALISIERT DURCH
IMAGE 2
3.1.2 INDENTATION RESULTS 47
3.1.3 COMPARISON OF YOUNG S MODULUS, FRACTURE STRESS AND FRACTURE
TOUGHNESS 55
3.1.4 FRACTURE SURFACES 57
3.1.5 DISCUSSION OF POSSIBLE MECHANISMS GOVERNING THE MECHANICAL ANOMALY
59
3.1.5.1 STRUCTURAL CHARACTERIZATION WITH XRD 60
3.1.5.2 PHASE STABILITY AT HIGH TEMPERATURES 61
3.1.5.3 ASSOCIATION AND DISSOCIATION OF DEFECTS 65
3.1.5.4 SPIN TRANSITION 66
3.1.5.5 THERMAL AND CHEMICAL EXPANSION 68
3.2 LSCF 70
3.2.1 NON-LINEARITY OF LOAD-DISPLACEMENT 70
3.2.2 YOUNG S MODULUS 72
3.2.2.1 YOUNG S MODULUS IN AIR 72
3.2.2.2 YOUNG S MODULUS UNDER VACUUM (10 S MBAR) 73
3.2.3 PHASE COMPOSITIONS OF LSCF 75
3.2.4 DTA/TG 77
3.2.5 THERMAL AND CHEMICAL EXPANSION 79
3.2.6 DOMAIN STRUCTURE OF LSCF 80
3.2.7 FRACTURE STRESS 84
3.2.8 INDENTATION 86
3.2.8.1 TEMPERATURE DEPENDENCE 86
3.2.8.2 COOLING RATE DEPENDENCE 87
3.2.9 MAGNETIC SUSCEPTIBILITY 90
3.2.10 RESIDUAL STRESSES 90
3.2.11 FRACTURE SURFACE 91
3.2.12 CREEP 94
3.3 LNO 99
3.3.1 STIFFNESS OF LNO 99
2
IMAGE 3
3.3.2 FRACTURE STRESS 101
3.3.3 TG/DTA 102
4. CONCLUSIONS 104
4.1 BSCF 104
4.2 LSCF 105
4.3 LNO 106
4.4 COMPARISON OF BSCF, LSCF AND LNO 106
REFERENCES 110
LIST OF FIGURES 121
LIST OF TABLES 125
NOMENCLATURE 126
ACKNOWLEDGEMENTS 129
LIST OF PUBLICATIONS 130
|
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| author | Huang, Bingxin |
| author_facet | Huang, Bingxin |
| author_role | aut |
| author_sort | Huang, Bingxin |
| author_variant | b h bh |
| building | Verbundindex |
| bvnumber | BV039867184 |
| ctrlnum | (OCoLC)780109003 (DE-599)DNB1019095709 |
| dewey-full | 620.198 |
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| dewey-ones | 620 - Engineering and allied operations |
| dewey-raw | 620.198 |
| dewey-search | 620.198 |
| dewey-sort | 3620.198 |
| dewey-tens | 620 - Engineering and allied operations |
| discipline | Maschinenbau / Maschinenwesen |
| format | Thesis Book |
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| id | DE-604.BV039867184 |
| illustrated | Illustrated |
| indexdate | 2024-07-10T00:13:00Z |
| institution | BVB |
| isbn | 9783893367467 |
| language | English |
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| physical | 130 S. Ill., graph. Darst. 24 cm |
| publishDate | 2011 |
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| series | Schriften des Forschungszentrums Jülich |
| series2 | Schriften des Forschungszentrums Jülich : Reihe Energie & Umwelt |
| spelling | Huang, Bingxin Verfasser aut Thermo-mechanical properties of mixed ion electron conducting membrane materials Bingxin Huang. Forschungszentrum Jülich GmbH, Institute of Energy and Climate Research (IEK), Microstructure and Properties of Materials (IEK-2) Jülich Forschungszentrum, Zentralbibliothek 2011 130 S. Ill., graph. Darst. 24 cm txt rdacontent n rdamedia nc rdacarrier Schriften des Forschungszentrums Jülich : Reihe Energie & Umwelt Bd. 124 Zugl.: Aachen, Techn. Hochsch., Diss., 2010 (DE-588)4113937-9 Hochschulschrift gnd-content Schriften des Forschungszentrums Jülich Reihe Energie & Umwelt ; Bd. 124 (DE-604)BV023393979 124 DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=024726599&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Huang, Bingxin Thermo-mechanical properties of mixed ion electron conducting membrane materials Schriften des Forschungszentrums Jülich |
| subject_GND | (DE-588)4113937-9 |
| title | Thermo-mechanical properties of mixed ion electron conducting membrane materials |
| title_auth | Thermo-mechanical properties of mixed ion electron conducting membrane materials |
| title_exact_search | Thermo-mechanical properties of mixed ion electron conducting membrane materials |
| title_full | Thermo-mechanical properties of mixed ion electron conducting membrane materials Bingxin Huang. Forschungszentrum Jülich GmbH, Institute of Energy and Climate Research (IEK), Microstructure and Properties of Materials (IEK-2) |
| title_fullStr | Thermo-mechanical properties of mixed ion electron conducting membrane materials Bingxin Huang. Forschungszentrum Jülich GmbH, Institute of Energy and Climate Research (IEK), Microstructure and Properties of Materials (IEK-2) |
| title_full_unstemmed | Thermo-mechanical properties of mixed ion electron conducting membrane materials Bingxin Huang. Forschungszentrum Jülich GmbH, Institute of Energy and Climate Research (IEK), Microstructure and Properties of Materials (IEK-2) |
| title_short | Thermo-mechanical properties of mixed ion electron conducting membrane materials |
| title_sort | thermo mechanical properties of mixed ion electron conducting membrane materials |
| topic_facet | Hochschulschrift |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=024726599&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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