Photoionization of Nitrogen-Containing Reactive Molecules with Synchrotron Radiation: = Photoionisation von stickstoffhaltigen reaktiven Molekülen mit Synchrotronstrahlung
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| Main Author: | |
|---|---|
| Format: | Thesis Book |
| Language: | English |
| Published: |
Würzburg
November 2015
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| Subjects: | |
| Online Access: | Volltext Inhaltsverzeichnis |
| Physical Description: | VIII, 314 Seiten Illustrationen, Diagramme |
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MARC
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| 245 | 1 | 0 | |a Photoionization of Nitrogen-Containing Reactive Molecules with Synchrotron Radiation |b = Photoionisation von stickstoffhaltigen reaktiven Molekülen mit Synchrotronstrahlung |c vorgelegt von Fabian Holzmeier, geboren in Würzburg |
| 246 | 1 | 1 | |a Photoionisation von stickstoffhaltigen reaktiven Molekülen mit Synchrotronstrahlung |
| 264 | 1 | |a Würzburg |c November 2015 | |
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| 336 | |b txt |2 rdacontent | ||
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| 338 | |b nc |2 rdacarrier | ||
| 502 | |b Dissertation |c Julius-Maximilians-Universität Würzburg |d 2016 | ||
| 546 | |a Zusammenfassung in deutscher und englischer Sprache | ||
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| 650 | 0 | 7 | |a Dissoziative Photoionisation |0 (DE-588)4466267-1 |2 gnd |9 rswk-swf |
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Record in the Search Index
| _version_ | 1804176163072901121 |
|---|---|
| adam_text | PHOTOIONIZATION OF
* T
*
OGEN-CO^^ REACTIVE
M O LECU LES W ITH
SYNCHROTRON RADIATION
DISSERTATION ZUR ERLANGUNG DES NATURWISSENSCHAFTLICHEN
DOKTORGRADES DER
JULIUS-MAXIMILIANS-UNIVERSRTAT XA/URZBURG
VORGELEGT VON
FABIAN HOLZMEIER
GEBOREN N WURZBURG
WUERZBURG, NOVEMBER
2015
CONTENTS
LIST OF PUBLICATIONS V
LIST OF ABBREVIATIONS VII
1
. INTRODUCTION 1
2. SPECTROSCOPIC TECHNIQUES 10
2.1 MONOCHROMATIC SYNCHROTRON RADIATION
.
...................................
10
2.1.1. GENERATION AND PROPERTIES OF SYNCHROTRON RADIATION . . 10
2.1.2 SWISS LIGHT SOURCE AND SYNCHROTRON SOLEIL . . . . . . 15
2.1.3 M
ONOCHROMATORS..........................................................
15
2.2.
PHOTOIONIZATION..............................................................................
18
2.3. PHOTOELECTRON
SPECTROSCOPY......................................................... 20
2.3.1. CONVENTIONAL ULTRAVIOLET PHOTOELECTRON SPECTROSCOPY . . 20
2.3.2. THRESHOLD PHOTOELECTRON SPECTROSCOPY . . . . . . . . . . 22
2.3.3 SLOW PHOTOELECTRON SPECTROSCOPY............................... 27
2.4. ROVIBRONIC PHOTOIONIZATION TRANSITIONS
.......................................
33
2.4.1 MOLECULAR R O TA TIO N
S.................................................... 34
2.4.2. PHOTOIONIZATION SELECTION R U
LES................................... 38
2.4.3. ROVIBRONIC INTENSITIES IN PHOTOELECTRON SPECTRA . . . . . 41
2.5. DISSOCIATIVE
PHOTOIONIZATION.........................................................
45
2.5.1. PEPICO
...........................................................................
46
2.5.2. STATISTICAL RATE T H E O R Y
............................................... 47
2.5.3 DATA M
ODELING............................................................. 50
2.6 MOLECULAR INNER SHEUSPE^^
............................................
56
2.6.1. *-*** ABSORPTION AND PHOTOELECTRON SPECTROSCOPY . . . 57
2.6.2. * -RAY EMISSION I D AUGER ELECTRON SPECTROSCOPY . . . . 60
3. EXPERIMENT 67
3.1 PYROLYSIS S O U R C E
....................................................... 67
3.2 SYNCHROTRON SOLEIL DESIRS BEAMLINE . . . . . . . . . . . . . 69
3.3 SWISS LIGHT SOURCE
V U V X04DB
BEAMLINE . . . . . . . . . . . .
74
3.4. SYNCHROTRON SOLEIL PLEIADES BEAMLINE . . . . . . . . . . . 76
3.5 COMPUTATIONAL M ETH O D
S........................................... 78
4. DETERMINATION OF PHOTOIONIZATION CROSS SECTIONS 81
4.1. MASS DISCRIMINATION F A C TO R
...................................... 84
4.2. PHOTOIONIZATION CROSS SECTION OT UYCLOPROPENYLIDENE . . . . . . 91
4.3 SUMMARY PHOTOIONIZATION 94
5. PHOTOIONIZATION OF NITROGEN-CONTAINING INTERMEDIATES 96
5.1. B CY AN IC ACID H N C O
.............................................. 96
5.1.1. VAIENCE SHELL PHOTOIONIZATION OF HNCO . . . . . . . . . 98
5.1.1.1. TPE SPECTRUM OF THE 2
*
* HNC0+ GROUND STATEIOO
5.1.1.2. TPE SPECTRUM OF HNCO 1 EXCITED STATES . . . 109
5.1.1.3. DISSOCIATIVE PHOTOIONIZATION OF HNCO . . . . I L L
5.1.2. INNER SHELL SPECTROSCOPY OF HNCO . . . . . . . . . . . . 117
5.1.2.1. NORMAL AUGER SPECTRA OF HNCO . . . . . . . . 122
5.1.2.2. NEXAFS SPECTRA OF HNCO . . . . . . . . . . 1 3 0
5.1.3. S UM NNY H N C O
........................................................
, . . 1 3 3
5.2 CARBONYL AMIDOGEN N C O
.........................................135
5.2.1. NCO RADICAL G E N E RA TIO N
..................................................
136
5.2.2. TPE SPECTRUM OF N C O
.....................................................
139
5.2.3. SUMMARY N C O
....................................................................
144
5.3 PYRROLYL C4H4N
..............................................................................146
5.3.1 PRECURSOR SELECTION AND MASS SPECTRA . . . . . . . . . . 1 4 8
5.3.2 TPE SPECTRUM OF PYRROLYL . . . . . . . . . . . . . . . . 1 4 9
5.3.3 PYROLYSIS MECHANISM OF *-METHOXYPYRIDINE . . . . . . . 154
5.3.4 DPI OF *-METHOXYPYRIDINE AND ENTHALPY OF FORMATION
OFPYRROLYL
........................................................................160
5.3.5. SUMMARY P Y RRO LY
L............................................................172
5.4. PYROLYSIS OF3-BROMOPYRIDINE
.
........................................................174
5.4.1. HYDROCARBON PYROLYSIS P RO D U C TS
......................................
175
5.4.2. TPE SPECTRUM OF CYANOVINYIACETYLENE . . . . . . . . . . 179
5.4.3 *-P Y RID Y
L.............................................................................
185
5.4.4 SUMMARY PYROLYSIS OF *-BROMOPYRIDINE . . . . . . . . . 190
5.5.
3-PICOLY*............................................................................................
191
5.5.1 R * C A L GENERATION OF 3-PICOLYL
.........................................
191
5.5.2 TPE SPECTRUM OF *-P IC O LY L
...............................................
194
5.5.3. SUMMARY *-PICOLYL
..............................................................
195
6
. PHOTOIONIZATION AND PYROLYSIS OF L *4-DI-TERT-BUTYI-L*4-AZABORININE
196
6.1. PHOTOIONIZATION OF L,4-DI-*ER*-BUTYL-L,4-AZABORINME . . . . . . 198
6.1.1. TPE SPECTRUM OF L,*D I-IERT-B UTYL-L,4-AZAB0RININE . . 198
6.1.2. DPI OF L,4-DI E?I-BUTYL-L,4-AZABORIMNE . . . . . . . . 2 0 2
6.2. PYROLYSIS OF L,4-DI-IER
*
*-BUTYL-L,4-AZABORMME . . . . . . . . . . 212
6.3. SUMMARY L,4 DI-*6RT-BUTYL-L,*AZABORMME . . . . . . . . . . . 223
7. CONCLUSION 226
8
* ZUSAMMENFASSUNG 230
A. FURTHER PROJECTS 234
*.*. IONIZATION ENERGY OF PHENYLPROPAXGYL RADICALS . . . . . . . . . .
234
*.2. DISSOCIATIVE PHOTOIONIZATION OF CYCLOPROPENYLIDENE . . . . . . .
239
*.3. PYROLYSIS OF 3,3,
*
AZOPYRIDME ........................................................ 248
*.4. PYROLYSIS OF
N~AMNOPYRROLE...........................................................
250
*.5. PYROLYSIS OF DI-IERI-BUTYL-IMINOBORANE
.........................................
253
B* SYNTHESIS 256
*.*. ISOCYANIC ACID
................................................................................
256
*.2. CHLORINE ISOCYANATE
.......................................................................
258
*.3. 3
*
3IAZOPYRIDINE
.............................................................................
258
*.4.
IV-AMINOPYRROLE.............................................................................
259
C.
ABSOLUTE PHOTOIONIZATION CROSS SECTION OF CYCLOPROPENYLIDENE
261
D. COMPUTED *ES OF C
4
H
4
W ISOMERS 263
E. SPES DATA TREATMENT FOR SLS 265
F. GEOMETRY OF 1*4-
*
1-1*11-**1**-1*4-*******1** 272
BIBLIOGRAPHY 284
DANKSAGUNG 312
|
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| dewey-tens | 540 - Chemistry and allied sciences |
| discipline | Chemie / Pharmazie |
| format | Thesis Book |
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| language | English |
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| physical | VIII, 314 Seiten Illustrationen, Diagramme |
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| spelling | Holzmeier, Fabian Verfasser (DE-588)1097300749 aut Photoionization of Nitrogen-Containing Reactive Molecules with Synchrotron Radiation = Photoionisation von stickstoffhaltigen reaktiven Molekülen mit Synchrotronstrahlung vorgelegt von Fabian Holzmeier, geboren in Würzburg Photoionisation von stickstoffhaltigen reaktiven Molekülen mit Synchrotronstrahlung Würzburg November 2015 VIII, 314 Seiten Illustrationen, Diagramme txt rdacontent n rdamedia nc rdacarrier Dissertation Julius-Maximilians-Universität Würzburg 2016 Zusammenfassung in deutscher und englischer Sprache Synchrotronstrahlung (DE-588)4184235-2 gnd rswk-swf Ultraviolett-Photoelektronenspektroskopie (DE-588)4264090-8 gnd rswk-swf Pyrolyse (DE-588)4047925-0 gnd rswk-swf Dissoziative Photoionisation (DE-588)4466267-1 gnd rswk-swf (DE-588)4113937-9 Hochschulschrift gnd-content Dissoziative Photoionisation (DE-588)4466267-1 s Pyrolyse (DE-588)4047925-0 s Synchrotronstrahlung (DE-588)4184235-2 s Ultraviolett-Photoelektronenspektroskopie (DE-588)4264090-8 s DE-604 Erscheint auch als Online-Ausgabe urn:nbn:de:bvb:20-opus-127763 https://nbn-resolving.org/urn:nbn:de:bvb:20-opus-127763 Resolving-System kostenfrei Volltext DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=028934194&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Holzmeier, Fabian Photoionization of Nitrogen-Containing Reactive Molecules with Synchrotron Radiation = Photoionisation von stickstoffhaltigen reaktiven Molekülen mit Synchrotronstrahlung Synchrotronstrahlung (DE-588)4184235-2 gnd Ultraviolett-Photoelektronenspektroskopie (DE-588)4264090-8 gnd Pyrolyse (DE-588)4047925-0 gnd Dissoziative Photoionisation (DE-588)4466267-1 gnd |
| subject_GND | (DE-588)4184235-2 (DE-588)4264090-8 (DE-588)4047925-0 (DE-588)4466267-1 (DE-588)4113937-9 |
| title | Photoionization of Nitrogen-Containing Reactive Molecules with Synchrotron Radiation = Photoionisation von stickstoffhaltigen reaktiven Molekülen mit Synchrotronstrahlung |
| title_alt | Photoionisation von stickstoffhaltigen reaktiven Molekülen mit Synchrotronstrahlung |
| title_auth | Photoionization of Nitrogen-Containing Reactive Molecules with Synchrotron Radiation = Photoionisation von stickstoffhaltigen reaktiven Molekülen mit Synchrotronstrahlung |
| title_exact_search | Photoionization of Nitrogen-Containing Reactive Molecules with Synchrotron Radiation = Photoionisation von stickstoffhaltigen reaktiven Molekülen mit Synchrotronstrahlung |
| title_full | Photoionization of Nitrogen-Containing Reactive Molecules with Synchrotron Radiation = Photoionisation von stickstoffhaltigen reaktiven Molekülen mit Synchrotronstrahlung vorgelegt von Fabian Holzmeier, geboren in Würzburg |
| title_fullStr | Photoionization of Nitrogen-Containing Reactive Molecules with Synchrotron Radiation = Photoionisation von stickstoffhaltigen reaktiven Molekülen mit Synchrotronstrahlung vorgelegt von Fabian Holzmeier, geboren in Würzburg |
| title_full_unstemmed | Photoionization of Nitrogen-Containing Reactive Molecules with Synchrotron Radiation = Photoionisation von stickstoffhaltigen reaktiven Molekülen mit Synchrotronstrahlung vorgelegt von Fabian Holzmeier, geboren in Würzburg |
| title_short | Photoionization of Nitrogen-Containing Reactive Molecules with Synchrotron Radiation |
| title_sort | photoionization of nitrogen containing reactive molecules with synchrotron radiation photoionisation von stickstoffhaltigen reaktiven molekulen mit synchrotronstrahlung |
| title_sub | = Photoionisation von stickstoffhaltigen reaktiven Molekülen mit Synchrotronstrahlung |
| topic | Synchrotronstrahlung (DE-588)4184235-2 gnd Ultraviolett-Photoelektronenspektroskopie (DE-588)4264090-8 gnd Pyrolyse (DE-588)4047925-0 gnd Dissoziative Photoionisation (DE-588)4466267-1 gnd |
| topic_facet | Synchrotronstrahlung Ultraviolett-Photoelektronenspektroskopie Pyrolyse Dissoziative Photoionisation Hochschulschrift |
| url | https://nbn-resolving.org/urn:nbn:de:bvb:20-opus-127763 http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=028934194&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT holzmeierfabian photoionizationofnitrogencontainingreactivemoleculeswithsynchrotronradiationphotoionisationvonstickstoffhaltigenreaktivenmolekulenmitsynchrotronstrahlung AT holzmeierfabian photoionisationvonstickstoffhaltigenreaktivenmolekulenmitsynchrotronstrahlung |