Programmed temperature gas chromatography:
Saved in:
| Main Authors: | , |
|---|---|
| Format: | Book |
| Language: | English |
| Published: |
New York
Wiley
1966
|
| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Physical Description: | XVI, 305 S. |
Staff View
MARC
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Record in the Search Index
| _version_ | 1804116380209905664 |
|---|---|
| adam_text | Programmed Temperature
Gas Chromatography
WALTER E HARRIS
Professor of Analytical Chemistry
Department of Chemistry
University of Alberta
Edmonton, Alberta, Canada
HENRY W HABGOOD
Chief Fuels Branch
Research Council of Alberta
Edmonton, Alberta, Canada
John Wiley amp; Sons, Inc , New York / London / Sydney
Contents
Principal symbols x n i
CHAPTERI
GASCHROMATOGRAPHYANDTEMPERATUREPROGRAMMING
1 01 General Introduction 1
1 02 Temperature Programming 11
1 03 Terms and Concepts • • 15
1 04 Summary • • • • • 21
References21
CHAPTER2
TEMPERATUREEFFECTSINGASCHROMATOGRAPHY
2 01 Flow Rate and Pressure Drop 23
2 02 Retention Volume 29
2 03 Band Broadening 34
2 04 Summary 46
References47
CHAPTER3
RETENTIONTHEORYIRETENTIONVOLUMEAND
RETENTIONTEMPERATURE
3 01 Corrected Isothermal Retention Volume 49
3 02 Stepwise Increase in Temperature 51
3 03 Linear Temperature Program 52
3 04 Characteristic Curves of Linear PTGC 56
3 05 Retention Volumes in Linear PTGC 59
3 06 Nonlinear Heating Programs 63
3 07 Effect of Pressure Drop 71
3 08 Exact Solutions to Characteristic Equations 75
3 09 Summary 82
References82
ix
X Contents
CHAPTER4
RETENTIONTHEORYIIOPTIONALANDAPPROXIMATEFORMS
FORTHECALCULATIONSOFPTGC
4 01 Reduced-Temperature Scale: Baumann, Klaver, and Johnson 84
4 02 Universal Curves: Said and Sternberg 86
4 03 Effect of Neglecting the Column Dead space 91
4 04 Calculations Neglecting Dead Space: Rowan 96
4 05 Significant Temperature: Giddings 101
4 06 Direct Use of Observed Retention Volumes and Retention
Times Instead of Pressure-Corrected Values 104
4 07 Summary 107
References107
CHAPTER5
COLUMNEFFICIENCYRESOLUTION
5 01 Column Efficiency: Number of Theoretical Plates 109
5 02 Band Broadening Due to Sample Injection and to Nonuni-
formity of Temperature
503Resolution
5 04 Intrinsic Resolution
5 05 Approximate Expression for Intrinsic Resolution of Closely
Spaced Peaks
5 06 Effect of Large Column Dead Space Capillary Columns
5 07 Relative Retention
5 08 Effective Peak Number
5 09 Maximizing Resolution
5 10 Summary
References
CHAPTER6
QUALITATIVEASPECTSOFRETENTIONTEMPERATURE
6 01 Homologous-Series Relationships 141
6 02 Retention Temperature Constants 149
6 03 Retention Indices 153
6 04 Other Index Systems Carbon Number, Steroid Number,
Phenyl Number 162
6 05 Relative Retention Volumes Theoretical-Nonane System 166
6 06 Summary 167
References168
Contents xi
CHAPTER7
PRACTICALINONINSTRUMENTAL
7 01 When to Choose Temperature Programming 169
7 02 Programming Conditions 172
7 03 Stationary Phase 178
7 04 Inert Support 186
7 05 Column Conditioning 187
7 06 Carrier Gas 188
7 07 Sample Injection 190
7 08 Speed of Analysis 201
7 09 Errors 203
7 10 Detection Limit 210
7 11 Reporting of Data Calculations 214
7 12 Summary 219
References 221
CHAPTER8
PRACTICALIIINSTRUMENTAL
8 01 Stabilization of Carrier-Gas Flow Rate 223
8 02 Base-Line Control, Dual Columns, and Dual Channels 226
8 03 Temperature Control 233
8 04 Laboratory-Built Instruments 242
8 05 Selection of Apparatus 245
8 06 Suppliers of Commercial Equipment 247
8 07 Summary 249
References250
CHAPTER9
SELECTEDAPPLICATIONS
9 01 Mixtures of Wide Boiling Range 251
9 02 Simulated Distillation 266
9 03 Trace Analysis 271
9 04 Pyrolysis Gas Chromatography 273
9 05 Preparative PTGC 276
9 06 Summary 279
References280
APPENDIX
Retention Indices of Hydrocarbons 283
AUTHORINDEX289
SUBJECTINDEX293
|
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| author | Harris, Walter E. Habgood, Henry W. |
| author_facet | Harris, Walter E. Habgood, Henry W. |
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| author_sort | Harris, Walter E. |
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| dewey-tens | 540 - Chemistry and allied sciences |
| discipline | Chemie / Pharmazie |
| format | Book |
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| genre | Temperaturprogramm gnd |
| genre_facet | Temperaturprogramm |
| id | DE-604.BV001939943 |
| illustrated | Not Illustrated |
| indexdate | 2024-07-09T15:37:35Z |
| institution | BVB |
| language | English |
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| physical | XVI, 305 S. |
| psigel | TUB-nveb |
| publishDate | 1966 |
| publishDateSearch | 1966 |
| publishDateSort | 1966 |
| publisher | Wiley |
| record_format | marc |
| spelling | Harris, Walter E. Verfasser aut Programmed temperature gas chromatography Walter E. Harris ; Henry W. Habgood New York Wiley 1966 XVI, 305 S. txt rdacontent n rdamedia nc rdacarrier Chromatographie en phase gazeuse ram Gas chromatography Gaschromatographie (DE-588)4019330-5 gnd rswk-swf Temperaturprogramm gnd rswk-swf Gaschromatographie (DE-588)4019330-5 s Temperaturprogramm f DE-604 Habgood, Henry W. Verfasser aut HEBIS Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=001264430&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Harris, Walter E. Habgood, Henry W. Programmed temperature gas chromatography Chromatographie en phase gazeuse ram Gas chromatography Gaschromatographie (DE-588)4019330-5 gnd |
| subject_GND | (DE-588)4019330-5 |
| title | Programmed temperature gas chromatography |
| title_auth | Programmed temperature gas chromatography |
| title_exact_search | Programmed temperature gas chromatography |
| title_full | Programmed temperature gas chromatography Walter E. Harris ; Henry W. Habgood |
| title_fullStr | Programmed temperature gas chromatography Walter E. Harris ; Henry W. Habgood |
| title_full_unstemmed | Programmed temperature gas chromatography Walter E. Harris ; Henry W. Habgood |
| title_short | Programmed temperature gas chromatography |
| title_sort | programmed temperature gas chromatography |
| topic | Chromatographie en phase gazeuse ram Gas chromatography Gaschromatographie (DE-588)4019330-5 gnd |
| topic_facet | Chromatographie en phase gazeuse Gas chromatography Gaschromatographie Temperaturprogramm |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=001264430&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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